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1. 发明授权

US06262292B1 Method for producing cyanophenyl derivatives 失效
标题翻译：制备氰基苯基衍生物的方法
公开(公告)号：US06262292B1
公开(公告)日：2001-07-17
申请号：US09343268
申请日：1999-06-30
申请人： Hiroshi Yasuda , Kimitaka Ohshiro , Kaneo Nozawa , Kohei Morikawa
发明人： Hiroshi Yasuda , Kimitaka Ohshiro , Kaneo Nozawa , Kohei Morikawa
IPC分类号： C07C25500
CPC分类号： C07C253/30 , C07C255/56 , C07C255/57
摘要： The invention relates to (1) a process for producing a cyanobenzaldehyde compound by converting the aminomethyl group in a cyanobenzylamine compound into an aldehyde group using an oxidizing agent without impairing the cyano group, to (2) a process for producing a cyanobenzoyl halide compound by converting the aldehyde group in a cyanobenzaldehyde compound into an acid halide group without impairing the cyano group, and to (3) a process for producing a cyanobenzoic acid compound by reacting a cyanobenzaldehyde compound with a hypohalogenous compound. According to the present invention, cyanophenyl derivatives that are useful as an intermediate of medical preparations, agricultural chemicals, liquid crystals, functional high molecular monomers and the like can be produced efficiently from raw materials that are obtained without difficulty.
摘要翻译：本发明涉及（1）通过使用氧化剂将氰基苄胺化合物中的氨基甲基转化为醛基而不损害氰基的方法，（2）通过以下方法制备氰基苯甲醛化合物的方法：（2）通过将氰基苯甲醛化合物中的醛基转化成酰卤基团而不损害氰基，和（3）通过使氰基苯甲醛化合物与低级光化合物反应来制备氰基苯甲酸化合物的方法。根据本发明，氰基苯基衍生物作为医药制剂，农药，液晶，功能性高分子单体等的中间体是有用的，可以从难以获得的原料中有效地制造。

2. 发明申请

US20080132597A1 Ethylenically Unsaturated Group-Containing Isocyanate Compound and Process for Producing the Same, and Reactive Monomer, Reactive (Meth) Acrylate Polymer and its Use 有权
标题翻译：含烯不饱和基团的异氰酸酯化合物及其制备方法，和反应性单体，反应性（甲基）丙烯酸酯聚合物及其用途
公开(公告)号：US20080132597A1
公开(公告)日：2008-06-05
申请号：US11666905
申请日：2005-10-31
申请人： Kaneo Nozawa , Katsutoshi Morinaka , Toru Sasaki , Katsumi Murofushi
发明人： Kaneo Nozawa , Katsutoshi Morinaka , Toru Sasaki , Katsumi Murofushi
IPC分类号： C08F299/00 , C07C69/34 , C08F126/00 , C08L39/00 , C08J3/28
CPC分类号： C07C265/04 , B33Y70/00 , C07C271/16 , C07C271/34 , C07C275/22 , C07C275/24 , C07C275/30 , C07C333/04 , C07C2601/14 , C07C2603/18 , C07C2603/74 , C08F222/1006 , C08F222/22 , G03F7/027 , H05K3/287 , Y10T428/24917
摘要： There are provided a novel ethylenically unsaturated group-containing isocyanate compound, a process for producing the same, and a reactive monomer produced from the isocyanate compound, a reactive polymer and its use. The ethylenically unsaturated group-containing isocyanate compound according to the present invention is represented by formula (I).
摘要翻译：提供了一种新颖的含烯键式不饱和基团的异氰酸酯化合物，其制备方法以及由异氰酸酯化合物，反应性聚合物及其用途制备的反应性单体。本发明的含烯属不饱和基团的异氰酸酯化合物由式（I）表示。

3. 发明申请

US20070197762A1 Method For Producing (Meth)Acrylate Derivative Having Isocyanate Group 有权
标题翻译：生产具有异氰酸酯基团（甲基）丙烯酸酯衍生物的方法
公开(公告)号：US20070197762A1
公开(公告)日：2007-08-23
申请号：US10594231
申请日：2005-03-22
申请人： Kaneo Nozawa , Katsutoshi Morinaka
发明人： Kaneo Nozawa , Katsutoshi Morinaka
IPC分类号： C08G63/00
CPC分类号： C07C263/20 , C07C263/16 , C07C265/04
摘要： The invention aims to provide a method whereby (meth)acrylate derivatives having an isocyanate group can be obtained in high yield by dehydrochlorination of 3-chloropropionate derivatives having an isocyanate group under industrially advantageous and mild conditions, and the content of residual hydrolyzable chlorine can be reduced. A method for producing a (meth)acrylate derivative having an isocyanate group comprises performing dehydrochlorination of a 3-chloropropionate derivative having an isocyanate group in the presence of a basic nitrogen compound having a tertiary nitrogen, the tertiary nitrogen of the basic nitrogen compound having at least one group other than an aromatic ring group.
摘要翻译：本发明的目的在于提供一种方法，可以在工业上有利且温和的条件下，通过使具有异氰酸酯基的3-氯丙酸酯衍生物的脱氯化氢以高产率获得具有异氰酸酯基的（甲基）丙烯酸酯衍生物，残留的可水解氯的含量可以为减少具有异氰酸酯基的（甲基）丙烯酸酯衍生物的制造方法包括在具有叔氮的碱性氮化合物的存在下，对具有异氰酸酯基的3-氯丙酸酯衍生物进行脱氯化氢，碱式氮化合物的叔氮具有除芳香族环以外的至少一个基团。

4. 发明授权

US06646156B2 (Meth)acryloyl-group-containing carbamoyl halides and production process therefor 失效
标题翻译：（甲基）丙烯酰基的氨基甲酰卤及其制备方法
公开(公告)号：US06646156B2
公开(公告)日：2003-11-11
申请号：US09835321
申请日：2001-04-17
申请人： Ayako Nishioka , Kaneo Nozawa
发明人： Ayako Nishioka , Kaneo Nozawa
IPC分类号： C07C6952
CPC分类号： C07C219/08 , C07C271/04
摘要： The present invention provides a (meth)acryloyl-group-containing carbamoyl halide represented by the following formula (1): where R1 represents a hydrogen atom or a methyl group; R2 represents a linear or branched C1-C10 alkylene group; R3 represents a C1-C5 alkyl group; and X represents a halogen atom. The present invention also provides a production process for the halide.
摘要翻译：本发明提供由下式（1）表示的（甲基）丙烯酰基的氨基甲酰卤：其中R1表示氢原子或甲基; R2表示直链或支链C1-C10亚烷基; R3表示C1-C5烷基; X表示卤素原子。本发明还提供了卤化物的制备方法。

5. 发明申请

US20100174109A1 METHOD FOR PRODUCING ETHYLENICALLY UNSATURATED GROUP-CONTAINING ISOCYANATE COMPOUND HAVING ETHER BOND 审中-公开
标题翻译：用于生产具有乙烯键的含乙烯基的不饱和基团的异氰酸酯化合物的方法
公开(公告)号：US20100174109A1
公开(公告)日：2010-07-08
申请号：US12600572
申请日：2008-05-19
申请人： Kaneo Nozawa , Katsutoshi Ohno , Yotaro Hattori
发明人： Kaneo Nozawa , Katsutoshi Ohno , Yotaro Hattori
IPC分类号： C07C69/52
CPC分类号： C07C263/10 , C07C265/04
摘要： To provide a method for producing an ethylenically unsaturated group-containing isocyanate compound having an ether bond under such conditions that the ether bond is unlikely to be cleaved and the polymerization of an unsaturated group can be suppressed. The method for producing an ethylenically unsaturated group-containing isocyanate compound having an ether bond of the present invention is a method for producing an ethylenically unsaturated double bond-containing isocyanate compound from an amino alcohol having an ether bond and is characterized in that a reaction solvent in which the solubility of hydrogen chloride is 0.1 mole percent or less at 25° C. is used.
摘要翻译：本发明提供一种在醚键不易断裂，可抑制不饱和基团的聚合的条件下制造具有醚键的含烯属不饱和基团的异氰酸酯化合物的方法。本发明的具有醚键的含烯属不饱和基团的异氰酸酯化合物的制造方法是由具有醚键的氨基醇制造含有烯键式不饱和双键的异氰酸酯化合物的方法，其特征在于反应溶剂其中使用氯化氢在25℃下的溶解度为0.1摩尔％以下。

6. 发明授权

US07632965B2 Method for producing (meth)acrylate derivative having isocyanate group 有权
标题翻译：具有异氰酸酯基的（甲基）丙烯酸酯衍生物的制造方法
公开(公告)号：US07632965B2
公开(公告)日：2009-12-15
申请号：US10594231
申请日：2005-03-22
申请人： Kaneo Nozawa , Katsutoshi Morinaka
发明人： Kaneo Nozawa , Katsutoshi Morinaka
IPC分类号： C07C263/20 , C07C265/04
CPC分类号： C07C263/20 , C07C263/16 , C07C265/04
摘要： The invention aims to provide a method whereby (meth)acrylate derivatives having an isocyanate group can be obtained in high yield by dehydrochlorination of 3-chloropropionate derivatives having an isocyanate group under industrially advantageous and mild conditions, and the content of residual hydrolyzable chlorine can be reduced. A method for producing a (meth)acrylate derivative having an isocyanate group comprises performing dehydrochlorination of a 3-chloropropionate derivative having an isocyanate group in the presence of a basic nitrogen compound having a tertiary nitrogen, the tertiary nitrogen of the basic nitrogen compound having at least one group other than an aromatic ring group.
摘要翻译：本发明的目的在于提供一种方法，可以在工业上有利且温和的条件下，通过使具有异氰酸酯基的3-氯丙酸酯衍生物的脱氯化氢以高产率获得具有异氰酸酯基的（甲基）丙烯酸酯衍生物，残留的可水解氯的含量可以为减少具有异氰酸酯基的（甲基）丙烯酸酯衍生物的制造方法包括在具有叔氮的碱性氮化合物的存在下，对具有异氰酸酯基的3-氯丙酸酯衍生物进行脱氯化氢，碱式氮化合物的叔氮具有除芳香族环以外的至少一个基团。

7. 发明授权

US08044235B2 (Meth) acryloyl group-containing aromatic isocyanate compound and production process thereof 失效
标题翻译：（甲基）丙烯酰基芳族异氰酸酯化合物及其制备方法
公开(公告)号：US08044235B2
公开(公告)日：2011-10-25
申请号：US11886487
申请日：2006-03-15
申请人： Kaneo Nozawa , Katsutoshi Ohno , Yotaro Hattori
发明人： Kaneo Nozawa , Katsutoshi Ohno , Yotaro Hattori
IPC分类号： C07C263/10 , C07C263/00
CPC分类号： C07C265/12 , B33Y70/00 , C07C271/16 , C07C271/28 , C07C2602/42 , C07C2603/18 , C08F220/36 , C08F222/1006 , C08G18/44 , C08G18/6229 , C08G18/8116 , G03F7/0007 , G03F7/027 , G03F7/105 , H05K3/287
摘要： A monomer is provided which is excellent in reactivity, can give high heat resistance and high refractive index, and has two or more polymerizable functional groups with different polymerization properties and an aromatic ring in the molecule. An industrial advantageous process for producing the monomer is also provided. The monomer is an aromatic isocyanate compound containing a (meth)acryloyl group, and is represented by Formula (I): wherein R1 is a single bond or a linear or branched alkylene group of 1 to 5 carbon atoms, R2 is a hydrogen atom or a methyl group, R3 is a single bond or a linear or branched alkylene group of 1 to 3 carbon atoms, X is independently a halogen atom or an electron-withdrawing group, m is an integer ranging from 0 to 4, n is an integer ranging from 1 to 3, and 1≦m+n≦5.
摘要翻译：提供了具有优异的反应性，可以赋予高耐热性和高折射率的单体，并且在分子中具有两个以上具有不同聚合性能的聚合性官能团和芳香环。还提供了用于制备单体的工业上有利的方法。单体是含有（甲基）丙烯酰基的芳香族异氰酸酯化合物，由式（I）表示：其中，R 1为单键或1〜5个碳原子的直链或支链亚烷基，R2为氢原子或甲基，R3为单键或1〜3个碳原子的直链或支链亚烷基，X独立地为卤素原子或吸电子基团，m为0〜4的整数，n为整数范围从1到3，和1＆nlE; m + n＆nlE; 5。

8. 发明授权

US07579066B2 Ethylenically unsaturated group-containing isocyanate compound and process for producing the same, and reactive monomer, reactive (meth) acrylate polymer and its use 有权
标题翻译：含烯键式不饱和基团的异氰酸酯化合物及其制备方法，反应性单体，反应性（甲基）丙烯酸酯聚合物及其用途
公开(公告)号：US07579066B2
公开(公告)日：2009-08-25
申请号：US11666905
申请日：2005-10-31
申请人： Kaneo Nozawa , Katsutoshi Morinaka , Toru Sasaki , Katsumi Murofushi
发明人： Kaneo Nozawa , Katsutoshi Morinaka , Toru Sasaki , Katsumi Murofushi
IPC分类号： C07C263/10 , C07C265/04 , C08F299/00
CPC分类号： C07C265/04 , B33Y70/00 , C07C271/16 , C07C271/34 , C07C275/22 , C07C275/24 , C07C275/30 , C07C333/04 , C07C2601/14 , C07C2603/18 , C07C2603/74 , C08F222/1006 , C08F222/22 , G03F7/027 , H05K3/287 , Y10T428/24917
摘要： There are provided a novel ethylenically unsaturated group-containing isocyanate compound, a process for producing the same, and a reactive monomer produced from the isocyanate compound, a reactive polymer and its use. The ethylenically unsaturated group-containing isocyanate compound according to the present invention is represented by formula (I).
摘要翻译：提供了一种新颖的含烯键式不饱和基团的异氰酸酯化合物，其制备方法以及由异氰酸酯化合物，反应性聚合物及其用途制备的反应性单体。本发明的含烯属不饱和基团的异氰酸酯化合物由式（I）表示。

9. 发明申请

US20090054543A1 (Meth) Acryloyl Group-Containing Aromatic Isocyanate Compound and Production Process Thereof 失效
标题翻译：（甲基）含丙烯酰基的芳族异氰酸酯化合物及其制备方法
公开(公告)号：US20090054543A1
公开(公告)日：2009-02-26
申请号：US11886487
申请日：2006-03-15
申请人： Kaneo Nozawa , Katsutoshi Ohno , Yotaro Hattori
发明人： Kaneo Nozawa , Katsutoshi Ohno , Yotaro Hattori
IPC分类号： C07C229/24 , C07C69/76 , C08F22/10
CPC分类号： C07C265/12 , B33Y70/00 , C07C271/16 , C07C271/28 , C07C2602/42 , C07C2603/18 , C08F220/36 , C08F222/1006 , C08G18/44 , C08G18/6229 , C08G18/8116 , G03F7/0007 , G03F7/027 , G03F7/105 , H05K3/287
摘要： A monomer is provided which is excellent in reactivity, can give high heat resistance and high refractive index, and has two or more polymerizable functional groups with different polymerization properties and an aromatic ring in the molecule. An industrial advantageous process for producing the monomer is also provided. The monomer is an aromatic isocyanate compound containing a (meth)acryloyl group, and is represented by Formula (I): wherein R1 is a single bond or a linear or branched alkylene group of 1 to 5 carbon atoms, R2 is a hydrogen atom or a methyl group, R3 is a single bond or a linear or branched alkylene group of 1 to 3 carbon atoms, X is independently a halogen atom or an electron-withdrawing group, m is an integer ranging from 0 to 4, n is an integer ranging from 1 to 3, and 1≦m+n≦5.
摘要翻译：提供了具有优异的反应性，可以赋予高耐热性和高折射率的单体，并且在分子中具有两个以上具有不同聚合性能的聚合性官能团和芳香环。还提供了用于制备单体的工业上有利的方法。单体是含有（甲基）丙烯酰基的芳香族异氰酸酯化合物，由式（I）表示：其中，R 1为单键或1〜5个碳原子的直链或支链亚烷基，R2为氢原子或甲基，R3为单键或1〜3个碳原子的直链或支链亚烷基，X独立地为卤素原子或吸电子基团，m为0〜4的整数，n为整数范围从1到3，1 <= m + n <= 5。

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