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1. 发明授权

US09260403B2 Methods for preparing 2,5-furandicarboxylic acid 有权
标题翻译：制备2,5-呋喃二羧酸的方法
公开(公告)号：US09260403B2
公开(公告)日：2016-02-16
申请号：US14229388
申请日：2014-03-28
申请人： Yasuo Yoshikuni , Susan R. Cooper , Adam J. Wargacki , Leo E. Manzer , James F. White , Lou Kapicak , Dennis J. Miller , Lars Peereboom
发明人： Yasuo Yoshikuni , Susan R. Cooper , Adam J. Wargacki , Leo E. Manzer , James F. White , Lou Kapicak , Dennis J. Miller , Lars Peereboom
IPC分类号： C07D307/68
CPC分类号： C07D307/68
摘要： Provided are methods of producing 2,5-furandicarboxylic acid (FDCA) from renewable sources such as seaweed, alginate, oligoalginate, pectin, oligopectin, polygalacturonate, galacturonate, and/or oligogalacturonate. The sugars in the renewable sources can be converted into one or more intermediates such as 4-deoxy-L-erythro-5-hexoseulose uronate (DEHU), 4-deoxy-L-threo-5-hexosulose uronate (DTHU), 5-hydroxymethyl furfural (HMF), 2,5-dihydroxymethyl furan (DHMF), and 5-formyl-2-furancarboxylic acid (FFA), which can be converted into FDCA by dehydration and cyclization to produce 5-formyl-2-furancarboxylic acid (FFA), followed by oxidation to produce FDCA. DEHU or DTHU may also be converted into FDCA by oxidation to produce 2,3-dihydroxy-5-oxohexanedioic acid (DOHA), which then undergoes dehydration and cyclization to produce FDCA.
摘要翻译：提供从可再生来源例如海藻，藻酸盐，低聚海藻酸盐，果胶，寡聚糖蛋白，聚半乳糖醛酸盐，半乳糖醛酸盐和/或寡聚半乳糖醛酸盐生产2,5-呋喃二羧酸（FDCA）的方法。可再生资源中的糖可以转化为一种或多种中间体，例如4-脱氧-L-赤式5-己糖糖酸糖（DEHU），4-脱氧-L-苏糖-5-己糖糖酸糖（DTHU），5- 羟基甲基糠醛（HMF），2,5-二羟甲基呋喃（DHMF）和5-甲酰基-2-呋喃甲酸（FFA），其可以通过脱水和环化转化成FDCA以产生5-甲酰基-2-呋喃甲酸（ FFA），然后氧化生成FDCA。 DEHU或DTHU也可以通过氧化转化成FDCA，生成2,3-二羟基-5-氧代己二酸（DOHA），然后进行脱水和环化以产生FDCA。

2. 发明授权

US07872158B2 Chemical production processes, systems, and catalyst compositions 有权
标题翻译：化学生产过程，系统和催化剂组合物
公开(公告)号：US07872158B2
公开(公告)日：2011-01-18
申请号：US11895414
申请日：2007-08-24
申请人： Thomas H. Peterson , Alan H. Zacher , Michel J. Gray , James F. White , Todd A. Werpy
发明人： Thomas H. Peterson , Alan H. Zacher , Michel J. Gray , James F. White , Todd A. Werpy
IPC分类号： C07C45/51 , C07C45/52
CPC分类号： B01J27/186 , B01J8/025 , B01J23/96 , B01J27/1856 , B01J27/285 , B01J37/03 , B01J38/12 , B01J2208/00212 , B01J2208/00256 , B01J2219/00247 , C07C45/52 , Y02P20/584 , C07C47/22 , C07C49/17
摘要： Chemical production processes are provided that can include exposing a reactant composition to a catalyst composition to form a product composition. The reactant composition can include a multihydric alcohol compound and the product composition can include a carbonyl compound. The catalyst composition can include a metal effective to facilitate catalyst activation. Processes disclosed also include supplementing a dehydration catalyst with a promoter, and activating the supplemented catalyst in the presence of oxygen. Processes also include providing a supplemented dehydration catalyst to within a reactor, and exposing a multihydric alcohol compound to the dehydration catalyst, with the exposing forming coke within the reactor. Oxygen can be provided to the reactor to remove at least a portion of the coke.
摘要翻译：提供化学生产方法，其可以包括将反应物组合物暴露于催化剂组合物以形成产物组合物。反应物组合物可以包括多元醇化合物，并且产物组合物可以包括羰基化合物。催化剂组合物可以包括有效促进催化剂活化的金属。所公开的方法还包括用助催化剂补充脱水催化剂，并在氧的存在下活化补充的催化剂。方法还包括向反应器内部提供补充的脱水催化剂，并将多元醇化合物暴露于脱水催化剂中，同时在反应器内形成曝光的焦炭。可以将氧气提供给反应器以除去至少一部分焦炭。

3. 发明申请

US20100256187A1 COMPOSITION OF 2,4,6- TRIFLUORO-N-[6-(1-METHYL-PIPERIDIN-4-CARBONYL)-PYRIDIN-2-YL]-BENZAMIDE 审中-公开
标题翻译： 2,4,6-三氟-N- [6-（1-甲基 - 哌啶-4-羰基） - 吡啶-2-基] - 苯甲酰胺的组合物
公开(公告)号：US20100256187A1
公开(公告)日：2010-10-07
申请号：US12753489
申请日：2010-04-02
申请人： Alison Pilgrim , James F. White , Nadia M.J. Rupniak
发明人： Alison Pilgrim , James F. White , Nadia M.J. Rupniak
IPC分类号： A61K31/4545 , A61P25/06
CPC分类号： A61K31/4545
摘要： The present invention relates to discloses a pharmaceutical composition of 2,4,6-trifluoro-N-[6-(1-methyl-piperidin-4-ylcarbonyl)-pyridin-2-yl]-benzamide and a pharmaceutically acceptable carrier.
摘要翻译：本发明涉及2,4,6-三氟-N- [6-（1-甲基 - 哌啶-4-基羰基） - 吡啶-2-基] - 苯甲酰胺和药学上可接受的载体的药物组合物。

4. 发明授权

US07700788B2 Hydroxymethyl furfural oxidation methods 有权
标题翻译：羟甲基糠醛氧化法
公开(公告)号：US07700788B2
公开(公告)日：2010-04-20
申请号：US11932436
申请日：2007-10-31
申请人： Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
发明人： Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
IPC分类号： C07D307/44
CPC分类号： C07D307/48 , C07D307/44
摘要： A method of oxidizing hydroxymethylfurfural (HMF) includes providing a starting material which includes HMF in a solvent comprising water into a reactor. At least one of air and O2 is provided into the reactor. The starting material is contacted with the catalyst comprising Pt on a support material where the contacting is conducted at a reactor temperature of from about 50° C. to about 200° C. A method of producing an oxidation catalyst where ZrO2 is provided and is calcined. The ZrO2 is mixed with platinum (II) acetylacetonate to form a mixture. The mixture is subjected to rotary evaporation to form a product. The product is calcined and reduced under hydrogen to form an activated product. The activated product is passivated under a flow of 2% O2.
摘要翻译：氧化羟甲基糠醛（HMF）的方法包括在包含水的溶剂中将包含HMF的原料提供到反应器中。将空气和O2中的至少一个提供到反应器中。起始材料与包含Pt的催化剂在载体材料上接触，其中接触在约50℃至约200℃的反应器温度下进行。制备其中提供ZrO 2并被煅烧的氧化催化剂的方法。将ZrO 2与乙酰丙酮化铂（II）混合以形成混合物。将混合物进行旋转蒸发以形成产物。将产物在氢气下煅烧和还原以形成活化产物。活化产物在2％O 2的流量下钝化。

5. 发明授权

US07674916B2 Process for producing cyclic compounds 有权
标题翻译：环状化合物的制备方法
公开(公告)号：US07674916B2
公开(公告)日：2010-03-09
申请号：US11688022
申请日：2007-03-19
申请人： Todd A. Werpy , John G. Frey, Jr. , James F. White , Johnathan E. Holladay , Alan H. Zacher
发明人： Todd A. Werpy , John G. Frey, Jr. , James F. White , Johnathan E. Holladay , Alan H. Zacher
IPC分类号： C07D207/267 , C07D213/63
CPC分类号： C07D207/404
摘要： The invention includes methods of processing an initial di-carbonyl compound by conversion to a cyclic compound. The cyclic compound is reacted with an alkylating agent to form a derivative having an alkylated ring nitrogen. The invention encompasses a method of producing an N-alkyl product. Ammonia content of a solution is adjusted to produce a ratio of ammonia to di-carboxylate compound of from about 1:1 to about 1.5:1. An alkylating agent is added and the initial compound is alkylated and cyclized. The invention includes methods of making N-methyl pyrrolidinone (NMP). Aqueous ammonia and succinate is introduced into a vessel and ammonia is adjusted to provide a ratio of ammonia to succinate of less than 2:1. A methylating agent is reacted with succinate at a temperature of from greater than 100° C. to about 400° C. to produce N-methyl succinimide which is purified and hydrogenated to form NMP.
摘要翻译：本发明包括通过转化为环状化合物来处理初始二羰基化合物的方法。环状化合物与烷基化剂反应形成具有烷基化环氮的衍生物。本发明包括生产N-烷基产物的方法。调节溶液的氨含量以产生约1：1至约1.5：1的氨与二羧酸酯化合物的比例。加入烷基化剂并将该初始化合物烷基化并环化。本发明包括制备N-甲基吡咯烷酮（NMP）的方法。将氨水和琥珀酸钠引入容器中，并调节氨以提供小于2:1的氨与琥珀酸的比例。甲基化剂与琥珀酸酯在大于100℃至约400℃的温度下反应，生成N-甲基琥珀酰亚胺，将其纯化并氢化形成NMP。

6. 发明授权

US5969340A Seed counting apparatus for a planter monitor 失效
标题翻译：播种机监视器种子计数装置
公开(公告)号：US5969340A
公开(公告)日：1999-10-19
申请号：US907495
申请日：1997-08-08
申请人： Rasvan N. Dragne , James F. White , Nikolai Tevs
发明人： Rasvan N. Dragne , James F. White , Nikolai Tevs
IPC分类号： A01C7/08 , A01C7/10 , G06M1/10 , G06M1/272 , G06M11/00 , H01J40/14
CPC分类号： A01C7/105 , G06M1/101 , G06M11/00
摘要： A seed counter for counting seeds flowing through a duct includes a light transmitter on one side of the duct and light receiver on the opposed side of the duct together with an electronic circuit effecting analysis of the signals received by the receiver to generate a seed count value which represents accurately as possible the number of seeds passing through the duct. The transmitter and receiver each comprise a channel-shaped body with diodes at a base of the channel with the channel filled with a translucent potting material facing into the duct. The circuit receives the signals which include for each passage of a seed or a clump of seeds a temporary reduction in light intensity which is converted to a reduction in voltage. Prior to start up the steady state voltage is measured and the current to the transmitter varied to provide a predetermined level of signal at the receiver. The circuit includes a DC compression circuit and a AC compression circuit at an amplifier so as to provide an output signal in a required amplitude range. An autobiasing section maintains a steady state signal at a required level. The amplitude of the signal is compared to a threshold by generating a first signal which is offset by the threshold and a second signal which is delayed by a predetermined time period, the comparison generating a square wave output when one of the signals crosses the other signal. The seed counter is used in a monitoring system having a central monitor which can be operated to vary the parameters of the comparison circuit including the time delay. The use of the comparison circuit assists in determining the difference between a single seed and a clump of seeds passing the transmitter/receiver simultaneously.
摘要翻译：用于计数流过管道的种子的种子计数器包括在管道的一侧上的光发射器和在管道的相对侧上的光接收器以及电子电路，其实现由接收器接收的信号的分析以产生种子计数值其尽可能准确地代表穿过管道的种子的数量。发射器和接收器各自包括在通道的基部处具有二极管的通道形体，其中通道填充有面向管道的半透明灌封材料。该电路接收包括种子或种子簇的每次通过的信号，其中光强度的临时降低被转换为电压的降低。在启动之前，测量稳态电压并且到发射机的电流变化以在接收器处提供预定水平的信号。该电路在放大器中包括DC压缩电路和AC压缩电路，以便提供所需幅度范围内的输出信号。自动偏置部分将稳态信号保持在所需的水平。通过产生被阈值偏移的第一信号和延迟预定时间段的第二信号将信号的幅度与阈值进行比较，该比较当其中一个信号与另一信号相交时产生方波输出。种子计数器用于具有中央监视器的监视系统，其可以被操作以改变包括时间延迟的比较电路的参数。比较电路的使用有助于确定单个种子和同时通过发射机/接收机的种子团簇之间的差异。

7. 发明授权

US5469981A Electrically blowable fuse structure manufacturing for organic insulators 失效
标题翻译：有机绝缘子可电熔熔丝结构制造
公开(公告)号：US5469981A
公开(公告)日：1995-11-28
申请号：US323196
申请日：1994-10-14
申请人： Kris V. Srikrishnan , James F. White , Jer-Ming Yang
发明人： Kris V. Srikrishnan , James F. White , Jer-Ming Yang
IPC分类号： H01L23/525 , H01L23/538 , H05K1/02 , H01B13/00
CPC分类号： H01L23/5256 , H01L23/5382 , H01L2924/0002 , H05K1/0263
摘要： An electrically blowable fuse structure usable with organic insulators in microelectronic parts is provided. The fuse structure is made of a first heat resistant member, a fusing element and a second heat resistant member. The heat resistant members are in substantial contact with the fuse and thermally insulate the fuse from the organic insulator. The ends of each fuse are electrically connected to a pair conductors.A process for fabricating an electrically blowable fuse structure usable with an organic insulator is provided. A substrate with an organic insulator coating and containing electrically conductive features with exposed contacts is provided. A heat shield layer and a fuse layer are deposited sequentially and patterned by subtractive etching. Plurality of conductors are formed over so as to electrically connect each fuse element to a pair of conductors. A second heat resistant member is formed over the fuse area and the substrate is subsequently quoted with an organic insulator.
摘要翻译：提供了可用于微电子部件中的有机绝缘体的可电熔熔融结构。熔丝结构由第一耐热构件，定影元件和第二耐热构件制成。耐热构件与保险丝基本接触，并将保险丝与有机绝缘体热绝缘。每个保险丝的端部电连接到一对导体。提供了一种用于制造可用于有机绝缘体的电可熔融熔丝结构的工艺。提供了具有有机绝缘体涂层并且包含具有暴露触点的导电特征的衬底。依次沉积热屏蔽层和熔丝层，并通过减去蚀刻图案化。形成多个导体以便将每个熔丝元件电连接到一对导体。在保险丝区域上形成第二耐热构件，随后用有机绝缘体引用衬底。

8. 发明授权

US5347046A Catalyst and process for using same for the preparation of unsaturated carboxylic acid esters 失效
标题翻译：用于制备不饱和羧酸酯的催化剂和方法
公开(公告)号：US5347046A
公开(公告)日：1994-09-13
申请号：US67445
申请日：1993-05-25
申请人： James F. White , Barbara Slawski , Geoffrey White
发明人： James F. White , Barbara Slawski , Geoffrey White
IPC分类号： B01J23/52 , B01J23/62 , B01J23/656 , B01J23/89 , B01J37/02 , C07B61/00 , C07C67/05 , C07C67/055 , C07C69/15 , C07C69/24 , C07C69/76 , B01J23/58 , B01J31/00
CPC分类号： C07C67/055 , B01J23/52 , B01J23/89 , B01J23/8926 , B01J37/0207
摘要： Disclosed are catalyst compositions comprising (i) one or more palladium group metals and/or compounds thereof; (ii) gold and/or compounds thereof; and (iii) optionally, an effective amount of one or more promoters selected from the group consisting of copper, nickel, cobalt, iron, manganese, lead, silver and compounds thereof. Preferably these catalyst compositions contain one or more promoters wherein the gram ratio of metal in the promoter to palladium group metal is up to about 0.4, wherein the catalysts are deposited on a support material and said support material is treated with one or more alkali metal bases and one or more alkali metal silicates prior to said deposition.Also described are processes for preparing ethylenically unsaturated esters comprising reacting in the vapor phase at least one olefinic compound with at least one carboxylic organic acid and molecular oxygen in the presence of an effective amount of the foregoing catalyst compositions.
摘要翻译：公开了包含（i）一种或多种钯族金属和/或其化合物的催化剂组合物; （ii）金和/或其化合物; 和（iii）任选的有效量的一种或多种选自铜，镍，钴，铁，锰，铅，银及其化合物的助催化剂。优选地，这些催化剂组合物含有一种或多种促进剂，其中促进剂与钯族金属中金属的克比高达约0.4，其中催化剂沉积在载体材料上，所述载体材料用一种或多种碱金属碱和一种或多种碱金属硅酸盐。还描述了制备烯键式不饱和酯的方法，包括在有效量的上述催化剂组合物存在下，在汽相中使至少一种烯属化合物与至少一种羧酸有机酸和分子氧反应。

9. 发明授权

US4113768A Preparation of acrylic or methacrylic acid from acrolein or methacrolein 失效
标题翻译：从丙烯醛或甲基丙烯醛制备丙烯酸或甲基丙烯酸
公开(公告)号：US4113768A
公开(公告)日：1978-09-12
申请号：US748081
申请日：1976-12-06
申请人： James F. White , Michael D. Applequist
发明人： James F. White , Michael D. Applequist
IPC分类号： B01J23/88 , B01J23/89 , B01J27/057 , B01J27/192 , C07C51/25 , C07C57/055 , C07C51/32
CPC分类号： B01J23/8876 , B01J23/8878 , B01J23/8993 , B01J27/0576 , B01J27/192 , C07C51/252 , B01J2523/00
摘要： Methacrylic acid or acrylic acid are produced by the oxidation of methacrolein or acrolein, respectively, with molecular oxygen in the vapor phase in the presence of a catalytic oxide of molybdenum, phosphorus, bismuth, copper, oxygen, optionally a halogen selected from the group consisting of chlorine, bromine or iodine, and optionally, at least one element selected from the group consisting of Fe, Cr, Ni, Mn, Sb, Te, Rh, and Pd.
摘要翻译：在钼，磷，铋，铜，氧，任选地选自以下的卤素的催化氧化物的存在下，分别用气相中的分子氧氧化异丁烯醛或丙烯醛来生产甲基丙烯酸或丙烯酸：的氯，溴或碘，以及任选的至少一种选自Fe，Cr，Ni，Mn，Sb，Te，Rh和Pd的元素。

10. 发明授权

US08501963B2 Process for producing cyclic compounds 有权
标题翻译：环状化合物的制备方法
公开(公告)号：US08501963B2
公开(公告)日：2013-08-06
申请号：US13175601
申请日：2011-07-01
申请人： Todd A. Werpy , John G. Frye, Jr. , James F. White , Johnathan E. Holladay , Alan H. Zacher
发明人： Todd A. Werpy , John G. Frye, Jr. , James F. White , Johnathan E. Holladay , Alan H. Zacher
IPC分类号： C07D207/267
CPC分类号： C07D207/404
摘要： The invention includes methods of processing an initial di-carbonyl compound by conversion to a cyclic compound. The cyclic compound is reacted with an alkylating agent to form a derivative having an alkylated ring nitrogen. The invention encompasses a method of producing an N-alkyl product. Ammonia content of a solution is adjusted to produce a ratio of ammonia to di-carboxylate compound of from about 1:1 to about 1.5:1. An alkylating agent is added and the initial compound is alkylated and cyclized. The invention includes methods of making N-methyl pyrrolidinone (NMP). Aqueous ammonia and succinate is introduced into a vessel and ammonia is adjusted to provide a ratio of ammonia to succinate of less than 2:1. A methylating agent is reacted with succinate at a temperature of from greater than 100° C. to about 400° C. to produce N-methyl succinimide which is purified and hydrogenated to form NMP.
摘要翻译：本发明包括通过转化为环状化合物来处理初始二羰基化合物的方法。环状化合物与烷基化剂反应形成具有烷基化环氮的衍生物。本发明包括生产N-烷基产物的方法。调节溶液的氨含量以产生约1：1至约1.5：1的氨与二羧酸酯化合物的比例。加入烷基化剂并将该初始化合物烷基化并环化。本发明包括制备N-甲基吡咯烷酮（NMP）的方法。将氨水和琥珀酸钠引入容器中，并调节氨以提供小于2:1的氨与琥珀酸的比例。甲基化剂与琥珀酸酯在大于100℃至约400℃的温度下反应，生成N-甲基琥珀酰亚胺，将其纯化并氢化形成NMP。

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