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    • 4. 发明授权
    • Method for producing a metal nanoparticle colloid
    • 金属纳米粒子胶体的制造方法
    • US09017578B2
    • 2015-04-28
    • US13700793
    • 2011-05-31
    • Isao Nakatani
    • Isao Nakatani
    • H01B1/22B01F17/00B01J13/00B22F1/02B22F1/00B82Y30/00
    • B01F17/0042B01J13/0043B22F1/0022B22F1/02B82Y30/00
    • The problems can be solved by using a method for producing a metal nanoparticle colloid, which comprises the steps of S1: mixing, into a nonpolar hydrocarbon oil having a vapor pressure of 10−3 Torr or less at room temperature, organic molecules having both a hydrophilic group and a lipophilic group and having in the end of the hydrophilic group an N, S, P, or O atom or having at the hydrophilic group a functional group of an NH2 group, an NH group, an SH group, a PO group, or an OH group to prepare a base liquid, and S2: placing the base liquid in a rotatable vacuum drum and charging a non-magnetic metal material in a crucible provided in the vacuum drum, and depositing the vapor of the non-magnetic metal material on the base liquid which adheres to the inner wall of the vacuum drum and rotates together with the rotating drum under conditions such that the inside of the vacuum drum is under a reduced pressure and the vacuum drum is rotated, and a task of the present invention is to provide a method for producing a metal nanoparticle colloid having non-magnetic metal nanoparticles having various shapes.
    • 通过使用金属纳米粒子胶体的制造方法可以解决上述问题,该方法包括以下步骤:S1在室温下混合成蒸气压为10-3乇或更低的非极性烃油, 亲水基团和亲油基团,并且在亲水基团末端具有N,S,P或O原子或在亲水基团具有NH 2基团,NH基团,SH基团,PO基团的官能团 或OH基以制备基础液体,S2:将基础液体放置在可旋转的真空鼓中,并将非磁性金属材料装入设置在真空鼓中的坩埚中,并沉积非磁性金属的蒸汽 在基本液体上附着在真空鼓的内壁上并与旋转滚筒一起旋转的基底液体的材料在真空鼓的内部处于减压下并且真空鼓旋转的条件下,并且本发明的任务 发明是 提供具有各种形状的非磁性金属纳米粒子的金属纳米粒子胶体的制造方法。
    • 6. 发明申请
    • Method for Producing Alloy Fine Particle Colloid
    • 生产合金微粒胶体的方法
    • US20090151512A1
    • 2009-06-18
    • US12226620
    • 2007-04-25
    • Isao Nakatani
    • Isao Nakatani
    • B22F9/04
    • C22C5/06B22F9/12B22F2999/00C22C5/02C22C5/04C22C9/02C22C9/10C22C19/03C22C19/052C22C19/07C22C30/00C22C30/02C22C38/02C22C38/10B22F2201/20
    • A method for producing an alloy fine particle colloid by heating and evaporating a raw material binary alloy which is in a solid state in an ambient temperature and pressure environment in a reduced-pressure environment, cooling a generated vapor for condensation and solidification and collecting a formed alloy fine particle in a liquid medium, wherein (1) when an atomic fraction of a component element in the raw material alloy is defined as X, a component ratio of each of the elements of the raw material alloy is regulated such that a fraction of a vapor pressure of the component element to the total vapor pressure of the raw material alloy falls within the range of from (X−0.1) to (X+0.1); and (2) the raw material binary alloy is an alloy species which forms a homogeneous alloy phase in an alloy ingot. Thus, an alloy fine particle colloid is rationally and efficiently produced.
    • 通过在环境温度和压力环境中在减压环境中加热和蒸发固体状态的原料二元合金来制造合金微粒胶体的方法,冷却产生的蒸气进行冷凝和凝固并收集形成 合金细颗粒在液体介质中,其中(1)当原料合金中的成分元素的原子分数定义为X时,原料合金的各元素的成分比例被调节为 成分元素的蒸汽压与原料合金的总蒸气压成
      比在(X-0.1)〜(X + 0.1)的范围内。 (2)原料二元合金是在合金锭中形成均质合金相的合金种类。 因此,合理且有效地制造合金微粒胶体。
    • 10. 发明申请
    • METHOD FOR PRODUCING A METAL NANOPARTICLE COLLOID
    • 生产金属纳米胶体的方法
    • US20130126798A1
    • 2013-05-23
    • US13700793
    • 2011-05-31
    • Isao Nakatani
    • Isao Nakatani
    • B01F17/00
    • B01F17/0042B01J13/0043B22F1/0022B22F1/02B82Y30/00
    • The problems can be solved by using a method for producing a metal nanoparticle colloid, which comprises the steps of S1: mixing, into a nonpolar hydrocarbon oil having a vapor pressure of 10−3 Torr or less at room temperature, organic molecules having both a hydrophilic group and a lipophilic group and having in the end of the hydrophilic group an N, S, P, or O atom or having at the hydrophilic group a functional group of an NH2 group, an NH group, an SH group, a PO group, or an OH group to prepare a base liquid, and S2: placing the base liquid in a rotatable vacuum drum and charging a non-magnetic metal material in a crucible provided in the vacuum drum, and depositing the vapor of the non-magnetic metal material on the base liquid which adheres to the inner wall of the vacuum drum and rotates together with the rotating drum under conditions such that the inside of the vacuum drum is under a reduced pressure and the vacuum drum is rotated, and a task of the present invention is to provide a method for producing a metal nanoparticle colloid having non-magnetic metal nanoparticles having various shapes.
    • 通过使用金属纳米粒子胶体的制造方法可以解决上述问题,该方法包括以下步骤:S1在室温下混合成蒸气压为10-3乇或更低的非极性烃油, 亲水基团和亲油基团,并且在亲水基团末端具有N,S,P或O原子或在亲水基团具有NH 2基团,NH基团,SH基团,PO基团的官能团 或OH基以制备基础液体,S2:将基础液体放置在可旋转的真空鼓中,并将非磁性金属材料装入设置在真空鼓中的坩埚中,并沉积非磁性金属的蒸汽 在基本液体上附着在真空鼓的内壁上并与旋转滚筒一起旋转的基底液体的材料在真空鼓的内部处于减压下并且真空鼓旋转的条件下,并且本发明的任务 发明是公 揭示了具有各种形状的非磁性金属纳米粒子的金属纳米粒子胶体的制造方法。