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1. 发明授权

US06812319B2 Wholly aromatic polyester carbonate and process for production of same 失效
标题翻译：全芳香族聚酯碳酸酯及其生产方法
公开(公告)号：US06812319B2
公开(公告)日：2004-11-02
申请号：US10411116
申请日：2003-04-11
申请人： Hiroshi Sakurai , Toyoaki Ishiwata , Shunichi Matsumura , Masayuki Chokai
发明人： Hiroshi Sakurai , Toyoaki Ishiwata , Shunichi Matsumura , Masayuki Chokai
IPC分类号： C08G6400
CPC分类号： C08G63/64 , C08G63/80
摘要： The present invention relates to a wholly aromatic polyester carbonate and a process for its production. An aromatic dicarboxylic acid, an aromatic diol, and a diaryl carbonate are used as starting materials in specific molar ratios, a prepolymerization step, a crystallization step, and a solid-phase polymerization step are essential steps, and a compression molding step is an optional step. This makes it possible to produce with good productivity a wholly aromatic polyester carbonate that has low coloration and a high degree of polymerization.
摘要翻译：本发明涉及全芳族聚酯碳酸酯及其制备方法。芳族二羧酸，芳族二醇和碳酸二芳基酯以特定的摩尔比用作原料，预聚合步骤，结晶步骤和固相聚合步骤是必须的步骤，压缩成型步骤是可选的步。这使得可以以高生产率生产具有低着色和高聚合度的全芳族聚酯碳酸酯。

2. 发明授权

US06858701B2 Wholly aromatic polyester carbonate and process therefor 失效
标题翻译：全芳香族聚酯碳酸酯及其工艺
公开(公告)号：US06858701B2
公开(公告)日：2005-02-22
申请号：US10297082
申请日：2001-05-31
申请人： Hiroshi Sakurai , Toyoaki Ishiwata , Takanori Miyoshi , Shunichi Matsumura
发明人： Hiroshi Sakurai , Toyoaki Ishiwata , Takanori Miyoshi , Shunichi Matsumura
IPC分类号： C08G63/64 , C08G63/00
CPC分类号： C08G63/64
摘要： A wholly aromatic polyester carbonate having a good color and excellent heat resistant stability. This polymer had an extremely low alkali metal content of 10 ppm or less. This polymer is advantageously produced by reacting an aromatic dicarboxylic acid, aromatic diol and diaryl carbonate in a specific molar ratio in the presence of a pyridine-based compound as a catalyst.
摘要翻译：具有良好的颜色和优异的耐热稳定性的全芳族聚酯碳酸酯。该聚合物的碱金属含量极低，为10ppm以下。通过在作为催化剂的吡啶类化合物存在下，通过使芳族二羧酸，芳族二醇和碳酸二芳基酯以特定的摩尔比进行反应来制备该聚合物。

3. 发明授权

US06596839B2 Wholly aromatic polyester and production process therefor 失效
标题翻译：全芳香聚酯及其生产工艺
公开(公告)号：US06596839B2
公开(公告)日：2003-07-22
申请号：US10169671
申请日：2002-07-08
申请人： Takanori Miyoshi , Hiroshi Sakurai , Toyoaki Ishiwata , Shunichi Matsumura
发明人： Takanori Miyoshi , Hiroshi Sakurai , Toyoaki Ishiwata , Shunichi Matsumura
IPC分类号： C08G6300
CPC分类号： C08G63/64 , C08G63/82 , C08G63/83 , C08G63/85 , C08G63/87
摘要： A process for producing a wholly aromatic polyester which is excellent in heat resistance, mechanical properties and yet color and has a high degree of polymerization by melt polymerizing a dicarboxylic acid and a diol directly on an industrial scale at a low cost in a short period of time without esterifying the dicarboxylic acid or diol in advance. To produce the wholly aromatic polyester by reacting and molding an aromatic dicarboxylic acid such as terephthalic acid, an aromatic diol such as 2,2-bis(4-hydroxyphenyl)propane and a diaryl carbonate by heating, a combination of a specific pyridine compound and an alkali metal (bi)carbonate, a combination of a specific pyridine compound and an organic tin compound or a specific titanium compound is existent as a catalyst. Thereby, the wholly aromatic polyester having the above properties is obtained.
摘要翻译：一种全芳香族聚酯的制造方法，其具有优异的耐热性，机械性能和颜色，并且通过在短时间内以低成本在工业规模上直接熔融聚合二羧酸和二醇具有高聚合度预先不二羧酸或二醇酯化。为了通过加热芳族二羧酸如对苯二甲酸，2,2-双（4-羟基苯基）丙烷等芳香族二醇和碳酸二芳基酯反应而成型，可以将特定的吡啶化合物和存在碱金属（bi）碳酸盐，特定吡啶化合物和有机锡化合物或特定钛化合物的组合作为催化剂。由此，得到具有上述特性的全芳香族聚酯。

4. 发明授权

US06696541B1 Method for crystallization of low molecular weight polycarbonate and method for preparing polycarbonate resin from it 失效
标题翻译：低分子量聚碳酸酯的结晶方法及其制备聚碳酸酯树脂的方法
公开(公告)号：US06696541B1
公开(公告)日：2004-02-24
申请号：US10088590
申请日：2002-03-21
申请人： Tomonori Sakurai , Nobuaki Kido , Shunichi Matsumura , Toyoaki Ishiwata , Kazuteru Kohno , Hirotaka Suzuki , Hironori Haga , Toru Hikosaka
发明人： Tomonori Sakurai , Nobuaki Kido , Shunichi Matsumura , Toyoaki Ishiwata , Kazuteru Kohno , Hirotaka Suzuki , Hironori Haga , Toru Hikosaka
IPC分类号： C08G6400
CPC分类号： C08G64/20 , C08G64/40
摘要： A method for crystallizing a low molecular weight aromatic polycarbonate effectively and a method for preparing a polycarbonate resin having a desired intrinsic viscosity by using the polycarbonate crystallized with the above method of crystallization. A low molecular weight aromatic polycarbonate (preferably, the one produced by melt polycondensation) is crystallized by bringing it into contact with an aromatic monohydroxy compound or a mixture of said compound and water. Or, a low molecular weight aromatic polycarbonate is melt mixed with at least one or more kinds of compounds selected from the group consisting of aromatic monohydroxy compounds, carbonic acid diester compounds and aromatic dihydroxy compounds to crystallize the low molecular weight aromatic polycarbonate. The crystallized product is heated at a temperature lower than its melting point under reduced pressure or in an inert gas flow to convert it into a high polymerized state. Thus, a polycarbonate resin having a desired intrinsic viscosity is prepared.
摘要翻译：一种低分子量芳族聚碳酸酯的有效结晶方法以及通过使用通过上述结晶方法结晶的聚碳酸酯制备具有所需特性粘度的聚碳酸酯树脂的方法。低分子量芳族聚碳酸酯（优选通过熔体缩聚）通过使其与芳族单羟基化合物或所述化合物和水的混合物接触而结晶。或者，将低分子量芳族聚碳酸酯与至少一种选自芳族单羟基化合物，碳酸二酯化合物和芳族二羟基化合物的化合物熔融混合，以使低分子量芳族聚碳酸酯结晶。将结晶产物在低于其熔点的温度下在减压或惰性气体流中加热以将其转化为高聚合状态。因此，制备具有所需特性粘度的聚碳酸酯树脂。

5. 发明授权

US07407702B2 Polymetaphenylene isophthalamide-based polymer porous film, process for its production and battery separator 失效
标题翻译：聚邻苯二甲酰间苯二胺基聚合物多孔膜，其生产工艺及电池隔膜
公开(公告)号：US07407702B2
公开(公告)日：2008-08-05
申请号：US10776184
申请日：2004-02-12
申请人： Takao Ohno , Jiro Sadanobu , Tsutomu Nakamura , Susumu Honda , Toyoaki Ishiwata
发明人： Takao Ohno , Jiro Sadanobu , Tsutomu Nakamura , Susumu Honda , Toyoaki Ishiwata
IPC分类号： B32B5/22 , B01D39/14 , B05D1/22
CPC分类号： B32B27/08 , B01D67/0011 , B01D67/0016 , B01D69/02 , B01D69/141 , B01D71/56 , B01D2323/08 , B01D2323/12 , B01D2325/22 , B01D2325/24 , B32B27/18 , B32B27/304 , B32B27/34 , B32B27/36 , B32B38/0036 , B32B2305/026 , B32B2307/306 , B32B2307/724 , B32B2309/025 , B32B2377/00 , B32B2457/10 , C08J5/18 , C08J9/28 , C08J2201/0542 , C08J2377/10 , H01M2/1646 , H01M2/1653 , H01M2/166 , Y10T428/249978 , Y10T428/249979 , Y10T428/24998 , Y10T428/249981 , Y10T428/249986 , Y10T428/249991 , Y10T428/249992 , Y10T428/249993 , Y10T428/31725
摘要： A polymetaphenylene isophthalamide-based polymer porous film having a satisfactory porous structure that exhibits excellent gas permeability and heat resistance. It is produced by a process which comprises casting a dope of the polymetaphenylene isophthalamide-based polymer and coagulating it in a coagulating bath. The porous film may also contain inorganic whiskers, and a composite porous film may be formed in combination with a separate thermoplastic polymer film.
摘要翻译：具有令人满意的多孔结构的聚邻苯二甲酰间苯二胺系聚合物多孔膜具有优异的透气性和耐热性。它是通过一种方法生产的，该方法包括将聚邻苯二甲酰间苯二胺基聚合物的掺杂物浇铸并在凝固浴中凝结。多孔膜也可以含有无机晶须，并且复合多孔膜可以与单独的热塑性聚合物膜组合形成。

6. 发明申请

US20100285292A1 Aromatic Polyimide Film and Process for the Production Thereof 审中-公开
标题翻译：芳族聚酰亚胺薄膜及其制备方法
公开(公告)号：US20100285292A1
公开(公告)日：2010-11-11
申请号：US11887510
申请日：2006-03-27
申请人： Toyoaki Ishiwata , Jyuhou Matsuo , Nobuaki Kido
发明人： Toyoaki Ishiwata , Jyuhou Matsuo , Nobuaki Kido
IPC分类号： C08G73/10 , B32B27/28 , B29D7/01
CPC分类号： B29C41/24 , B29C55/143 , B29K2079/08 , C08G73/105 , C08G73/1071 , C08J5/18 , C08J2379/08 , C08L79/08
摘要： Disclosed is an aromatic polyimide film having specific elastic modulus and thermal expansion coefficient. Also disclosed is a method for producing such an aromatic polyimide film. Specifically disclosed is an aromatic polyimide film which is composed of an aromatic polyimide containing not less than 70 mol % of repeating units represented by the following formula (I): (I) while satisfying the following relations (1) and (2): CTEMD≦−11×MiMD+70 (1) CTETD≦−11×MiTD+70 (2) wherein CTEMD represents the in-plane thermal expansion coefficient (ppm·K−1) in the machine direction; CTETD represents the in-plane thermal expansion coefficient (ppm·K−1) in the transverse direction; MiMD represents the elastic modulus (GPa) in the machine direction; and MiTD represents the elastic modulus (GPa) in the transverse direction. Also specifically disclosed is a method for producing such an aromatic polyimide film.
摘要翻译：公开了具有比弹性模量和热膨胀系数的芳族聚酰亚胺膜。还公开了一种制备这种芳族聚酰亚胺膜的方法。具体公开了一种芳族聚酰亚胺膜，其由满足下列关系式（1）和（2）的含有不少于70摩尔％的由下式（I）表示的重复单元的芳族聚酰亚胺组成：（I）：CTEMD＆nlE ; -11×MiMD + 70（1）CTETD＆nlE; -11×MiTD + 70（2）其中CTEMD表示机器方向上的面内热膨胀系数（ppm·K-1） CTETD表示横向的面内热膨胀系数（ppm·K-1） MiMD表示机器方向的弹性模量（GPa） MiTD表示横向的弹性模量（GPa）。还具体公开了这种芳族聚酰亚胺膜的制造方法。

7. 发明授权

US10047478B2 Prepreg and method for manufacturing same 有权
公开(公告)号：US10047478B2
公开(公告)日：2018-08-14
申请号：US13981807
申请日：2012-03-21
申请人： Takaya Suzuki , Toyoaki Ishiwata , Yoshinori Suzuki , Hiroshi Numata
发明人： Takaya Suzuki , Toyoaki Ishiwata , Yoshinori Suzuki , Hiroshi Numata
IPC分类号： D06M15/55 , B29D7/01 , C08J5/24 , C08G59/50 , C08L63/00 , B29C70/50
摘要： The present invention provides a prepreg comprising: a primary pre-pregnant made of a reinforced fiber substrate and an epoxy resin composition containing at least epoxy resin and thermoplastic resin impregnated into the reinforcing fiber that forms the reinforced fiber substrate; and a surface layer made of epoxy resin composition containing at least an epoxy resin and an epoxy resin-soluble thermoplastic resin that dissolves in the epoxy resin, the surface layer being formed on one or both surfaces of the primary prepreg; the prepreg being characterized in that only one of either the epoxy resin composition of the primary prepreg or the epoxy resin composition of the surface layer contains a hardening agent for an epoxy resin.

8. 发明授权

US06646060B1 Resin composition containing crystalline polyimide 失效
标题翻译：含有结晶聚酰亚胺的树脂组合物
公开(公告)号：US06646060B1
公开(公告)日：2003-11-11
申请号：US09743408
申请日：2001-01-10
申请人： Kiyotsuna Toyohara , Toyoaki Ishiwata , Daisuke Ozaki , Jiro Sadanobu
发明人： Kiyotsuna Toyohara , Toyoaki Ishiwata , Daisuke Ozaki , Jiro Sadanobu
IPC分类号： C08G6948
CPC分类号： C08L67/02 , C08G73/1082 , C08L79/08 , Y10T428/31721
摘要： A resin composition containing a mixture produced by blending a crystalline polyamide expressed e.g. by formula (1) (in the formula, R1 is a bivalent organic aromatic group or aliphatic group having a carbon number of 2 to 30, optionally having substituent and optionally containing non-reactive groups such as ether group and aromatic group in the main chain, and Ar1 is an aromatic residue having a carbon number of 6 to 45 and optionally having substituent) with a thermoplastic polyester. The resin composition has excellent mechanical characteristics such as high elastic modulus, flow properties and heat-resistance and is suitable as a material for an electronic part for surface mounting.
摘要翻译：一种树脂组合物，其含有通过将结晶聚酰胺共混而制得的混合物，通式（1）（式中，R 1为二价有机芳香族基团或碳数为2〜30的脂肪族基，任选具有取代基且任选地含有非反应性基团，例如主链中的醚基和芳香族基团，Ar 1为碳原子数为6〜45，可以具有取代基的芳香族残基）与热塑性聚酯。树脂组合物具有优异的机械特性，例如高弹性模量，流动性和耐热性，并且适合作为用于表面安装的电子部件的材料。

9. 发明授权

US5853878A Elastic fiber, process for the same and polyester elastomer used thereof 失效
标题翻译：弹性纤维，与其相同的方法和使用的聚酯弹性体
公开(公告)号：US5853878A
公开(公告)日：1998-12-29
申请号：US704539
申请日：1996-09-12
申请人： Toyoaki Ishiwata , Jiro Sadanobu
发明人： Toyoaki Ishiwata , Jiro Sadanobu
IPC分类号： C08G63/672 , D01F6/86 , C08G63/66 , C08F20/00 , C08G63/00 , C08G63/02
CPC分类号： D01F6/86 , C08G63/672 , Y10T428/2913 , Y10T428/2969
摘要： The present invention relates to an elastic fiber of polyester elastomer mainly comprising the polyester elastomer further comprising aromatic polyester component as a hard segment and poly(alkyleneoxide)glycol having a number-average molecular weight of 500 to 5000 as a soft segment, wherein a residual elongation after 400 percent stretching does not exceed 100 percent. Made of the polyester elastomer comprising 1,2-bis�4-(2-hydroxyethyl)phenoxy!ethane as the diol component constituting said aromatic polyester component, or 1,4-benzenediethanol and ethyleneglycol as the diol component constituting said aromatic polyester component, the elastic fiber features excellent elastic properties in the event of great deformation and provides suitable material for clothing.
摘要翻译： PCT No.PCT / JP96 / 00729 Sec。 371日期：1996年9月12日 102（e）1996年9月12日PCT PCT 1996年3月21日PCT公布。 WO96 / 30427PC PCT出版物日期：1996年10月3日本发明涉及一种聚酯弹性体弹性纤维，主要由聚酯弹性体构成，该聚酯弹性体还包含作为硬链段的芳族聚酯组分和数均分子量为500〜5000的聚（环氧烷）二醇作为软质其中400％拉伸后的残余伸长率不超过100％。由构成所述芳香族聚酯成分的二醇成分的1,2-双[4-（2-羟乙基）苯氧基]乙烷或作为构成所述芳香族聚酯成分的二醇成分的1,4-苯二乙醇和乙二醇的聚酯弹性体构成，弹性纤维在大变形的情况下具有优异的弹性，并为衣服提供合适的材料。

10. 发明申请

US20110111663A1 EPOXY RESIN COMPOSITION AND PREPREG USING THE SAME 审中-公开
标题翻译：环氧树脂组合物和使用它的预制物
公开(公告)号：US20110111663A1
公开(公告)日：2011-05-12
申请号：US13001375
申请日：2009-06-06
申请人： Hironori Kawamoto , Toyoaki Ishiwata
发明人： Hironori Kawamoto , Toyoaki Ishiwata
IPC分类号： B32B27/04 , C08G59/00 , B32B27/38
CPC分类号： C08J5/24 , C08G59/5033 , C08J2363/00 , C08K5/18 , C08K5/29 , C08L13/00 , C08L63/00 , Y10T442/20 , Y10T442/2951 , Y10T442/645
摘要： Disclosed is an epoxy resin composition comprising at least component [A]: a glycidyl-amino-group-containing polyfunctional epoxy resin, component [B]: an epoxy resin other than the component [A], component [C]: a polyisocyanate compound, component [D]: an aromatic-amine-based curing agent, and component [E]: a thermoplastic resin, characterized in that the epoxy resin composition has an epoxy group concentration of 0.67 to 1.51 Eq/kg of the total amount of the components [A] to [D], and preferably that the component [E] is in a proportion of 10 to 50% by weight of the total epoxy resin composition. Use of a prepreg having the resin composition as a matrix resin makes it possible to obtain a composite material with excellent heat resistance and wet heat resistance together with high mechanical properties.
摘要翻译：公开了至少含有成分[A]：含缩水甘油基氨基的多官能环氧树脂，成分[B]：除[A]成分以外的环氧树脂，成分[C]的成分的环氧树脂组合物：多异氰酸酯化合物，成分[D]：芳香族胺系固化剂，[E]成分：热塑性树脂，其特征在于，所述环氧树脂组合物的环氧基浓度为0.67〜1.51 组分[A]至[D]，优选组分[E]的比例为总环氧树脂组合物的10至50重量％。使用具有树脂组合物的预浸料作为基质树脂使得可以获得具有优异的耐热性和耐湿热性以及高机械性能的复合材料。

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