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1. 发明授权

US06270540B1 Star-like poly(oxyalkyene)triamide alkoxylates gasoline additive and the method for producing the same 失效
标题翻译：星状聚（氧化烯）三酰胺烷氧基化汽油添加剂及其制备方法
公开(公告)号：US06270540B1
公开(公告)日：2001-08-07
申请号：US09411651
申请日：1999-10-04
申请人： Jiang-Jen Lin , I-Fun Su , Kun-Hai Lin , Yung-Sheng Ho , Che-Nan Lee , Wen-Jei Shiu , Wei-Shiun Ku
发明人： Jiang-Jen Lin , I-Fun Su , Kun-Hai Lin , Yung-Sheng Ho , Che-Nan Lee , Wen-Jei Shiu , Wei-Shiun Ku
IPC分类号： C10L118
CPC分类号： C10L1/238 , C10L1/143 , C10L10/04
摘要： A new class of useful gasoline additives is prepared via two consecutive reactions including: (1) amidation of water-soluble hydrophilic, low molecular weight triamine with alkyl acetate at an elevated temperature under N2 pressure to prepare a symmetrical triamide; and (2) alkoxylation of the triamides with 1,2-epoxyalkane to prepare poly(oxyalkylene)triamide alkoxylate of three telechelic hydroxy groups, having the general formula: wherein x, y and z are from 1 to 20, R is poly(oxyalkylene) of a molecular weight from 72 to 1000, and R′ is an alkyl having a carbon number from 2 to 18.
摘要翻译：通过两个连续的反应制备了一类新的有用的汽油添加剂，包括：（1）在氮气压力升高的温度下，将水溶性亲水性低分子量三胺与乙酸烷基酯酰胺化以制备对称的三酰胺; 和（2）三酰胺与1,2-环氧烷烃的烷氧基化以制备三个遥爪羟基的聚（氧化烯）三酰胺烷氧基化物，其具有以下通式：其中x，y和z为1至20，R为聚（氧化烯），分子量为72〜1000，R'为碳数为2〜18的烷基。

2. 发明授权

US06627775B2 Process for manufacturing gasoline additives of ester-free polyoxyalkylene amide 失效
标题翻译：制造无酯聚氧化烯酰胺汽油添加剂的方法
公开(公告)号：US06627775B2
公开(公告)日：2003-09-30
申请号：US10056014
申请日：2002-01-28
申请人： Jiang-Jen Lin , Yung-Sheng Ho , Wei-Shiun Ku , Wen-Jei Shiu , Che-Nan Lee
发明人： Jiang-Jen Lin , Yung-Sheng Ho , Wei-Shiun Ku , Wen-Jei Shiu , Che-Nan Lee
IPC分类号： C07C23305
CPC分类号： C10L1/224 , C07C233/36 , C08G65/2633 , C08G65/3322 , C08G65/333 , C08G2650/50 , C10L1/22 , C10L1/238 , C10L10/04
摘要： An improved process to prepare poly(oxyalkylene)amide for gasoline additives involves three consecutive reactions. The reactions are (1) amidation of water-soluble low molecular weight of polyalkylene polyamine with alkyl acetate at an elevated temperature under N2 pressure to convert amines to amides, (2) Butoxylation of the amides with 1,2-epoxybutane to prepare the poly(oxyalkylene) amides, and (3) selective hydrolysis of in situ poly(oxyalkylene)-amine-ester-amides into poly(oxyalkylene)-amine-alcohol-amides and removal of acetic acid byproducts, via acid/base hydrolysis and water extraction procedures. The process step of selective hydrolysis is essential for removal the harmful composition of poly(oxyalkylene)-amine-ester-amides in resulting the better performance of the additive, particularly the positive engine's octane requirement or reducing the combustion chamber deposits. More specifically the butoxylation process generally produces poly(oxyalkylene)amides and poly(oxyalkylene)esters via an exchange reaction (trans-amidation/trans-esterification) and the poly(oxyalkylene)esters in the product mixtures is removed to obtain better performance products.
摘要翻译：制备用于汽油添加剂的聚（氧化烯）酰胺的改进方法包括三次连续的反应。反应是（1）在氮气压力升高的温度下，将水溶性低分子量聚亚烷基多胺与烷基乙酸酯进行酰胺化以将胺转化为酰胺，（2）用1,2-环氧丁烷对酰胺进行丁氧基化以制备聚（氧化烯）酰胺，和（3）通过酸/碱水解和水提取将原位聚（氧化烯） - 胺 - 酯 - 酰胺选择性水解成聚（氧化烯） - 胺 - 醇 - 酰胺和除去乙酸副产物程序。选择性水解的工艺步骤对于去除聚（氧化烯） - 胺 - 酯 - 酰胺的有害组合物是必不可少的，从而获得更好的添加剂性能，特别是正发动机的辛烷值要求或减少燃烧室沉积物。更具体地，丁氧基化方法通常通过交换反应（反式酰胺化/反式酯化）产生聚（氧化烯）酰胺和聚（氧化烯）酯，并且除去产物混合物中的聚（氧化烯）酯以获得更好的性能产物。

3. 发明授权

US06454818B1 Poly(oxyalkylene) amide-amine gasoline additives 失效
标题翻译：聚（氧化烯）酰胺胺汽油添加剂
公开(公告)号：US06454818B1
公开(公告)日：2002-09-24
申请号：US09649031
申请日：2000-08-28
申请人： Jiang-Jen Lin , Wei-Shiun Ku , Che-Nan Lee , Yung-Sheng Ho , Kun-Hai Lin , Kuo-Min Wei
发明人： Jiang-Jen Lin , Wei-Shiun Ku , Che-Nan Lee , Yung-Sheng Ho , Kun-Hai Lin , Kuo-Min Wei
IPC分类号： C10L118
CPC分类号： C10L1/238 , C10L1/2383 , C10L10/04
摘要： The present invention is one kind of gasoline additives. The compounds consist of tertiary amine, amide and poly(oxybutylene) backbone in the same molecule. The process of making this type of products required an initiator containing primary amine and tertiary amine as the starting diamines. The primary amine will be converted into amide, while the tertiary amine remained intact. Then the amide is converted into butoxylates through butoxylation at CON—H position. The preparation therefore involved two steps: (1) amidation of diamines containing primary/tertiary amines with ethyl acetate to form amidoamines, and (2) butoxylation of this amidoamines to poly(oxybutylene)amidoamine. The product is gasoline soluble and can be used as additive having good performance of detergency and octane requirement reduction.
摘要翻译：本发明是一种汽油添加剂。该化合物由同一分子中的叔胺，酰胺和聚（氧丁烯）主链组成。制造这种类型的产物的方法需要含有伯胺和叔胺的引发剂作为起始的二胺。伯胺将转化为酰胺，而叔胺保持完整。然后通过在CON-H位置的丁氧基化将酰胺转化成丁酸盐。因此，该制剂涉及两个步骤：（1）使用乙酸乙酯将二胺与二乙胺进行酰胺化以形成酰氨基胺，和（2）将该酰氨基胺丁酰化成聚（氧丁烯）酰氨基胺。该产品是汽油可溶性的，可用作具有良好洗涤性能和辛烷值要求降低性能的添加剂。

4. 发明授权

US06458292B1 Composition of an anti-scale-forming agent 有权
标题翻译：防垢剂的组成
公开(公告)号：US06458292B1
公开(公告)日：2002-10-01
申请号：US09686937
申请日：2000-10-12
申请人： Jiang-Jen Lin , Jann-Chen Lin , Wen-Hen L{dot over (o)} , Wen-Shwong Hwang , Kun-Hai Lin
发明人： Jiang-Jen Lin , Jann-Chen Lin , Wen-Hen L{dot over (o)} , Wen-Shwong Hwang , Kun-Hai Lin
IPC分类号： C02F514
CPC分类号： C10G75/04 , C02F5/12 , C02F5/14 , C07F9/224 , Y10S585/95
摘要： A composition for an anti-scale-forming agent includes oil-based polyalkylenes, amines phosphorous and oxygen in a polymer for providing dispersivity and anti-oxidation and having the following formula: By integrating both characteristics into a single polymer, the anti-scale-forming agent in accordance with the present invention can be used as an anti-scale-forming agent for a manufacturing process in a petroleum refinery plant or the like chemistry factory. R1, R2 and x are defined herein.
摘要翻译：用于防垢剂的组合物包括用于提供分散性和抗氧化性的聚合物中的油基聚亚烷基，亚磷酸和氧，并具有以下结构式：通过将两种特性整合到单一聚合物中，根据本发明的成型剂可以用作炼油厂等化学工厂中的制造方法的防垢剂。 R1，R2和x在本文中定义。

5. 发明授权

US08952087B2 Method for reducing metal ion with nanosilicate platelets and dispersing metal nanoparticle and product thereof 有权
标题翻译：用纳米硅酸盐血小板还原金属离子并分散金属纳米粒子及其产物的方法
公开(公告)号：US08952087B2
公开(公告)日：2015-02-10
申请号：US12258402
申请日：2008-10-25
申请人： Jiang-Jen Lin , Yi-Lin Liao , Chien-Chia Chu , Chih-Wei Chiu
发明人： Jiang-Jen Lin , Yi-Lin Liao , Chien-Chia Chu , Chih-Wei Chiu
IPC分类号： C08K3/08 , B22F9/00 , B22F1/00 , B22F9/24 , B82Y30/00
CPC分类号： B22F9/24 , B22F1/0022 , B22F2999/00 , B82Y30/00 , B22F1/0059
摘要： The present invention provides a method for reducing metal ions (for example, silver ions) and stably dispersing metal nanoparticles by nanosilicate platelets. An organic dispersant, nanosilicate platelets and a metal ionic solution are mixed to perform a reductive reaction, wherein the organic dispersant is tri-sodium citrate dihydrate (SCD), chitosan or polyvinyl pyrrolidone (PVP), to produce a mixture of stably dispersed metal nanoparticles.
摘要翻译：本发明提供了还原金属离子（例如银离子）并通过纳米硅酸盐片稳定分散金属纳米粒子的方法。将有机分散剂，纳米硅酸盐片和金属离子溶液混合以进行还原反应，其中有机分散剂是柠檬酸三钠二水合物（SCD），壳聚糖或聚乙烯吡咯烷酮（PVP）），以产生稳定分散的金属纳米颗粒。

6. 发明申请

US20130172447A1 PHOSPHOROUS FLAME RETARDANT INCLUDING NSP 审中-公开
标题翻译：含磷阻燃剂，包括NSP
公开(公告)号：US20130172447A1
公开(公告)日：2013-07-04
申请号：US13561072
申请日：2012-07-29
申请人： Jiang-Jen Lin , Ying-Nan Chan , Jau-Yu Chiou
发明人： Jiang-Jen Lin , Ying-Nan Chan , Jau-Yu Chiou
IPC分类号： C09K21/12 , C08K3/36 , C08L63/02 , B82Y30/00
CPC分类号： C08K5/5399 , B82Y30/00 , C07F9/65815 , C08K9/04 , C08L63/00 , C09K21/12
摘要： A phosphorous flame retardant including nanosilicate platelets (NSP) is made by first reacting hexachlorotriphosphazene (HCP) with poly(oxyalkylene)amine, then mixing the HCP product with nano silicate platelets (NSP) to obtain the phosphorous flame retardant including NSP. The phosphorous flame retardant can be further applied to an epoxy resin as a curing agent.
摘要翻译：通过首先使六氯三磷腈（HCP）与聚（氧化烯）胺反应，然后将HCP产物与纳米硅酸盐血小板（NSP）混合以获得包括NSP的磷阻燃剂，制备包括纳米硅酸盐血小板（NSP）的磷阻燃剂。磷阻燃剂可以进一步用作环氧树脂作为固化剂。

7. 发明申请

US20130005918A1 METHOD FOR PRODUCING POLYMERIC POLYAMINES 审中-公开
标题翻译：生产聚合聚氨酯的方法
公开(公告)号：US20130005918A1
公开(公告)日：2013-01-03
申请号：US13612052
申请日：2012-09-12
申请人： Jiang-Jen Lin , Wei-Cheng Tsai , Yen-Chi Hsu , Wen-Hsin Chang
发明人： Jiang-Jen Lin , Wei-Cheng Tsai , Yen-Chi Hsu , Wen-Hsin Chang
IPC分类号： C07C231/02 , C08F8/32
CPC分类号： C08F26/00
摘要： Polymeric polyamine is produced by polymerizing polyoxyalkylene-amine and a linker. The polyoxyalkylene-amine has a structural formula H2N—R—NH2, wherein R is selected from the group consisting of dianhydride, diacid, epoxy, diisocyanate and poly(styrene-co-maleic anhydride) copolymers (SMA). The linker can be anhydride, carboxylic acid, epoxy, isocyanate or poly(styrene-co-maleic anhydride) copolymers (SMA). The polymeric polyamine so produced can be used as a stabilizer or dispersant of the Ag nanoparticles.
摘要翻译：聚合多胺通过聚合聚氧亚烷基 - 胺和接头来制备。聚氧化烯胺具有结构式H2N-R-NH2，其中R选自二酐，二酸，环氧，二异氰酸酯和聚（苯乙烯 - 共 - 马来酸酐）共聚物（SMA）。接头可以是酐，羧酸，环氧，异氰酸酯或聚（苯乙烯 - 共 - 马来酸酐）共聚物（SMA）。如此生产的聚合多胺可用作Ag纳米颗粒的稳定剂或分散剂。

8. 发明申请

US20120279352A1 METHOD FOR PREPARING SILVER NANOPARTICLES BY EMPLOYING ETHANOLAMINE AND POLY(STYRENE-CO-MALEIC ANHYDRIDE) COPOLYMERS 有权
标题翻译：通过使用乙醇胺和聚（苯乙烯 - 马来酸酐）共聚物制备银纳米粒子的方法
公开(公告)号：US20120279352A1
公开(公告)日：2012-11-08
申请号：US13549417
申请日：2012-07-14
申请人： Jiang-Jen Lin , Wei-Cheng Tsai , Chao-Po Hsu , Wei-Li Lin , Yueh-Hsien Wu
发明人： Jiang-Jen Lin , Wei-Cheng Tsai , Chao-Po Hsu , Wei-Li Lin , Yueh-Hsien Wu
IPC分类号： B22F9/16 , B82Y40/00
CPC分类号： B22F9/24 , B22F1/0018 , B82Y30/00 , Y10S977/896
摘要： The present invention provides a method for producing silver nanoparticles by employing ethanolamine. The method of this invention can be easily operated and no organic solvent is required. Ethanolamine first reacts with copolymers of poly(styrene-co-maleic anhydride) (abbreviated as SMA) to generate polymeric polymers. The polymeric polymers then reduce silver ions to silver atoms which are dispersed in the form of silver nanoparticles. Functional groups of the polymeric polymers can chelate with silver ions and be stably compatible with water or organic solvents, whereby the silver nanoparticles can be stably dispersed without aggregation and the produced silver nanoparticles.
摘要翻译：本发明提供使用乙醇胺制造银纳米粒子的方法。本发明的方法可以容易地操作，不需要有机溶剂。乙醇胺首先与聚（苯乙烯 - 共 - 马来酸酐）（缩写为SMA）的共聚物反应生成聚合物聚合物。聚合物聚合物然后将银离子还原成以银纳米颗粒形式分散的银原子。聚合物聚合物的官能团可以与银离子螯合并与水或有机溶剂稳定地相容，由此可以稳定地分散银纳米颗粒而不会聚集，并且所制备的银纳米颗粒。

9. 发明申请

US20120031846A1 METHOD FOR COLLECTING OIL WITH MODIFIED CLAY 有权
标题翻译：用改性粘土收集油的方法
公开(公告)号：US20120031846A1
公开(公告)日：2012-02-09
申请号：US13039335
申请日：2011-03-03
申请人： Jiang-Jen Lin , Ru-Siou Hsu
发明人： Jiang-Jen Lin , Ru-Siou Hsu
IPC分类号： B01D59/30
CPC分类号： C02F1/281 , B01D17/0202 , B01J20/10 , B01J20/12 , B01J20/3204 , B01J20/3272 , C02F1/285 , C02F1/288 , C02F1/681 , C02F2001/425 , C02F2101/32 , C10G25/003 , C10G33/04
摘要： The present invention provides a method for collecting oil with a modified clay. By mixing the modified clay and oil, the oil can be adsorbed to the clay. The modified clay is obtained by intercalating a hydrophobic polymer such as acidified poly(oxyalkylene)-amine into layered silicate clay, mica or talc to enlarge the interlayer space. The modified clay thus becomes hydrophobic and adsorption to the oil is promoted.
摘要翻译：本发明提供一种用改性粘土收集油的方法。通过混合改性粘土和油，油可以吸附到粘土上。改性粘土是通过将层状硅酸盐粘土，云母或滑石中的疏水性聚合物如酸化的聚（氧化烯） - 胺嵌入而获得的，以扩大层间空间。因此，改性粘土变得疏水，促进了对油的吸附。

10. 发明申请

US20100274036A1 ORGANIC/INORGANIC COMPOSITIVE DISPERSANT INCLUDING INORGANIC CLAY AND ORGANIC SURFACTANT 有权
标题翻译：有机/无机组合物分散剂，包括无机粘土和有机表面活性剂
公开(公告)号：US20100274036A1
公开(公告)日：2010-10-28
申请号：US12765853
申请日：2010-04-22
申请人： Jiang-Jen Lin , Wei-Ting Chen , Yen-Chi Hsu , Chih-Wei Chiu
发明人： Jiang-Jen Lin , Wei-Ting Chen , Yen-Chi Hsu , Chih-Wei Chiu
IPC分类号： C07F7/02
CPC分类号： C08K13/02 , B01F17/0007 , B01F17/0021 , B01F17/0042 , B01F17/0085
摘要： The present invention provides an organic/inorganic compositive dispersant and a method for producing the same. The compositive dispersant comprises a complex of inorganic clay and an organic surfactant. The compositive dispersant is produced by reacting inorganic clay with the organic surfactant in a solvent to generate a complex. The inorganic clay is layered or platelet. The organic surfactant is an anionic surfactant such as alkyl sulfates, a nonionic surfactant such as octylphenol polyethoxylate and polyoxyethylene alkyl ether, or a cationic surfactant such as fatty (C12˜C32) quaternary ammonium salts and fatty (C12˜C32) quaternary ammonium chlorides.
摘要翻译：本发明提供一种有机/无机复合分散剂及其制造方法。复合分散剂包括无机粘土和有机表面活性剂的复合物。复合分散剂通过无机粘土与有机表面活性剂在溶剂中反应生成复合物。无机粘土是分层的或血小板的。有机表面活性剂是阴离子表面活性剂，如烷基硫酸盐，非离子表面活性剂如辛基苯酚聚乙氧基化物和聚氧乙烯烷基醚，或阳离子表面活性剂如脂肪（C12〜C32）季铵盐和脂肪（C12〜C32）季铵氯化物。

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