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1. 发明授权

US07279075B2 Thermal separating process between at least one gaseous and at least one liquid stream, of which at least one comprises (meth)acrylic monomers 有权
标题翻译：至少一种气态和至少一种液体物流之间的热分离过程，其中至少一种液体物流包含（甲基）丙烯酸单体
公开(公告)号：US07279075B2
公开(公告)日：2007-10-09
申请号：US10647241
申请日：2003-08-26
申请人： Joachim Thiel , Hugues Vandenmersch , Juergen Schroeder , Albrecht Dams
发明人： Joachim Thiel , Hugues Vandenmersch , Juergen Schroeder , Albrecht Dams
IPC分类号： B01D3/42 , C07C51/42
CPC分类号： C07C51/44 , C07C45/783 , C07C45/81 , C07C45/82 , C07C67/54 , Y10S203/11 , C07C57/04 , C07C69/54
摘要： In a thermal separating process between at least one gaseous and at least one liquid stream, of which at least one comprises (meth)acrylic monomers, in a separating column containing sieve trays as separating internals, at least some of the sieve trays are operated above an entrainment fraction of 10% by weight.
摘要翻译：在至少一种气态和至少一种液态物流之间的热分离过程中，至少一种液体物流在至少一种包含（甲基）丙烯酸类单体的分离塔中，该分离塔含有作为分离内部物质的筛板，至少一些筛板在上面操作 10％重量的夹带部分。

2. 发明授权

US07294240B2 Method for producing (meth)acrylic acid esters 有权
标题翻译：（甲基）丙烯酸酯的制造方法
公开(公告)号：US07294240B2
公开(公告)日：2007-11-13
申请号：US10479962
申请日：2002-05-28
申请人： Matthias Geisendoerfer , Gerhard Nestler , Juergen Schroeder , Hugues Vandenmersch
发明人： Matthias Geisendoerfer , Gerhard Nestler , Juergen Schroeder , Hugues Vandenmersch
IPC分类号： B01D3/34 , C07C213/06 , C07C213/10 , C07C51/44 , C07C67/54
CPC分类号： C07C213/06 , C07C213/10 , Y02P20/582 , Y10S203/20 , Y10S203/22 , Y10S203/90 , C07C219/08
摘要： Basic (meth)acrylates IV are prepared by transesterification of alkyl (meth)acrylates I in the presence of a catalyst and working-up of the reaction mixture by distillation, by a process in which a gas or gas mixture which is inert under the reaction conditions is passed through the reaction zone and/or heat exchanger.
摘要翻译：碱性（甲基）丙烯酸酯IV通过烷基（甲基）丙烯酸烷基酯I在催化剂存在下进行酯交换和通过蒸馏处理反应混合物，通过其中反应惰性气体或气体混合物条件通过反应区和/或热交换器。

3. 发明授权

US07071354B2 Method for producing N-phosphonomethylglycine 失效
标题翻译： N-膦酰基甲基甘氨酸的制备方法
公开(公告)号：US07071354B2
公开(公告)日：2006-07-04
申请号：US10481565
申请日：2002-06-21
申请人： Hugues Vandenmersch , Hartwig Voss , Stefan Orsten , Christian Wulff
发明人： Hugues Vandenmersch , Hartwig Voss , Stefan Orsten , Christian Wulff
IPC分类号： C07F9/22 , C07F9/28
CPC分类号： C07F9/3813
摘要： The present invention relates to a process for the recovery of N-phosphonomethylglycine from an aqueous mixture which contains N-phosphonomethylglycine, ammonium halides, and alkali metal or alkaline earth metal halides and optionally organic impurities in dissolved form, where (a) the pH of the mixture is adjusted to a value in the range from 2 to 8, (b) a separation of the mixture on a selective nanofiltration membrane is performed, a retentate which is richer in N-phosphonomethylglycine and poorer in halides and a permeate which is richer in halides and poorer in N-phosphonomethylglycine being obtained, and (c) the N-phosphonomethylglycine is recovered from the retentate. The process according to the invention makes possible the recovery of the N-phosphonomethylglycine with simultaneous separation of the halide salts.
摘要翻译：本发明涉及从含有N-膦酰基甲基甘氨酸，卤化铵和碱金属或碱土金属卤化物和任选的溶解形式的有机杂质的含水混合物中回收N-膦酰基甲基甘氨酸的方法，其中（a）将混合物调节至2至8范围内的值，（b）进行选择性纳滤膜上的混合物分离，更富含N-膦酰基甲基甘氨酸并且较差的卤化物的渗余物和富含物的渗透物在得到的N-膦酰基甲基甘氨酸的卤化物和较差的碱中，和（c）从渗余物中回收N-膦酰基甲基甘氨酸。根据本发明的方法使得可以同时分离卤化物盐来回收N-膦酰基甲基甘氨酸。

4. 发明申请

US20120073953A1 PROCESS FOR ISOLATING TETRAHYDROFURAN 有权
标题翻译：分离四氢呋喃的方法
公开(公告)号：US20120073953A1
公开(公告)日：2012-03-29
申请号：US13235427
申请日：2011-09-18
申请人： Maria GUIXA GUARDIA , Rolf Pinkos , Nadja Pollmer , Wolf-Steffen Weissker , Hugues Vandenmersch
发明人： Maria GUIXA GUARDIA , Rolf Pinkos , Nadja Pollmer , Wolf-Steffen Weissker , Hugues Vandenmersch
IPC分类号： B01D3/36
CPC分类号： B01D3/143 , B01D3/36 , C07D307/36
摘要： A process which isolates tetrahydrofuran from a stream of tetrahydrofuran, alkanol and high boilers, by: (a) separating off a first stream of tetrahydrofuran and alkanol as azeotrope in a first distillation stage; (b) feeding part of the first stream into a reactor for esterifying maleic anhydride, giving a second stream of tetrahydrofuran and monoalkyl maleate; (c) separating the second stream into a third stream of monoalkyl maleate and a fourth stream of tetrahydrofuran in a second distillation stage; (d) feeding the fourth stream of tetrahydrofuran from the second distillation stage and the part of the first stream from (a) which is not fed to the reactor into a third distillation stage to obtain a product stream of tetrahydrofuran and a sixth stream of tetrahydrofuran and alkanol; (e) recirculating the sixth stream from the third distillation stage into the first distillation stage or the reactor in (b).
摘要翻译：通过以下步骤分离四氢呋喃与四氢呋喃，烷醇和高沸点物流的方法：（a）在第一蒸馏阶段中分离第一流的四氢呋喃和链烷醇作为共沸物; （b）将第一流的一部分进料到用于酯化马来酸酐的反应器中，得到第二股四氢呋喃和马来酸单烷基酯; （c）在第二蒸馏阶段将第二物流分离成马来酸单烷基酯和第四四氢呋喃流; （d）将来自第二蒸馏阶段的第四个四氢呋喃流和来自（a）的未进料到反应器的第一个物流部分进入第三个蒸馏阶段以获得四氢呋喃的产物流和第六个四氢呋喃流和链烷醇; （e）将第六流从第三蒸馏段再循环到第一蒸馏阶段或（b）中的反应器中。

5. 发明授权

US09186599B2 Process for isolating tetrahydrofuran 有权
标题翻译：四氢呋喃分离方法
公开(公告)号：US09186599B2
公开(公告)日：2015-11-17
申请号：US13235427
申请日：2011-09-18
申请人： Maria Guixa Guardia , Rolf Pinkos , Nadja Pollmer , Wolf-Steffen Weissker , Hugues Vandenmersch
发明人： Maria Guixa Guardia , Rolf Pinkos , Nadja Pollmer , Wolf-Steffen Weissker , Hugues Vandenmersch
IPC分类号： C07D307/00 , B01D3/14 , B01D3/36 , C07D307/36
CPC分类号： B01D3/143 , B01D3/36 , C07D307/36
摘要： A process which isolates tetrahydrofuran from a stream of tetrahydrofuran, alkanol and high boilers, by: (a) separating off a first stream of tetrahydrofuran and alkanol as azeotrope in a first distillation stage; (b) feeding part of the first stream into a reactor for esterifying maleic anhydride, giving a second stream of tetrahydrofuran and monoalkyl maleate; (c) separating the second stream into a third stream of monoalkyl maleate and a fourth stream of tetrahydrofuran in a second distillation stage; (d) feeding the fourth stream of tetrahydrofuran from the second distillation stage and the part of the first stream from (a) which is not fed to the reactor into a third distillation stage to obtain a product stream of tetrahydrofuran and a sixth stream of tetrahydrofuran and alkanol; (e) recirculating the sixth stream from the third distillation stage into the first distillation stage or the reactor in (b).
摘要翻译：通过以下步骤分离四氢呋喃与四氢呋喃，烷醇和高沸点物流的方法：（a）在第一蒸馏阶段中分离第一流的四氢呋喃和链烷醇作为共沸物; （b）将第一流的一部分进料到用于酯化马来酸酐的反应器中，得到第二股四氢呋喃和马来酸单烷基酯; （c）在第二蒸馏阶段将第二物流分离成马来酸单烷基酯和第四四氢呋喃流; （d）将来自第二蒸馏阶段的第四个四氢呋喃流和来自（a）的未进料到反应器中的第一个物流部分进入第三个蒸馏阶段以获得四氢呋喃的产物流和第六个四氢呋喃流和链烷醇; （e）将第六流从第三蒸馏段再循环到第一蒸馏阶段或（b）中的反应器中。

6. 发明申请

US20080146831A1 Continuous Method for Producing Cyclohexyl(Meth)Acrylate 审中-公开
标题翻译：连续生产环己基（甲基）丙烯酸酯的方法
公开(公告)号：US20080146831A1
公开(公告)日：2008-06-19
申请号：US11814148
申请日：2006-02-10
申请人： Hugues Vandenmersch , Mattias Geisendorfer , Horst Hofmann
发明人： Hugues Vandenmersch , Mattias Geisendorfer , Horst Hofmann
IPC分类号： C07C69/76
CPC分类号： C07C67/08 , C07C67/54 , C07C67/62 , C07C2601/14 , C07C69/54
摘要： A continuous process is proposed for preparing cyclohexyl (meth)acrylate by acid-catalyzed esterification of cyclohexanol with glacial (meth)acrylic acid in the presence of an azeotroping agent for the water of esterification and of a polymerization inhibitor, comprising the following process steps: esterification of the (meth)acrylic acid (1) with cyclohexanol (2) in the presence of the acidic catalyst (3), of the polymerization inhibitor (4) and of the azeotroping agent for the water of esterification (5) in a reaction zone (A), in which the water of esterification is removed as an azeotrope with the azeotroping agent in a distillation zone attached to the reaction zone (A) to obtain a reaction effluent (process stage A) which is fed to a neutralization in which the acidic catalyst (3) and unconverted (meth)acrylic acid (1) from the reaction effluent from the esterification are neutralized by means of an alkaline solution to obtain crude cyclohexyl (meth)acrylate (process stage B); washing of the crude cyclohexyl (meth)acrylate from process stage (B), in which residues of salts are removed from the crude cyclohexyl (meth)acrylate (process stage C), and subsequent distillative workup of the crude cyclohexyl (meth)acrylate (process stages D to G).
摘要翻译：提出了在酯化水共聚剂和阻聚剂共沸剂存在下，通过环己醇与冰川（甲基）丙烯酸的酸催化酯化制备环己基（甲基）丙烯酸酯的连续方法，包括以下步骤：在酸性催化剂（3），聚合抑制剂（4）和酯化水共沸剂（5）的反应中，（甲基）丙烯酸（1）与环己醇（2）的酯化反应区域（A），其中在与反应区（A）连接的蒸馏区中与共沸剂作为共沸物除去酯化水，得到反应流出物（处理阶段A），其进料到中和，其中来自酯化反应流出物的酸性催化剂（3）和未转化的（甲基）丙烯酸（1）通过碱溶液中和，得到粗制环己基（甲基）丙烯酸酯（工艺阶段B）; 从粗制环己基（甲基）丙烯酸酯（工艺阶段C）除去盐的残留物的方法阶段（B）中洗涤粗制环己基（甲基）丙烯酸酯，随后进行粗制环己基（甲基）丙烯酸酯处理阶段D至G）。

7. 发明授权

US06200429B1 Method for trioxane isolation 失效
标题翻译：三恶烷分离方法
公开(公告)号：US06200429B1
公开(公告)日：2001-03-13
申请号：US09462627
申请日：2000-01-11
申请人： Reinhard Freyhof , Stefan Bitterlich , Hugues Vandenmersch
发明人： Reinhard Freyhof , Stefan Bitterlich , Hugues Vandenmersch
IPC分类号： B01D300
CPC分类号： B01D61/362 , C07D323/06 , Y10S159/27 , Y10S159/28
摘要： A process for isolating trioxane from an aqueous mixture which includes trioxane, water and formaldehyde, including removing trioxane from the mixture by pervaporation, and subjecting the mixture enriched in trioxane (permeate) to rectification to give trioxane and an azeotropic mixture of trioxane, water and formaldehyde.
摘要翻译：从含有三恶烷，水和甲醛的含水混合物中分离三恶烷的方法，包括通过渗透蒸发从混合物中除去三恶烷，并将富含三恶烷（渗透物）的混合物进行精馏，得到三恶烷，三恶烷，水和三恶烷的共沸混合物甲醛。

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