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1. 发明授权

US4278601A Process for conditioning phthalocyanine pigment 失效
标题翻译：酞菁颜料调理方法
公开(公告)号：US4278601A
公开(公告)日：1981-07-14
申请号：US93488
申请日：1979-11-13
申请人： Ian R. Wheeler , George H. Robertson , David McGregor
发明人： Ian R. Wheeler , George H. Robertson , David McGregor
IPC分类号： C09B67/20 , C09B47/26 , C09B67/00 , C09B67/22 , C09B67/50 , C09B47/04
CPC分类号： C09B67/0035 , C09B47/26 , C09B67/0032
摘要： A process for conditioning pigments which comprises grinding a crude copper phthalocyanine pigment and a crystallizing solvent in the absence of inorganic salt but in the presence of one or more sulphonated phthalocyanine amine derivative having the general formula ##STR1## wherein Pc is a phthalocyanine, R.sup.1, R.sup.3 and R.sup.4 are hydrogen or a hydrocarbon residue, R.sup.2 is a hydrocarbon residue, p is 0 to 3, q is 1 to 4, and the sum of p and q is 1 to 4, the resulting pigment composition is freely dischargeable from the mill in high yield and is, moreover largely in the .beta.-form.
摘要翻译：用于调节颜料的方法，其包括在不存在无机盐的情况下研磨粗铜酞菁颜料和结晶溶剂，但在一种或多种具有通式为“IMAGE”的磺化酞菁胺衍生物存在下，其中Pc为酞菁，R1， R3和R4是氢或烃残基，R2是烃残基，p是0-3，q是1-4，p和q之和为1〜4，所得颜料组合物可以从研磨机自由放出高产量，而且大部分是β形式。

2. 发明授权

US4133695A Pigment composition 失效
标题翻译：颜料组成
公开(公告)号：US4133695A
公开(公告)日：1979-01-09
申请号：US865064
申请日：1977-12-27
申请人： Ian R. Wheeler , George H. Robertson
发明人： Ian R. Wheeler , George H. Robertson
IPC分类号： C09B47/32 , C09B47/26 , C09B67/22 , C09B69/04 , C08K5/34
CPC分类号： C09B67/0035 , C09B47/26 , C09B69/04
摘要： A phthalocyanine pigment composition comprising a phthalocyanine pigment and a sulphonated phthalocyanine derivative of the formula(RNHSO.sub.2).sub.m --Pc--(SO.sub.3.sup..crclbar. N.sup..sym. H.sub.3 R).sub.nwherein the sum of m and n is 1 to 4 and R is a tertiary alkyl having 18 to 22 carbon atoms, which composition gives very good flow and strength when incorporated into paint and ink application media.
摘要翻译：一种酞菁颜料组合物，其包含酞菁颜料和式（RNHSO 2）m -Pc-（SO 3（ - ）N（+）H 3 R）n的磺化酞菁衍生物，其中M和N为1至4，R为具有18至22个碳原子的叔烷基，该组合物在掺入涂料和油墨应用介质中时具有非常好的流动性和强度。

3. 发明授权

US4194921A Pigment compositions and process for dust free pigment beads 失效
标题翻译：颜料组合物和无尘颜料珠的工艺
公开(公告)号：US4194921A
公开(公告)日：1980-03-25
申请号：US916169
申请日：1978-06-16
申请人： Ian R. Wheeler , George H. Robertson
发明人： Ian R. Wheeler , George H. Robertson
IPC分类号： C09B67/02 , C09B67/00 , C09B67/08 , C09C3/08 , C09C3/10
CPC分类号： C09B67/0095
摘要： A process for the manufacture of substantially dust free meterable and readily dispersible beads of a pigment composition which comprises contacting with agitation a suspension of a finely divided pigment or pigment composition in a mixture of water and an oxygenated aliphatic hydrocarbon solvent containing from 1 to 5 carbon atoms and having appreciable solubility in water, together with a solution of a carrier which is substantially water insoluble and soluble in the respective solvent at reflux temperature and then distilling off the solvent and recovering the resultant beads by filtration from the aqueous phase.
摘要翻译：一种用于制造颜料组合物的基本上无粉尘的可分散且容易分散的珠粒的方法，该方法包括将细分散的颜料或颜料组合物的悬浮液与水和含有1至5碳的氧化脂族烃溶剂的混合物原子并且在水中具有明显的溶解度，以及在回流温度下基本上不溶于水并可溶于相应溶剂的载体溶液，然后蒸馏出溶剂并通过从水相中过滤回收所得的珠子。

4. 发明授权

US4205995A Pigment compositions 失效
标题翻译：颜料组成
公开(公告)号：US4205995A
公开(公告)日：1980-06-03
申请号：US854865
申请日：1977-11-25
申请人： Ian R. Wheeler , George H. Robertson
发明人： Ian R. Wheeler , George H. Robertson
IPC分类号： C09B47/32 , C09B47/06 , C09B67/22 , C09B67/50 , C08K5/34
CPC分类号： C09B67/0035 , C09B47/06 , C09B67/0026
摘要： A pigment composition comprising 80-99% weight/weight of copper phthalocyanine containing 1.5-10% weight/weight of peripherally-bound chlorine, and 20-1% weight/weight of a sulphonated copper phthalocyanine derivative having the formula: ##STR1## wherein CuPc represents a copper phthalocyanine residue, R.sub.1, R.sub.2, R.sub.3, R.sub.4, R.sub.5 and R.sub.6 are the same or different and each represents a hydrogen atom, an alkyl group having from 1 to 22 carbon atoms or a cyclic alkyl group having from 5 to 22 carbon atoms, an aryl,aralkyl,alkaryl or dehydroabietyl group, X represents hydrogen or an alkali metal atom and m, n and p can each be 0 or a value in the range of from 1 to 4, with the proviso that the sum of m, n and p is within the range of from 1 to 4; the composition being characterized by its x-ray diffraction spectrum as resembling the .gamma.--crystal form, and further characterized by the substantial absence of any tendency to crystallize on prolonged contact with aromatic solvents, even at elevated temperatures, which composition, without further pigmentization stages, is suitable for direct incorporation in surface coating media, and provides excellent strength and flow properties therein.
摘要翻译：一种颜料组合物，其包含80-99重量％重量的含有1.5-10重量％外围结合氯的铜酞菁和20-1重量％的具有下式的磺化铜酞菁衍生物：＆lt; IMAGE＆gt; 其中CuPc表示铜酞菁残基，R 1，R 2，R 3，R 4，R 5和R 6相同或不同，表示氢原子，具有1至22个碳原子的烷基或具有5至 22个碳原子，芳基，芳烷基，烷芳基或脱氢松香基，X表示氢或碱金属原子，m，n和p各自为0或1至4的数值，条件是总和 m，n和p在1〜4的范围内; 该组合物的特征在于其X-射线衍射光谱类似于γ-晶体形式，并且进一步的特征在于，即使在高温下，即使在没有进一步着色阶段的情况下，在长时间与芳族溶剂接触的情况下也不会有结晶倾向适用于直接掺入表面涂层介质中，并在其中提供优异的强度和流动性能。

5. 发明授权

US4496481A Production of azo compounds 失效
标题翻译：生产偶氮化合物
公开(公告)号：US4496481A
公开(公告)日：1985-01-29
申请号：US329860
申请日：1981-12-11
申请人： Ian R. Wheeler
发明人： Ian R. Wheeler
IPC分类号： C09B41/00 , C09B29/32
CPC分类号： C09B41/009
摘要： A process for the production of an azo compound comprising contacting with agitation a solution or dispersion of a diazotizable amine, a solution or dispersion of a coupling component and an organic or inorganic nitrite compound, in a water insoluble liquid organic acid, adding to the reaction mixture so formed aqueous alkali to transfer the organic acid, as its soluble salt, into the aqueous phase and separating the azo compound from the liquors.The azo compounds are produced in high yield and purity and are suitable for use as pigments and disperse dyes.
摘要翻译：一种制备偶氮化合物的方法，其包括将可重氮化胺，偶联组分和有机或无机亚硝酸盐化合物的溶液或分散体搅拌在水不溶性液体有机酸中，加入反应物混合物形成水溶液，将有机酸作为其可溶性盐转移到水相中，并将偶氮化合物与液体分离。偶氮化合物以高产率和纯度生产，适用于颜料和分散染料。

6. 发明授权

US4135944A Pigment composition 失效
标题翻译：颜料组成
公开(公告)号：US4135944A
公开(公告)日：1979-01-23
申请号：US835072
申请日：1977-09-20
申请人： Ian R. Wheeler
发明人： Ian R. Wheeler
IPC分类号： C09B47/04 , C09B47/06 , C09B67/22 , C09B67/50 , C08K5/34
CPC分类号： C09B47/06 , C09B67/0026 , C09B67/0035
摘要： A single stage process for the production of copper phthalocyanine pigment compositions having x-ray diffraction spectra corresponding to the form of pure, or substantially pure .epsilon.-crystal modification of copper phthalocyanine comprising reacting, at an elevated temperature and in an organic solvent, an organic compound capable of forming the phthalocyanine ring system, a copper compound capable of providing the copper atom of the phthalocyanine molecule, a reaction catalyst, and a nitrogen source, in the presence of, as crystal form modifier, a compound of the formula: ##STR1## where Pc represents a copper phthalocyanine residue, R.sub.1, R.sub.2, R.sub.3, R.sub.4, R.sub.5 and R.sub.6 are the same or different and each is a hydrogen atom, an alkyl group, a cycloalkyl group, an aryl, aralkyl, alkaryl, cycloalkaryl or dehydroabietyl group, the alkyl and cycloalkyl groups being optionally unsaturated and/or interrupted by heteroatoms, M represents hydrogen or an alkali metal atom and x, y and z are each in the range of from 0 to 4 with the proviso that the sum of x, y and z is within the range of from 1 to 4. Very red shade copper phthalocyanine pigment compositions of the advantageous .epsilon.-modification can be produced in a single stage without the use of high shear forces.

7. 发明授权

US4725317A Process for preparing pigment compositions 失效
标题翻译：颜料组合物的制备方法
公开(公告)号：US4725317A
公开(公告)日：1988-02-16
申请号：US832027
申请日：1986-02-24
申请人： Ian R. Wheeler
发明人： Ian R. Wheeler
IPC分类号： C09B67/00 , C09C1/00 , C09C1/62 , C09D17/00
CPC分类号： B82Y30/00 , C09B67/0094 , C09C1/62 , C09D17/006 , C01P2004/32 , C01P2004/51 , C01P2004/61 , C01P2004/64 , Y02P10/138
摘要： The invention relates to a process for preparing low- or non-dusting substantially completely non-volatile metal pigment compositions by forming a coherent paste comprising an organic binder medium, an organic liquid vehicle and metal pigment, in powder or flake form, the paste being formed by mixing a first component comprising the organic binder medium and a second component comprising metal pigment with either or both of the first and second components comprising organic liquid vehicle and the paste containing from 1 to 70 percent, preferably from 3 to 45 percent, of the organic binder medium based on the weight of the metal pigment, and removing substantially all of the organic liquid vehicle(s) from the coherent paste, optionally after sub-dividing the coherent paste into particles, such as pellets, tablets or granules. The resulting solid metal pigment composition comprises metal pigment particles dispersed in a matrix of the organic binder material.
摘要翻译：本发明涉及通过以粉末或片状形式形成包含有机粘合剂介质，有机液体载体和金属颜料的粘性糊料来制备低或不起尘的基本上完全非挥发性的金属颜料组合物的方法，通过将包含有机粘合剂介质的第一组分和包含金属颜料的第二组分与包含有机液体载体的第一和第二组分中的一种或两种混合而形成，所述第一组分含有1至70重量％，优选3至45重量％所述有机粘合剂介质基于所述金属颜料的重量，以及基本上从所述粘性浆料中去除所述有机液体载体，任选地在将所述粘性浆料分解成颗粒，例如颗粒，片剂或颗粒之后。所得固体金属颜料组合物包含分散在有机粘合剂材料的基质中的金属颜料颗粒。

8. 发明授权

US4255375A Process for the preparation of dustless, readily-dispersible pigment or dyestuff granules 失效
标题翻译：无尘，易分散颜料或染料颗粒的制备方法
公开(公告)号：US4255375A
公开(公告)日：1981-03-10
申请号：US43592
申请日：1979-05-29
申请人： Ian A. Macpherson , John A. Stirling , Ian R. Wheeler , James M. McCrae
发明人： Ian A. Macpherson , John A. Stirling , Ian R. Wheeler , James M. McCrae
IPC分类号： C09B67/08 , C09B67/00 , C09B67/10 , C09B67/14 , C08L91/00
CPC分类号： C09B67/0095 , C09B67/0017
摘要： A process for producing a pigment or dyestuff composition in the form of dustless readily dispersible granules, which process comprises contacting, with agitation, an aqueous dispersion of a pigment and a composition comprising one or more organic acids which are liquid at temperatures below 100.degree. C. or their salts, at a pH value at which the acid is insoluble in water, the temperature being maintained during contacting above the melting point of the acid until the pigment has completely transferred into the organic phase; increasing the pH to a value suitable to render the acid soluble in water and recovering the resulting granules.
摘要翻译：一种制备无尘容易分散颗粒形式的颜料或染料组合物的方法，该方法包括在搅拌下使颜料的水分散体和包含一种或多种在100℃以下的液体的有机酸的组合物接触或其盐，在酸不溶于水的pH值下，在酸的熔点以上接触时保持温度，直到颜料完全转移到有机相中; 将pH增加到适于使酸溶于水并回收所得颗粒的值。

9. 发明授权

US4171309A Process for the preparation of a solvent-stable, red-shade copper phthalocyanine pigment composition 失效
标题翻译：制备溶剂稳定的红色铜酞菁颜料组合物的方法
公开(公告)号：US4171309A
公开(公告)日：1979-10-16
申请号：US875844
申请日：1978-02-07
申请人： Ian R. Wheeler
发明人： Ian R. Wheeler
IPC分类号： C09B47/32 , C09B47/06 , C09B67/22 , C09B67/00
CPC分类号： C09B47/06 , C09B67/0035
摘要： A process for the preparation of a solvent-stable, red shade copper phthalocyanine pigment composition by reacting an organic compound capable of forming the phthalocyanine ring system, benzophenone 3,3',4,4'-tetracarboxylic acid or a derivative thereof, a copper compound capable of providing the copper atom of the copper phthalocyanine molecule, a reaction catalyst, and a nitrogen source, optionally in the presence of at least one phthalocyanine compound substituted by 1 to 4 groups of a sulphonate or sulphonic acid and/or sulphonamide which may be N-substituted.
摘要翻译：通过使能够形成酞菁环体系的有机化合物，二苯甲酮3,3'，4,4'-四羧酸或其衍生物，铜，二苯甲酮或其衍生物反应制备溶剂稳定的红色阴离子铜酞菁颜料组合物的方法能够提供铜酞菁分子的铜原子，反应催化剂和氮源的化合物，任选地在至少一种被1至4个磺酸基或磺酸和/或磺酰胺基团取代的酞菁化合物存在下，其可以被N取代。

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