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1. 发明授权

US07674929B2 Method for the production of β-aminopropionic acid derivatives 有权
标题翻译：生产氨基丙酸衍生物的方法
公开(公告)号：US07674929B2
公开(公告)日：2010-03-09
申请号：US12066681
申请日：2006-09-13
申请人： Holger Evers , Johann-Peter Melder , Thomas Preiss , Harald Meissner
发明人： Holger Evers , Johann-Peter Melder , Thomas Preiss , Harald Meissner
IPC分类号： C07C255/00
CPC分类号： C07C253/30 , C07B43/04 , C07C227/06 , C07C2601/14 , C07C255/24
摘要： The invention relates to a process for preparing β-aminopropionic acid derivatives by reacting a primary or secondary amine with an acrylic acid derivative, wherein comprises (i) a first primary or secondary amine is provided as an amine of value and reacted with the acrylic acid derivative, to obtain a reaction mixture comprising a first β-aminopropionic acid derivative as a product of value and additionally unconverted acrylic acid derivative, (ii) the unconverted acrylic acid derivative present in the reaction mixture is reacted with a second secondary amine as a scavenger amine virtually fully to give a second β-aminopropionic acid derivative to obtain a reaction mixture comprising the first β-aminopropionic acid derivative as a product of value, the second β-aminopropionic acid derivative and unconverted secondary amine.
摘要翻译：本发明涉及一种通过使伯胺或仲胺与丙烯酸衍生物反应来制备β-氨基丙酸衍生物的方法，其中包括（i）第一伯胺或仲胺作为有价值的胺并与丙烯酸反应酸衍生物，得到包含第一和次氨基丙酸衍生物作为值的产物和另外未转化的丙烯酸衍生物的反应混合物，（ii）将存在于反应混合物中的未转化的丙烯酸衍生物与第二仲胺反应，一种清除剂胺实际上完全可以得到第二种 - 氨基丙酸衍生物，以获得包含第一种和第二种 - 氨基丙酸衍生物和未转化的仲胺的第一种 - 氨基丙酸衍生物的反应混合物。

2. 发明申请

US20080249333A1 Method for the Production of Beta-Aminopropionic Acid Derivatives 有权
标题翻译： β-氨基丙酸衍生物的制备方法
公开(公告)号：US20080249333A1
公开(公告)日：2008-10-09
申请号：US12066681
申请日：2006-09-13
申请人： Holger Evers , Johann-Peter Melder , Thomas Preiss , Harald Meissner
发明人： Holger Evers , Johann-Peter Melder , Thomas Preiss , Harald Meissner
IPC分类号： C07C229/02
CPC分类号： C07C253/30 , C07B43/04 , C07C227/06 , C07C2601/14 , C07C255/24
摘要： The invention relates to a process for preparing β-aminopropionic acid derivatives by reacting a primary or secondary amine with an acrylic acid derivative, wherein comprises (i) a first primary or secondary amine is provided as an amine of value and reacted with the acrylic acid derivative, to obtain a reaction mixture comprising a first β-aminopropionic acid derivative as a product of value and additionally unconverted acrylic acid derivative, (ii) the unconverted acrylic acid derivative present in the reaction mixture is reacted with a second secondary amine as a scavenger amine virtually fully to give a second β-aminopropionic acid derivative to obtain a reaction mixture comprising the first β-aminopropionic acid derivative as a product of value, the second β-aminopropionic acid derivative and unconverted secondary amine.
摘要翻译：本发明涉及通过使伯胺或仲胺与丙烯酸衍生物反应来制备β-氨基丙酸衍生物的方法，其中包括（i）第一伯胺或仲胺作为有价值的胺并与丙烯酸反应衍生物，以获得包含作为有价值的产物的第一β-氨基丙酸衍生物和另外未转化的丙烯酸衍生物的反应混合物，（ii）反应混合物中存在的未转化的丙烯酸衍生物与作为清除剂的第二仲胺反应胺实际上完全提供第二β-氨基丙酸衍生物以获得包含第一β-氨基丙酸衍生物作为有价值的产物，第二β-氨基丙酸衍生物和未转化的仲胺的反应混合物。

3. 发明申请

US20080306299A1 Method for the Production of Aminoalkane Acid Amides 失效
标题翻译：氨基烷酰胺的制备方法
公开(公告)号：US20080306299A1
公开(公告)日：2008-12-11
申请号：US12158200
申请日：2006-12-15
申请人： Martin Ernst , Andreas Kusche , Gunnar Heydrich , Horst Grafmans , Holger Evers , Johann-Peter Melder , Harald Meissner , Torsten Freund
发明人： Martin Ernst , Andreas Kusche , Gunnar Heydrich , Horst Grafmans , Holger Evers , Johann-Peter Melder , Harald Meissner , Torsten Freund
IPC分类号： C07C231/14
CPC分类号： C07C231/14 , Y02P20/582 , C07C237/06
摘要： The invention relates to a process for preparing aminoalkanamides by reacting cyanoalkanoic esters with a) ammonia or an amine and b) hydrogen in the presence of a catalyst, the reaction with component b) being started simultaneously or not later than a maximum of 100 minutes after commencement of the reaction of the cyanoalkanoic ester with component a).
摘要翻译：本发明涉及一种通过氰基链烷酸酯与a）氨或胺反应制备氨基烷酰胺的方法，和b）在催化剂存在下使氢气反应，与组分b）的反应同时或不迟于最多100分钟开始开始氰基链烷酸酯与组分a）的反应。

4. 发明授权

US07754922B2 Process for preparing amines and zirconium dioxide- and nickel-containing catalysts for use therein 失效
标题翻译：制备用于其中的胺和二氧化锆和含镍催化剂的方法
公开(公告)号：US07754922B2
公开(公告)日：2010-07-13
申请号：US12373793
申请日：2007-07-04
申请人： Petr Kubanek , Bram Willem Hoffer , Ekkehard Schwab , Johann-Peter Melder , Holger Evers , Till Gerlach
发明人： Petr Kubanek , Bram Willem Hoffer , Ekkehard Schwab , Johann-Peter Melder , Holger Evers , Till Gerlach
IPC分类号： C07C209/16 , C07C209/18 , C07C209/26 , B01J23/28
CPC分类号： C07C213/02 , B01J23/002 , B01J23/885 , B01J37/0009 , B01J37/0045 , B01J37/03 , B01J37/18 , B01J2523/00 , C07C209/16 , C07C209/26 , C07D295/023 , C07C211/10 , C07C215/08 , C07C217/08
摘要： Processes comprising: (i) providing a reactant selected from the group consisting of primary alcohols, secondary alcohols, aldehydes, ketones and mixtures thereof; and (ii) reacting the reactant with hydrogen and a nitrogen compound selected from the group consisting of ammonia, primary amines, secondary amines and mixtures thereof, in the presence of a catalyst comprising a zirconium dioxide- and nickel-containing catalytically active composition, to form an amine; wherein the catalytically active composition, prior to reduction with hydrogen, comprises oxygen compounds of zirconium, copper, nickel and cobalt, and one or more oxygen compounds of molybdenum in an amount of 5.5 to 12% by weight, calculated as MoO3.
摘要翻译：方法包括：（i）提供选自伯醇，仲醇，醛，酮及其混合物的反应物; 和（ii）在包含二氧化锆和含镍的催化活性组合物的催化剂存在下，使反应物与氢气和选自氨，伯胺，仲胺及其混合物的氮化合物反应，形成胺; 其中所述催化活性组合物在用氢还原之前包括锆，铜，镍和钴的氧化合物，以及以MoO 3计算的一种或多种重量百分比为5.5至12％的钼的氧化合物。

5. 发明授权

US07615665B2 Method for producing ethylene amines 有权
标题翻译：生产乙烯胺的方法
公开(公告)号：US07615665B2
公开(公告)日：2009-11-10
申请号：US12088548
申请日：2006-09-25
申请人： Till Gerlach , Holger Evers , Johann-Peter Melder
发明人： Till Gerlach , Holger Evers , Johann-Peter Melder
IPC分类号： C07C211/00
CPC分类号： C07C209/64 , B01J23/70 , B01J35/026 , C07D295/023 , C07D295/027 , C07D295/13 , C07C211/14
摘要： Processes comprising: providing a starting material comprising ethylenediamine; and reacting the starting material in the presence of a heterogeneous transition metal catalyst to form one or more ethylene amines; wherein the catalyst comprises a catalytically active composition, which prior to treatment with hydrogen, comprises a mixture of oxygen-containing compounds of aluminum, copper, nickel and cobalt; and wherein the catalyst is present as one or more shaped catalyst particles selected from spheres, extrudates, pellets and other geometries, wherein the sphere or extrudate has a diameter of
摘要翻译：方法包括：提供包含乙二胺的原料; 和在非均相过渡金属催化剂存在下使原料反应形成一种或多种亚乙基胺; 其中所述催化剂包含催化活性组合物，其在用氢处理之前包括铝，铜，镍和钴的含氧化合物的混合物; 并且其中所述催化剂作为选自球体，挤出物，丸粒和其它几何形状的一种或多种成型催化剂颗粒存在，其中所述球体或挤出物的直径<3mm，所述颗粒具有<3mm的高度，而另一种几何形状具有等效直径L = 1 / a'<0.70mm，其中a'是每单位体积的外表面积（mms2 / mmp3），由'= A p V p定义，其中Ap是外表面积的催化剂颗粒（mms2），Vp是催化剂颗粒的体积（mmp3）。

6. 发明授权

US07696384B2 Process for producing ethyleneamines 有权
标题翻译：制备亚乙基胺的方法
公开(公告)号：US07696384B2
公开(公告)日：2010-04-13
申请号：US12088715
申请日：2006-09-25
申请人： Gunther Van Cauwenberge , Johann-Peter Melder , Holger Evers , Till Gerlach , Frank Kiesslich , Ekkehard Schwab , Bram Willem Hoffer
发明人： Gunther Van Cauwenberge , Johann-Peter Melder , Holger Evers , Till Gerlach , Frank Kiesslich , Ekkehard Schwab , Bram Willem Hoffer
IPC分类号： C07C211/00
CPC分类号： C07C209/16 , B01J21/04 , B01J23/755 , B01J35/023 , B01J37/0201 , B01J37/18 , C07D295/02 , C07D295/13 , C07C211/10 , C07C211/14
摘要： Processes comprising: providing a starting material comprising monoethanolamine; and reacting the starting material with ammonia in the presence of a heterogeneous transition metal catalyst to form a reaction product comprising one or more ethylene amines; wherein the catalyst comprises a catalytically active composition, which prior to treatment with hydrogen, comprises a mixture of oxygen-containing compounds of aluminum, copper, nickel and cobalt; and wherein the catalyst is present as one or more shaped catalyst particles selected from spheres, extrudates, pellets and other geometries, wherein the sphere or extrudate has a diameter of
摘要翻译：方法包括：提供包含单乙醇胺的原料; 并在非均相过渡金属催化剂的存在下使原料与氨反应形成包含一种或多种亚乙基胺的反应产物; 其中所述催化剂包含催化活性组合物，其在用氢处理之前包括铝，铜，镍和钴的含氧化合物的混合物; 并且其中所述催化剂作为选自球体，挤出物，丸粒和其它几何形状的一种或多种成型催化剂颗粒存在，其中所述球体或挤出物的直径<3mm，所述颗粒具有<3mm的高度，而另一种几何形状具有等效直径L = 1 / a'<0.70mm，其中a'是每单位体积的外表面积（mms2 / mmp3），由'= A p V p定义，其中Ap是外表面积的催化剂颗粒（mms2），Vp是催化剂颗粒的体积（mmp3）。

7. 发明申请

US20090264652A1 METHOD FOR PRODUCING AN AMINE 审中-公开
标题翻译：生产氨的方法
公开(公告)号：US20090264652A1
公开(公告)日：2009-10-22
申请号：US12373783
申请日：2007-07-04
申请人： Petr Kubanek , Bram Willem Hoffer , Ekkehard Schwab , Johann-Peter Melder , Holger Evers , Till Gerlach
发明人： Petr Kubanek , Bram Willem Hoffer , Ekkehard Schwab , Johann-Peter Melder , Holger Evers , Till Gerlach
IPC分类号： C07D265/30 , B01J23/72
CPC分类号： B01J23/8926 , B01J37/03 , B01J37/14 , B01J37/18 , C07C213/02 , C07D295/023
摘要： Processes comprising: (i) providing a reactant selected from the group consisting of primary alcohols, secondary alcohols, aldehydes, ketones and mixtures thereof; and (ii) reacting the reactant with hydrogen and a nitrogen compound selected from the group consisting of ammonia, primary amines, secondary amines and mixtures thereof in the presence of a catalyst comprising a zirconium dioxide- and nickel-containing catalytically active composition, to form an amine; wherein the catalytically active composition, prior to reduction with hydrogen, comprises oxygen compounds of zirconium, copper, nickel and cobalt, and one or more oxygen compounds of silver in an amount of 0.5 to 6% by weight, calculated as AgO.
摘要翻译：方法包括：（i）提供选自伯醇，仲醇，醛，酮及其混合物的反应物; 和（ii）在包含含二氧化锆和含镍的催化活性组合物的催化剂存在下，使反应物与氢气和选自氨，伯胺，仲胺及其混合物的氮化合物反应，形成胺; 其中所述催化活性组合物在用氢还原之前包含锆，铜，镍和钴的氧化合物，以及一种或多种以AgO计算的0.5至6重量％的银的氧化合物。

8. 发明申请

US20080255351A1 Method for Preparing Aminodiglycol (Adg) and Morpholine 审中-公开
标题翻译：制备氨基二甘醇（Adg）和吗啉的方法
公开(公告)号：US20080255351A1
公开(公告)日：2008-10-16
申请号：US12088718
申请日：2006-09-25
申请人： Bram Willem Hoffer , Holger Evers , Petr Kubanek , Till Gerlach , Johann-Peter Melder , Frank Funke , Matthias Frauenkron , Helmut Schmidtke
发明人： Bram Willem Hoffer , Holger Evers , Petr Kubanek , Till Gerlach , Johann-Peter Melder , Frank Funke , Matthias Frauenkron , Helmut Schmidtke
IPC分类号： C07D265/30
CPC分类号： C07D295/023 , C07C213/02 , C07C217/08
摘要： Processes comprising: providing a starting material comprising diethylene glycol; and reacting the starting material with ammonia in the presence of a heterogeneous transition metal catalyst to form a reaction product comprising aminodiglycol and morpholine; wherein the catalyst comprises a catalytically active composition, which prior to treatment with hydrogen, comprises a mixture of oxygen-containing compounds of copper, nickel, cobalt and at least one of aluminum and zirconium; and wherein the catalyst is present as one or more shaped catalyst particles selected from spheres, extrudates, pellets and other geometries, wherein the sphere or extradate has a diameter of
摘要翻译：方法包括：提供包含二甘醇的原料; 并在非均相过渡金属催化剂存在下使原料与氨反应形成包含氨基二甘醇和吗啉的反应产物; 其中所述催化剂包含催化活性组合物，其在用氢处理之前包含铜，镍，钴和铝和锆中的至少一种的含氧化合物的混合物; 并且其中所述催化剂作为选自球体，挤出物，丸粒和其它几何形状的一种或多种成型催化剂颗粒存在，其中所述球体或引体具有<3mm的直径，所述颗粒具有<3mm的高度，而另一个几何形状具有等效直径L = 1 / a'<0.70mm，其中a'是每单位体积的外表面积（mm×s×2 / 由 ${定义的}^{3 MI> a =A/ MSUB>Vp其中A < SUB>是催化剂颗粒的外表面积（mm 2），V p是催化剂颗粒的体积（mm 3） 3＆lt; 3＆gt; 3＆lt; 3＆gt;）。}$

9. 发明授权

US08759580B2 Method for the production of aminoalkane acid amides 失效
标题翻译：生产氨基烷酰胺的方法
公开(公告)号：US08759580B2
公开(公告)日：2014-06-24
申请号：US12158200
申请日：2006-12-15
申请人： Martin Ernst , Andreas Kusche , Gunnar Heydrich , Horst Grafmans , Holger Evers , Johann-Peter Melder , Harald Meiβner , Torsten Freund
发明人： Martin Ernst , Andreas Kusche , Gunnar Heydrich , Horst Grafmans , Holger Evers , Johann-Peter Melder , Harald Meiβner , Torsten Freund
IPC分类号： C07C231/04
CPC分类号： C07C231/14 , Y02P20/582 , C07C237/06
摘要： The invention relates to a process for preparing aminoalkanamides by reacting cyanoalkanoic esters with a) ammonia or an amine and b) hydrogen in the presence of a catalyst, the reaction with component b) being started simultaneously or not later than a maximum of 100 minutes after commencement of the reaction of the cyanoalkanoic ester with component a).
摘要翻译：本发明涉及一种通过氰基链烷酸酯与a）氨或胺反应制备氨基烷酰胺的方法，和b）在催化剂存在下使氢气反应，与组分b）的反应同时或不迟于最多100分钟开始开始氰基链烷酸酯与组分a）的反应。

10. 发明申请

US20100010264A1 METHOD FOR PRODUCING AN AMINE 失效
标题翻译：生产氨的方法
公开(公告)号：US20100010264A1
公开(公告)日：2010-01-14
申请号：US12373849
申请日：2007-07-04
申请人： Petr Kubanek , Bram Willem Hoffer , Ekkehard Schwab , Johann-Peter Melder , Holger Evers , Till Gerlach
发明人： Petr Kubanek , Bram Willem Hoffer , Ekkehard Schwab , Johann-Peter Melder , Holger Evers , Till Gerlach
IPC分类号： C07C209/00 , B01J23/72 , B01J23/755
CPC分类号： C07C209/16 , B01J23/825 , B01J23/835 , B01J23/8435 , B01J23/8437 , B01J37/0009 , B01J37/03 , B01J37/14 , B01J37/18 , C07C209/26 , C07C213/02 , C07D295/02 , C07D295/023 , C07C211/10 , C07C215/08 , C07C217/08
摘要： Processes comprising: (i) providing a reactant selected from the group consisting of primary alcohols, secondary alcohols, aldehydes, ketones and mixtures thereof; and (ii) reacting the reactant with hydrogen and a nitrogen compound selected from the group consisting of ammonia, primary amines, secondary amines and mixtures thereof, in the presence of a catalyst comprising a zirconium dioxide- and nickel-containing catalytically active composition, to form an amine; wherein the catalytically active composition, prior to reduction with hydrogen, comprises oxygen compounds of zirconium, copper, and nickel, and one or more oxygen compounds of one or more metals selected from the group consisting of Sb, Pb, Bi, and In.
摘要翻译：方法包括：（i）提供选自伯醇，仲醇，醛，酮及其混合物的反应物; 和（ii）在包含二氧化锆和含镍的催化活性组合物的催化剂存在下，使反应物与氢气和选自氨，伯胺，仲胺及其混合物的氮化合物反应，形成胺; 其中所述催化活性组合物在用氢还原之前包含锆，铜和镍的氧化合物和一种或多种选自Sb，Pb，Bi和In的一种或多种金属的氧化合物。

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