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1. 发明授权

US5910612A Preparation of anhydrous 2-amino-1-methoxypropane 失效
标题翻译：无水2-氨基-1-甲氧基丙烷的制备
公开(公告)号：US5910612A
公开(公告)日：1999-06-08
申请号：US82543
申请日：1998-05-21
申请人： Joachim Simon , Andreas Henne , Heinz Lingk
发明人： Joachim Simon , Andreas Henne , Heinz Lingk
IPC分类号： C07C213/02 , C07C213/10 , C07C217/08 , C07C209/02
CPC分类号： C07C213/02 , C07C213/10
摘要： The process for preparing anhydrous 2-amino-1-methoxypropane proceeds by(a) admixing a 2-amino-1-methoxypropane-containing water-containing reaction mixture, obtainable from the reaction of 1-methoxy-2-propanol with ammonia on a catalyst, with sodium hydroxide solution, forming an aqueous phase containing sodium hydroxide solution and a 2-amino-1-methoxypropane-containing phase,(b) separating off the 2-amino-1-methoxypropane-containing phase from the aqueous phase and(c) distilling the 2-amino-1-methoxypropane-containing phase, an azeotrope of water and 2-amino-1-methoxypropane, which is recycled to step (a) or (b), first being produced and anhydrous 2-amino-1-methoxypropane then being produced.
摘要翻译：制备无水2-氨基-1-甲氧基丙烷的方法是：（a）将可从1-甲氧基-2-丙醇反应得到的含2-氨基-1-甲氧基丙烷的含水反应混合物与氨混合，催化剂，用氢氧化钠溶液，形成含有氢氧化钠溶液和含2-氨基-1-甲氧基丙烷的相的水相，（b）从水相中分离出含2-氨基-1-甲氧基丙烷的相和（ c）蒸馏出含有2-氨基-1-甲氧基丙烷的相，再循环至步骤（a）或（b）的水和2-氨基-1-甲氧基丙烷的共沸物，首先制得无水2-氨基-1-甲氧基丙烷，然后生产1-甲氧基丙烷。

2. 发明授权

US5847131A Preparation of N-substituted cyclic amines 失效
标题翻译： N-取代的环胺的制备
公开(公告)号：US5847131A
公开(公告)日：1998-12-08
申请号：US876329
申请日：1997-06-16
申请人： Joachim Simon , Roman Dostalek , Heinz Lingk , Rainer Becker , Andreas Henne , Rolf Lebkucher , Cristina Freire Erdbrugger , Michael Hesse , Detlef Kratz
发明人： Joachim Simon , Roman Dostalek , Heinz Lingk , Rainer Becker , Andreas Henne , Rolf Lebkucher , Cristina Freire Erdbrugger , Michael Hesse , Detlef Kratz
IPC分类号： C07D295/02 , B01J23/72 , B01J37/02 , C07B61/00 , C07D295/03 , C07D295/023
CPC分类号： C07D295/03 , B01J23/72 , B01J37/0203
摘要： N-Substituted cyclic amines are prepared by reacting diols with primary amines over a copper-containing catalyst which is obtainable by impregnation of an inert support with an aqueous solution of an ammine complex of a readily thermally decomposable copper compound and subsequent drying and calcination and contains from 5 to 50% by weight of copper, calculated as CuO.
摘要翻译： N-取代的环胺通过二元醇与伯胺在含铜催化剂上反应制备，所述催化剂可通过用容易热分解的铜化合物的氨络合物的水溶液浸渍惰性载体而得到，随后进行干燥和煅烧， 5至50重量％的铜，以CuO计。

3. 发明授权

US6111100A Preparation of bis(2-morpholinoethyl) ether 有权
标题翻译：双（2-吗啉代乙基）醚的制备
公开(公告)号：US6111100A
公开(公告)日：2000-08-29
申请号：US474906
申请日：1999-12-30
申请人： Hartmut Riechers , Joachim Simon , Andreas Henne , Arthur Hohn
发明人： Hartmut Riechers , Joachim Simon , Andreas Henne , Arthur Hohn
IPC分类号： C07D295/08 , B01J23/72 , C07D295/088 , C07D413/12
CPC分类号： C07D295/088
摘要： In a process for preparing bis(2-morpholinoethyl) ether by reacting diethylene glycol with ammonia under superatmospheric pressure and at elevated temperature in the presence of hydrogen and a hydrogenation catalyst, the catalytically active composition of the catalyst prior to reduction with hydrogen comprisesfrom 20 to 85% by weight of aluminum oxide (Al.sub.2 O.sub.3), zirconium dioxide (ZrO.sub.2), titanium dioxide (TiO.sub.2) and/or silicon dioxide (SiO.sub.2),from 1 to 70% by weight of oxygen-containing compounds of copper, calculated as CuO,from 0 to 50% by weight of oxygen-containing compounds of magnesium, calculated as MgO, oxygen-containing compounds of chromium, calculated as Cr.sub.2 O.sub.3, oxygen-containing compounds of zinc, calculated as ZnO, oxygen-containing compounds of barium, calculated as BaO, and/or oxygen-containing compounds of calcium, calculated as CaO, andless than 20% by weight of oxygen-containing compounds of nickel, calculated as NiO, based on the oxygen-containing compounds of copper, calculated as CuO.
摘要翻译：在氢气和氢化催化剂的存在下，在二氧化乙烯与氨在超大气压和升高的温度下反应制备双（2-吗啉代乙基）醚的方法中，用氢还原之前的催化剂催化活性组合物包括20 至85重量％的氧化铝（Al 2 O 3），二氧化锆（ZrO 2），二氧化钛（TiO 2）和/或二氧化硅（SiO 2），1至70重量％的含氧化合物的铜，以CuO ，0〜50重量％的以氧化镁计的含氧化合物的镁，以Cr 2 O 3计算的含氧化合物的铬，以ZnO计的氧的含氧化合物，钡的含氧化合物，计算值作为BaO，和/或以CaO计的钙的含氧化合物，以NiO计，基于含氧化合物的铜，小于20重量％的含氧化合物的镍，以CuO计算。

4. 发明授权

US6093677A Catalyst for dehydrogenating 1,4-butanediol to .gamma.-butyrolactone 有权
标题翻译：将1,4-丁二醇脱氢为γ-丁内酯的催化剂
公开(公告)号：US6093677A
公开(公告)日：2000-07-25
申请号：US323919
申请日：1999-06-02
申请人： Hans Jochen Mercker , Frank-Friedrich Pape , Joachim Simon , Andreas Henne , Michael Hesse , Ulrich Kohler , Roman Dostalek , Cristina Freire Erdbrugger , Detlef Kratz
发明人： Hans Jochen Mercker , Frank-Friedrich Pape , Joachim Simon , Andreas Henne , Michael Hesse , Ulrich Kohler , Roman Dostalek , Cristina Freire Erdbrugger , Detlef Kratz
IPC分类号： C07D307/33 , B01J23/72 , B01J23/78 , C07B61/00 , C07D315/00 , B01J23/70
CPC分类号： C07D315/00 , B01J23/78 , B01J23/72 , B01J35/0053 , B01J35/0066
摘要： A process for dehydrogenating 1,4-butanediol to .gamma.-butyrolactone in the gas phase in the presence of a copper-containing catalyst, wherein the catalyst contains 4-40% by weight of copper and 0-5% by weight of Na.sub.2 O, based on the total weight of the catalyst, on a carrier consisting of 80-100% by weight of SiO.sub.2 and 0-20% by weight of CaO.
摘要翻译：在含铜催化剂存在下，在气相中将1,4-丁二醇脱氢为γ-丁内酯的方法，其中催化剂含有4-40重量％的铜和0-5重量％的Na 2 O，基于在由80-100重量％的SiO 2和0-20重量％的CaO组成的载体上的催化剂的总重量。

5. 发明授权

US5955620A Dehydrogenation of 1,4-butanediol to .gamma.-butyrolactone 失效
标题翻译：将1,4-丁二醇脱氢成γ-丁内酯
公开(公告)号：US5955620A
公开(公告)日：1999-09-21
申请号：US923553
申请日：1997-09-04
申请人： Hans Jochen Mercker , Frank-Friedrich Pape , Joachim Simon , Andreas Henne , Michael Hesse , Ulrich Kohler , Roman Dostalek , Cristina Freire Erdbrugger , Detlef Kratz
发明人： Hans Jochen Mercker , Frank-Friedrich Pape , Joachim Simon , Andreas Henne , Michael Hesse , Ulrich Kohler , Roman Dostalek , Cristina Freire Erdbrugger , Detlef Kratz
IPC分类号： C07D307/33 , B01J23/72 , B01J23/78 , C07B61/00 , C07D315/00 , C07D307/32
CPC分类号： C07D315/00 , B01J23/78 , B01J23/72 , B01J35/0053 , B01J35/0066
摘要： A process for dehydrogenating 1,4-butanediol to .gamma.-butyrolactone in the gas phase in the presence of a copper-containing catalyst, wherein the catalyst contains 4-40% by weight of copper and 0-5% by weight of Na.sub.2 O, based on the total weight of the catalyst, on a carrier consisting of 80-100% by weight of SiO.sub.2 and 0-20% by weight of CaO.
摘要翻译：在含铜催化剂存在下，在气相中将1,4-丁二醇脱氢为γ-丁内酯的方法，其中催化剂含有4-40重量％的铜和0-5重量％的Na 2 O，基于在由80-100重量％的SiO 2和0-20重量％的CaO组成的载体上的催化剂的总重量。

6. 发明授权

US06403787B2 Thermoplastic material consisting of aliphatic carbamic acid derivatives of polysaccharides and low-molecular urea derivatives as well as a process for their preparation and use of the same 失效
标题翻译：由多糖和低分子量脲衍生物的脂肪族氨基甲酸衍生物组成的热塑性材料以及它们的制备和使用方法
公开(公告)号：US06403787B2
公开(公告)日：2002-06-11
申请号：US08831213
申请日：1997-04-02
申请人： Jürgen Engelhardt , Joachim Simon , Hanns-Peter Müller , Rainhard Koch , Dirk-Jacques Dijkstra
发明人： Jürgen Engelhardt , Joachim Simon , Hanns-Peter Müller , Rainhard Koch , Dirk-Jacques Dijkstra
IPC分类号： C08B900
CPC分类号： C08B15/06 , C08B11/20 , Y10T428/31978
摘要： The present invention relates to evenly substituted polysaccharide derivatives having the general structure: polysaccharide—O—R wherein polysaccharide—O represents a substituted or unsubstituted polysaccharide unit and R is a substituent of a polysaccharide-OH group having either the structure R=—A—B— or the structure R=—B—, wherein A is a linear polyether chain having the following structure: A=(—D—O—)n wherein D denotes a linear aliphatic branched or unbranched chain having 2 to 12 C atoms, O represents an oxygen atom and n is a number equal to or greater than 1, and B represents a substituted carbamic acid having the structure wherein E denotes a linear or branched aliphatic chain having 1 to 18 C atoms.
摘要翻译：本发明涉及具有以下一般结构的均匀取代的多糖衍生物：其中多糖-O代表取代或未取代的多糖单元，R是具有结构或其结构的多糖-OH基团的取代基，其中A是具有以下结构：其中D表示具有2至12个C原子的直链脂族支链或非支链链，O表示氧原子，n表示等于或大于1的数，B表示具有结构的取代氨基甲酸，其中E表示直链或具有1至18个C原子的支链脂族链。

7. 发明授权

US06353118B1 Dewatering and purification of crude pyrrolidine 有权
标题翻译：脱水和纯化粗吡咯烷
公开(公告)号：US06353118B1
公开(公告)日：2002-03-05
申请号：US09716835
申请日：2000-11-20
申请人： Joachim Simon , Peter Wahl , Willi Schmidt
发明人： Joachim Simon , Peter Wahl , Willi Schmidt
IPC分类号： C07O295023
CPC分类号： C07D295/023
摘要： In a process for purifying crude pyrrolidine to give a pyrrolidine composition comprising more than 99% (m/m) of pyrrolidine and less than 0.3% (m/m) of water, crude pyrrolidine comprising from 40 to 98% (m/m) of pyrrolidine and having a water content of more than 2% (m/m) is subjected to continuous distillation at a pressure at the top of less than 950 hPa in a column having a stripping section and a rectifying section.
摘要翻译：在纯化粗制吡咯烷的方法中，得到包含大于99％（m / m）的吡咯烷和小于0.3％（m / m）的水的吡咯烷组合物，包含40-98％（m / m）的吡咯烷并且具有大于2％（m / m）的水含量的混合物在具有汽提段和精馏段的塔中在小于950hPa的顶部的压力下进行连续蒸馏。

8. 发明授权

US06191071B1 Plant-treatment agents 失效
标题翻译：植物处理剂
公开(公告)号：US06191071B1
公开(公告)日：2001-02-20
申请号：US09297628
申请日：1999-05-04
申请人： Joachim Simon , Hanns Peter Müller , Uwe Priesnitz , Hans-Georg Rast
发明人： Joachim Simon , Hanns Peter Müller , Uwe Priesnitz , Hans-Georg Rast
IPC分类号： A01N2510
CPC分类号： A01N25/10
摘要： The invention concerns novel plant-treatment agents comprising: at least one thermoplastically processable biodegradable polyester amide, optionally in a mixture with one or a plurality of further thermoplastically processable, biodegradable polymer components; at least one agrochemical substance; and optionally additives. The invention further concerns a process for preparing these agents, and their use in the application of agrochemical substances.
摘要翻译：本发明涉及新颖的植物处理剂，其包括：至少一种热塑性可加工的可生物降解的聚酯酰胺，任选地与一种或多种另外的热塑性可加工的可生物降解的聚合物组分的混合物; 至少一种农用化学物质; 和任选的添加剂。本发明还涉及制备这些试剂的方法及其在应用农药物质中的应用。

9. 发明授权

US6162928A Preparation of pyrroles 有权
标题翻译：吡咯的制备
公开(公告)号：US6162928A
公开(公告)日：2000-12-19
申请号：US553254
申请日：2000-04-20
申请人： Joachim Wulff-Doring , Joachim Simon , Michael Hesse , Peter Wahl
发明人： Joachim Wulff-Doring , Joachim Simon , Michael Hesse , Peter Wahl
IPC分类号： B01J23/44 , B01J23/63 , C07B61/00 , C07D207/32 , C07D207/323
CPC分类号： C07D207/323 , B01J23/44 , B01J23/63
摘要： A process for preparing pyrroles of the formula I: ##STR1## where R.sub.1, R.sup.2, R.sup.3 and R.sup.4 are identical or different and are hydrogen atoms, alkyl groups having from 1 to 12 carbon atoms or cycloalkyl groups having from 3 to 12 carbon atoms, by dehydrogenation of pyrrolidines of the formula II: ##STR2## where R.sup.1, R.sup.2, R.sup.3 and R.sup.4 are as defined above, in the presence of a supported noble metal catalyst is described. In this process, the dehydrogenation is carried out at from 150 to 300.degree. C. and pressures of from 0.01 to 50 bar and the noble metal catalyst comprises from 30 to 100% by weight of:a) palladium on an oxide of a rare earth or an oxide of an element of the 4.sup.th group (transition group IV) of the Periodic Table, orb) a platinum/palladium mixture on aluminum oxide, an oxide of a rare earth or an oxide of an element of the 4.sup.th groupand from 0 to 70% by weight of alkali metal oxide or alkaline earth metal oxide.
摘要翻译：制备式I的吡咯的方法：其中R 1，R 2，R 3和R 4相同或不同，为氢原子，具有1至12个碳原子的烷基或具有3至12个碳原子的环烷基，通过脱氢描述了在负载的贵金属催化剂的存在下，式II的吡咯烷（其中R 1，R 2，R 3和R 4如上定义）。在该方法中，脱氢在150-300℃，压力为0.01至50巴，贵金属催化剂包含30-100重量％的：a）在稀土氧化物上的钯或元素周期表第4族元素（过渡组IV）的氧化物，或b）在氧化铝上的铂/钯混合物，稀土的氧化物或第4族元素的氧化物， 0〜70重量％的碱金属氧化物或碱土金属氧化物。

10. 发明授权

US6160178A Racemization of optically active amines 有权
标题翻译：光学活性胺的外消旋化
公开(公告)号：US6160178A
公开(公告)日：2000-12-12
申请号：US303599
申请日：1999-05-03
申请人： Hartmut Riechers , Joachim Simon , Arthur Hohn , Andreas Kramer , Frank Funke , Wolfgang Siegel , Christoph Nubling
发明人： Hartmut Riechers , Joachim Simon , Arthur Hohn , Andreas Kramer , Frank Funke , Wolfgang Siegel , Christoph Nubling
IPC分类号： B01J23/72 , B01J23/755 , B01J37/18 , C07B55/00 , C07B61/00 , C07C209/00 , C07C209/68 , C07C211/07 , C07C213/08 , C07C217/08
CPC分类号： C07C213/08 , C07B2200/07 , C07C209/68 , C07C217/08 , C07C211/07
摘要： Optically active amines are racemized by reaction of the optically active amine in the gas phase at elevated temperature in the presence of hydrogen and a hydrogenation or dehydrogenation catalyst.
摘要翻译：光学活性胺通过在氢气和氢化或脱氢催化剂存在下在高温下在气相中的光学活性胺的反应进行外消旋化。

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