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1. 发明授权

US07214439B2 Triborohydride salts as hydrogen storage materials and preparation thereof 失效
标题翻译：三氢硼酸盐作为储氢材料及其制备
公开(公告)号：US07214439B2
公开(公告)日：2007-05-08
申请号：US10741192
申请日：2003-12-19
申请人： Jeffrey V. Ortega , Michael T. Kelly , Jonathan L. Snover , Jason C. Brady , Ying Wu
发明人： Jeffrey V. Ortega , Michael T. Kelly , Jonathan L. Snover , Jason C. Brady , Ying Wu
IPC分类号： H01M8/06 , C01B3/06 , B01J7/00 , C01B6/19 , C01B6/21 , C10L1/12 , C08G79/08
CPC分类号： C01B3/065 , C01B6/21 , F17C11/005 , Y02E60/362
摘要： The present invention relates to the use of triborohydride salts as hydrogen storage materials. The present invention also relates to a system of using triborohydride salts to generate hydrogen gas for use in a fuel cell or other hydrogen-consuming device. A novel method of preparing triborohydride salts is also disclosed, wherein gaseous diborane is reacted with a carbonate suspended in a non-aqueous solvent in a suitable vessel with agitation. The process is typically carried out utilizing sodium carbonate to form sodium triborohydride. Other triborohydride salts can then be formed by cationic exchange. Hydrogen generating fuels according to the present invention include aqueous or hydroalcoholic solutions or slurries of a triborohydride salt, which may additionally contain a borohydride salt to provide operation over a broader temperature range.
摘要翻译：本发明涉及使用三氢化铈盐作为储氢材料。本发明还涉及一种使用三氢化烃盐产生用于燃料电池或其它耗氢装置的氢气的系统。还公开了一种制备三氢化硼盐的新方法，其中将气态乙硼烷与悬浮在非水溶剂中的碳酸酯在合适的容器中与搅拌反应。该方法通常使用碳酸钠进行以形成三氢化钠。然后可以通过阳离子交换形成其它三氯化硼盐。根据本发明的产生氢的燃料包括三氢化烃盐的水溶液或水醇溶液或浆料，其可以另外含有硼氢化物盐以在更宽的温度范围内提供操作。

2. 发明授权

US06586563B1 Processes for synthesizing alkali metal borohydride compounds 失效
标题翻译：碱金属硼氢化合物合成方法
公开(公告)号：US06586563B1
公开(公告)日：2003-07-01
申请号：US10022077
申请日：2001-12-18
申请人： Jeffrey V. Ortega , Ying Wu , Steven C. Amendola , Michael T. Kelly
发明人： Jeffrey V. Ortega , Ying Wu , Steven C. Amendola , Michael T. Kelly
IPC分类号： C08G7908
CPC分类号： C01B6/23 , C01B6/21
摘要： Processes for synthesizing borohydride compounds with reduced energy requirements and high efficiency are disclosed. The processes include the reaction of a base with a borane complex or diborane to produce a borohydride compound of formula YBH4, where Y is a monovalent cationic moiety.
摘要翻译：公开了具有降低的能量需求和高效率合成硼氢化合物的方法。该方法包括碱与硼烷络合物或乙硼烷的反应，生成式YBH4的硼氢化合物，其中Y是一价阳离子部分。

3. 发明申请

US20090090638A1 Processes and reactors for alkali metal production 审中-公开
标题翻译：碱金属生产工艺和反应堆
公开(公告)号：US20090090638A1
公开(公告)日：2009-04-09
申请号：US11905924
申请日：2007-10-05
申请人： Michael T. Kelly , Oscar A. Moreno , Jeffrey V. Ortega , Ying Wu
发明人： Michael T. Kelly , Oscar A. Moreno , Jeffrey V. Ortega , Ying Wu
IPC分类号： C25C3/02
CPC分类号： C25C3/02 , C01B6/21 , C25B1/14 , C25B9/08 , C25C1/02
摘要： Electrochemical processes and apparatus for obtaining metals from metal salts, including for separating alkali metal and alcohols from alkali metal alkoxide compounds, are disclosed. Aqueous solutions of metal alkoxides or metal carbonates are converted to metals by electrochemical processes which may also be integrated into processes for the production of borohydrides, such as sodium borohydride.
摘要翻译：公开了用于从金属盐获得金属的电化学方法和装置，包括用于从碱金属醇盐化合物中分离碱金属和醇。金属醇盐或金属碳酸盐的水溶液通过电化学方法转化为金属，其也可以被整合到生产硼氢化钠如硼氢化钠的方法中。

4. 发明授权

US06670444B2 Processes for synthesizing borohydride compounds 失效
标题翻译：合成硼氢化合物的方法
公开(公告)号：US06670444B2
公开(公告)日：2003-12-30
申请号：US10331674
申请日：2002-12-27
申请人： Steven C. Amendola , Michael T. Kelly , Jeffrey V. Ortega , Ying Wu
发明人： Steven C. Amendola , Michael T. Kelly , Jeffrey V. Ortega , Ying Wu
IPC分类号： C08G7908
CPC分类号： C01B6/21 , C01B3/34 , C01B6/13 , C01B6/19 , C01B2203/0227 , C01B2203/0283 , F17C11/005 , Y02P20/582
摘要： The present invention relates to processes for producing borohydride compounds. In particular, the present invention provides efficient processes and compositions for the large-scale production of borohydride compounds of the formula YBH4 by the reaction of a boron-containing compound represented by the formula BX3 with hydrogen or an aldehyde to obtain diborane and HX, and reacting the diborane with a Y-containing base selected from those represented by the formula Y2O, YOH and Y2CO3 to obtain YBH4 and YBO2. Y is selected from the group consisting of the alkali metals, pseudo-alkali metals, alkaline earth metals, an ammonium ion, and quaternary amines of the formula NR4+, wherein each R is independently selected from hydrogen and a straight- or branched-chain C1-4 alkyl group, and X is selected from the group consisting of halide ions, —OH, —R′ and —OR′ groups, chalcogens, and chalcogenides, wherein R′ is a straight- or branched-chain C1-4 alkyl group.
摘要翻译：本发明涉及生产硼氢化合物的方法。特别地，本发明提供了通过式BX3表示的含硼化合物与氢或醛反应而大规模生产式YBH4的硼氢化合物的有效方法和组合物，以获得乙硼烷和HX，以及使乙硼烷与选自由式Y 2 O，YOH和Y 2 CO 3表示的Y含量碱反应，得到YBH 4和YBO 2。 Y选自碱金属，假碱金属，碱土金属，铵离子和式NR4 +的季胺，其中每个R独立地选自氢和直链或支链的 - 链C 1-4烷基，X选自卤离子，-OH，-R'和-OR'基，硫属元素和硫族化物，其中R'是直链或支链C1- 4烷基。

5. 发明申请

US20120328478A1 COMPOSITIONS, DEVICES AND METHODS FOR HYDROGEN GENERATION 有权
公开(公告)号：US20120328478A1
公开(公告)日：2012-12-27
申请号：US13570859
申请日：2012-08-09
申请人： Michael T. Kelly , Jeffrey V. Ortega , Richard M. Mohring
发明人： Michael T. Kelly , Jeffrey V. Ortega , Richard M. Mohring
IPC分类号： B01J19/00
CPC分类号： C01B3/26 , C01B3/02 , C01B3/065 , C01B3/24 , C01B2203/0838 , Y02E60/362
摘要： Methods and systems for hydrogen generation from solid hydrogen storage compositions which generate hydrogen in an exothermic reaction wherein the heat released can be absorbed by solid endothermic compositions are disclosed. The solid hydrogen storage compositions comprise mixtures of chemical hydrides and water surrogate compounds. Fuel cartridges suitable for use with compositions which generate hydrogen upon the application of thermal initiation and methods for operating the fuel cartridges are also disclosed.

6. 发明申请

US20090017348A1 Techniques for packaging and utilizing solid hydrogen-producing fuel 失效
标题翻译：包装和利用固体产氢燃料的技术
公开(公告)号：US20090017348A1
公开(公告)日：2009-01-15
申请号：US12078034
申请日：2008-03-26
申请人： Michael T. Kelly , Jeffrey V. Ortega
发明人： Michael T. Kelly , Jeffrey V. Ortega
IPC分类号： H01M8/18 , H01M8/00
CPC分类号： H01M8/0606 , C01B3/065 , C01B3/503 , C01B2203/0405 , C01B2203/047 , C01B2203/0475 , C01B2203/048 , H01M8/04014 , H01M8/04089 , H01M8/04208 , H01M8/04216 , H01M8/0612 , H01M8/065 , Y02E60/362 , Y10T29/49108 , Y10T29/49808
摘要： Techniques for packaging and utilizing solid hydrogen-producing fuel are described herein. The fuel may be in the form of a bonded/compressed powder, granules, or pellets. The fuel is packaged in cartridges having hydrogen-permeable enclosures. In operation, the fuel undergoes a hydrogen-releasing Thermally Initiated Hydrolysis (TIH) reaction. A cartridge may comprise one or more fuel chambers, and several cartridges may be assembled together.
摘要翻译：本文描述了用于包装和利用固体产氢燃料的技术。燃料可以是粘合/压缩粉末，颗粒或丸粒的形式。燃料包装在具有氢气可渗透外壳的盒中。在操作中，燃料经历氢释放热起始水解（TIH）反应。墨盒可以包括一个或多个燃料室，并且几个墨盒可以组装在一起。

7. 发明授权

US09061910B2 Compositions, devices and methods for hydrogen generation 有权
公开(公告)号：US09061910B2
公开(公告)日：2015-06-23
申请号：US13570891
申请日：2012-08-09
申请人： Michael T. Kelly , Jeffrey V. Ortega , Richard M. Mohring
发明人： Michael T. Kelly , Jeffrey V. Ortega , Richard M. Mohring
IPC分类号： B01J7/00 , C01B3/26 , C01B3/02 , C01B3/06 , C01B3/24
CPC分类号： C01B3/26 , C01B3/02 , C01B3/065 , C01B3/24 , C01B2203/0838 , Y02E60/362
摘要： Methods and systems for hydrogen generation from solid hydrogen storage compositions which generate hydrogen in an exothermic reaction wherein the heat released can be absorbed by solid endothermic compositions are disclosed. The solid hydrogen storage compositions comprise mixtures of chemical hydrides and water surrogate compounds. Fuel cartridges suitable for use with compositions which generate hydrogen upon the application of thermal initiation and methods for operating the fuel cartridges are also disclosed.

8. 发明授权

US08586261B2 Techniques for packaging and utilizing solid hydrogen-producing fuel 失效
公开(公告)号：US08586261B2
公开(公告)日：2013-11-19
申请号：US12078034
申请日：2008-03-26
申请人： Michael T. Kelly , Jeffrey V. Ortega
发明人： Michael T. Kelly , Jeffrey V. Ortega
IPC分类号： H01M8/00 , H01M8/06 , H01M8/22 , C10L5/00 , B23P17/00 , B65D21/02
CPC分类号： H01M8/0606 , C01B3/065 , C01B3/503 , C01B2203/0405 , C01B2203/047 , C01B2203/0475 , C01B2203/048 , H01M8/04014 , H01M8/04089 , H01M8/04208 , H01M8/04216 , H01M8/0612 , H01M8/065 , Y02E60/362 , Y10T29/49108 , Y10T29/49808
摘要： Techniques for packaging and utilizing solid hydrogen-producing fuel are described herein. The fuel may be in the form of a bonded/compressed powder, granules, or pellets. The fuel is packaged in cartridges having hydrogen-permeable enclosures. In operation, the fuel undergoes a hydrogen-releasing Thermally Initiated Hydrolysis (TIH) reaction. A cartridge may comprise one or more fuel chambers, and several cartridges may be assembled together.

9. 发明授权

US08268028B2 Compositions, devices and methods for hydrogen generation 有权
标题翻译：用于氢气生成的组合物，装置和方法
公开(公告)号：US08268028B2
公开(公告)日：2012-09-18
申请号：US11892515
申请日：2007-08-23
申请人： Michael T. Kelly , Jeffrey V. Ortega , Richard M. Mohring
发明人： Michael T. Kelly , Jeffrey V. Ortega , Richard M. Mohring
IPC分类号： B01J8/04
CPC分类号： C01B3/26 , C01B3/02 , C01B3/065 , C01B3/24 , C01B2203/0838 , Y02E60/362
摘要： Methods and systems for hydrogen generation from solid hydrogen storage compositions which generate hydrogen in an exothermic reaction wherein the heat released can be absorbed by solid endothermic compositions are disclosed. The solid hydrogen storage compositions comprise mixtures of chemical hydrides and water surrogate compounds. Fuel cartridges suitable for use with compositions which generate hydrogen upon the application of thermal initiation and methods for operating the fuel cartridges are also disclosed.
摘要翻译：公开了在放热反应中产生氢的固体储氢组合物产生氢气的方法和系统，其中释放的热量可被固体吸热组合物吸收。固体储氢组合物包含化学氢化物和水替代化合物的混合物。还公开了适用于在施加热起始时产生氢气的组合物的燃料盒和用于操作燃料盒的方法。

10. 发明申请

US20110076228A1 COMPOSITIONS, DEVICES AND METHODS FOR HYDROGEN GENERATION 审中-公开
标题翻译：用于氢生成的组合物，装置和方法
公开(公告)号：US20110076228A1
公开(公告)日：2011-03-31
申请号：US12959090
申请日：2010-12-02
申请人： Michael T. Kelly , Jeffrey V. Ortega
发明人： Michael T. Kelly , Jeffrey V. Ortega
IPC分类号： C01B3/04 , C01B3/02
CPC分类号： C01B3/065 , C01B3/02 , C10L5/40 , Y02E50/30 , Y02E60/362
摘要： Hydrogen storage fuel compositions and devices comprising a mixture of at least one chemical hydride compound and at least one proton source, and methods for thermally initiated hydrogen generation from fuel compositions are disclosed. The fuel compositions comprise an excess of hydridic hydrogens relative to protic hydrogens. Fuel cartridges suitable for use with compositions which generate hydrogen upon the application of thermal initiation and methods for operating the fuel cartridges are also disclosed.
摘要翻译：公开了包含至少一种化学氢化物化合物和至少一种质子源的混合物的储氢燃料组合物和装置，以及用于从燃料组合物产生热引发氢的方法。燃料组合物相对于质子氢包含过量的氢化氢。还公开了适用于在施加热起始时产生氢气的组合物的燃料盒和用于操作燃料盒的方法。

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