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1. 发明授权

US06841650B2 Crystallizable poly (2,5-di-substituted-1,4-phenylene oxide) and a method of preparing the same 有权
标题翻译：可结晶的聚（2,5-二取代-1,4-亚苯基氧化物）及其制备方法
公开(公告)号：US06841650B2
公开(公告)日：2005-01-11
申请号：US10157862
申请日：2002-05-31
申请人： Hideyuki Higashimura , Kiyoshi Fujisawa , Yoshihiko Moro-Oka , Shiro Kobayashi
发明人： Hideyuki Higashimura , Kiyoshi Fujisawa , Yoshihiko Moro-Oka , Shiro Kobayashi
IPC分类号： C08G65/44 , C08G59/50
CPC分类号： C08G65/44
摘要： There is disclosed a crystallizable poly(2,5-di-substituted-1,4-phenylene oxide), which exhibits an exothermic peak for crystallization of not less than 5 J/g at 150° C. or over when cooled after melting, and/or an endothermic peak, at the time of melting of crystals thereof, of not less than 5 J/g at 150° C. or over when re-heated after cooling of the melt, and which comprises a recurring unit of the following formula (I), and a method of preparing the same by polymerization of a 2,5-di-substituted-phenol of the following formula (II) by use of a copper complex catalyst made of a tridentate ligand of which nitrogen atoms coordinate to a copper atom in coexistence with oxygen: wherein R1's independently represent a hydrocarbon group or a substituted hydrocarbon group, and they may be the same or different. The crystallizable poly(2,5-di-substituted-1,4-phenylene oxide) is able to provide a melt molding which has a reduced degree of coloration and good heat resistance.
摘要翻译：公开了一种可结晶的聚（2,5-二取代-1,4-亚苯基氧化物），其在熔化后冷却时在150℃或更高温度下表现出不低于5J / g的结晶放热峰，和/或其结晶时的吸热峰在熔融物冷却后再加热时在150℃以上不低于5J / g，并且其包含以下的重复单元式（I）的方法和通过使用由氮原子配位的三齿配体构成的铜络合物催化剂聚合下述式（II）的2,5-二取代苯酚而制备的方法与氧共存的铜原子：其中R 1独立地表示烃基或取代的烃基，它们可以相同或不同。可结晶的聚（2,5-二取代-1,4-亚苯基氧化物）能够提供具有降低的着色程度和良好的耐热性的熔融模塑。

2. 发明授权

US06576800B2 Oxidation polymer of a substituted phenol 失效
标题翻译：取代苯酚的氧化聚合物
公开(公告)号：US06576800B2
公开(公告)日：2003-06-10
申请号：US09905978
申请日：2001-07-17
申请人： Hideyuki Higashimura , Shiro Kobayashi
发明人： Hideyuki Higashimura , Shiro Kobayashi
IPC分类号： C07C4100
CPC分类号： C08G65/44
摘要： An oxidation polymer of a substituted phenol, obtained by oxidative polymerization of at least one compound selected from the group consisting of a compound of formula (Ia) and a compound of formula (Ib), in which the oxidation polymer has a number-average polymerization degree of 3 or more: wherein R1 to R4 each represent a hydrogen atom and the like; provided that at least one of R1 to R4 represents a substituted or unsubstituted, saturated hydrocarbon group having 10 or more carbon atoms, and R1 and/or R4 represent a hydrogen atom; wherein R11 represents a substituted or unsubstituted, saturated hydrocarbon group having 15 or more carbon atoms, and R12 is the same as R11, or when R12 is different from R11, R12 represents a substituted or unsubstituted hydrocarbon group and the like.
摘要翻译：通过氧化聚合至少一种选自式（Ia）化合物和式（Ib）化合物的化合物的化合物获得的取代苯酚的氧化聚合物，其中氧化聚合物具有数均聚合 3以上：其中，R1〜R4各自表示氢原子等; 条件是R 1至R 4中的至少一个表示具有10个或更多个碳原子的取代或未取代的饱和烃基，R 1和/或R 4表示氢原子;其中R 11表示取代或未取代的饱和烃基，其具有15或更多的碳原子，R 12与R 11相同，或者当R 12与R 11不同时，R 12表示取代或未取代的烃基等。

3. 发明授权

US07161000B2 Method for producing phenol condensate 有权
标题翻译：生产苯酚缩合物的方法
公开(公告)号：US07161000B2
公开(公告)日：2007-01-09
申请号：US10854334
申请日：2004-05-27
申请人： Hideyuki Higashimura , Eiichi Kotake , Masaaki Kubota , Shiro Kobayashi
发明人： Hideyuki Higashimura , Eiichi Kotake , Masaaki Kubota , Shiro Kobayashi
IPC分类号： C07D225/00 , C07C39/12
CPC分类号： C07C49/753 , C07C45/39
摘要： Provided is a method for producing a phenol condensate by oxidative condensation of a phenol compound not having a substituted group on at least one ortho-position, in the presence of a specific complex (II) and oxygen, wherein a condensate coupled at para-position of the phenol can be produced in an excellent yield, L-M (X)n (II) wherein L represents a ligand having 2 to 4 nitrogen atoms as donor atoms, M represents copper ion, nickel ion, cobalt ion, iron ion, manganese ion, chromium ion or vanadyl ion, X represents a counter ion, n is a number of Xs.
摘要翻译：本发明提供一种通过在特定络合物（II）和氧气存在下，在至少一个邻位的不具有取代基的酚化合物进行氧化缩合来制备苯酚缩合物的方法，其中在对位可以以优异的产率制备苯酚，<？在线公式描述=“在线公式”end =“lead”？> LM（X）n（II）其中L表示作为供体原子的具有2〜4个氮原子的配体，M表示铜离子，镍离子，钴离子，铁离子，锰离子，铬离子或氧离子离子，X表示抗衡离子，n是X的数量。

4. 发明授权

US06541596B1 Crystallizable poly (2,5-di-substituted-1,4-phenylene oxide) and a method of preparing the same 失效
标题翻译：可结晶的聚（2,5-二取代-1,4-亚苯基氧化物）及其制备方法
公开(公告)号：US06541596B1
公开(公告)日：2003-04-01
申请号：US09496268
申请日：2000-02-01
申请人： Hideyuki Higashimura , Kiyoshi Fujisawa , Yoshihiko Moro-oka , Shiro Kobayashi
发明人： Hideyuki Higashimura , Kiyoshi Fujisawa , Yoshihiko Moro-oka , Shiro Kobayashi
IPC分类号： C08G5950
CPC分类号： C08G65/44
摘要： There is disclosed a crystallizable poly(2,5-di-substituted-1,4-phenylene oxide), which exhibits an exothermic peak for crystallization of not less than 5 J/g at 150° C. or over when cooled after melting, and/or an endothermic peak, at the time of melting of crystals thereof, of not less than 5 J/g at 150° C. or over when re-heated after cooling of the melt, and which comprises a recurring unit of the following formula (I), and a method of preparing the same by polymerization of a 2,5-di-substituted-phenol of the following formula (II) by use of a copper complex catalyst made of a tridentate ligand of which nitrogen atoms coordinate to a copper atom in coexistence with oxygen: wherein R1's independently represent a hydrocarbon group or a substituted hydrocarbon group, and they may be the same or different. The crystallizable poly(2,5-di-substituted-1,4-phenylene oxide) is able to provide a melt molding which has a reduced degree of coloration and good heat resistance.
摘要翻译：公开了一种可结晶的聚（2,5-二取代-1,4-亚苯基氧化物），其在熔化后冷却时在150℃或更高温度下表现出不低于5J / g的结晶放热峰，和/或其结晶时的吸热峰在熔融物冷却后再加热时在150℃以上不低于5J / g，并且其包含以下的重复单元式（I）的方法和通过使用由氮原子配位的三齿配体构成的铜络合物催化剂聚合下述式（II）的2,5-二取代苯酚而制备的方法与氧共存的铜原子：其中R1独立地表示烃基或取代的烃基，它们可以相同或不同。可结晶的聚（2,5-二取代-1,4-亚苯基氧化物）能够提供具有降低的着色程度和良好的耐热性的熔融模塑。

5. 发明授权

US06383636B2 (2,5-disubstituted-1,4-phenylene oxide) block or graft copolymer 有权
标题翻译：（2,5-二取代-1,4-亚苯基氧化物）嵌段或接枝共聚物
公开(公告)号：US06383636B2
公开(公告)日：2002-05-07
申请号：US09818758
申请日：2001-03-28
申请人： Hideyuki Higashimura , Shuhei Namekawa , Shiro Kobayashi
发明人： Hideyuki Higashimura , Shuhei Namekawa , Shiro Kobayashi
IPC分类号： B32B1502
CPC分类号： C08G65/485 , C08G61/12 , C08L71/123 , Y10T428/2982 , C08L2666/04
摘要： There is disclosed a (2,5-disubstituted-1,4-phenylene oxide) block copolymer which comprises one or more block structural units represented by formula (I) and at least one particular divalent structural unit in a molecule. There is also disclosed a (2,5-disubstituted-1,4-phenylene oxide) graft polymer which comprises one or more structural units of formula (IV), or three or more of structural unit of formula (IV) and particular divalent structural unit, in a molecule. (wherein R1 represents an unsubstituted or substituted hydrocarbon group, and the two R1s may be the same or different; a represents a number average degree of polymerization and is 5 or more; R4 represents a trifunctional unsubstituted or substituted hydrocarbon group; U represents —CO—, —OCO—, or —NHCO—; and f is 1 or 0.)
摘要翻译：公开了一种（2,5-二取代-1,4-亚苯基氧化物）嵌段共聚物，其包含一个或多个由式（I）表示的嵌段结构单元和分子中至少一个特定的二价结构单元。还公开了一种（2,5-二取代-1,4-亚苯基氧化物）接枝聚合物，其包含一种或多种式（IV）的结构单元，或三种或更多种式（IV）的结构单元和特定的二价结构单元，其中R1表示未取代或取代的烃基，两个R 1可以相同或不同; a表示数均聚合度，为5以上; R 4表示三官能的未取代或取代的烃基团; U表示-CO-，-OCO-或-NHCO-; f为1或0）

6. 发明授权

US09704612B2 Composition of silver-conjugated compound composite 有权
公开(公告)号：US09704612B2
公开(公告)日：2017-07-11
申请号：US14005099
申请日：2012-03-15
申请人： Takayuki Iijima , Hideyuki Higashimura
发明人： Takayuki Iijima , Hideyuki Higashimura
IPC分类号： H01B1/00 , H01B1/12 , B22F1/00 , B22F1/02 , C22C5/06 , H01B1/22 , C08K3/08 , H01B1/02 , H01L51/00 , H01L51/50
CPC分类号： H01B1/121 , B22F1/0003 , B22F1/02 , C08G2261/91 , C08G2261/95 , C08K3/08 , C22C5/06 , H01B1/02 , H01B1/22 , H01L51/0035 , H01L51/0039 , H01L51/0043 , H01L51/5076 , C08K5/098 , C08L65/00
摘要： A composition of a silver-conjugated compound composite containing (1) a silver-conjugated compound composite containing a silver particle with a Feret diameter of 1,000 nm or less and a conjugated compound having a weight average molecular weight of 3.0×102 or more being adsorbed to the silver particles and (2) an ionic compound. The ionic compound may be a compound having a structure represented by the following Formula (hh-1): [Chem. 1] Mm′+aX′n′−b (hh-1) wherein Mm′+ represents a metal cation, X′n′− represents an anion, a and b each independently represent an integer of 1 or more, and when Mm′+ and X′n′− are each plurally present, they may be the same as or different from each other.

7. 发明授权

US09184388B2 Layered structure, electronic device using same, aromatic compound, and method for manufacturing said compound 有权
标题翻译：层状结构，使用其的电子器件，芳族化合物，以及所述化合物的制造方法
公开(公告)号：US09184388B2
公开(公告)日：2015-11-10
申请号：US13812678
申请日：2011-07-29
申请人： Arihiro Yashiro , Hideyuki Higashimura , Rui Ishikawa , Masanobu Tanaka
发明人： Arihiro Yashiro , Hideyuki Higashimura , Rui Ishikawa , Masanobu Tanaka
IPC分类号： H01L51/50 , H01L51/00 , C07C211/56 , C07C211/63 , C07F9/54 , C07F9/572 , C08G61/12 , C07D209/86 , C07F5/02
CPC分类号： H01L51/0035 , C07C211/56 , C07C211/63 , C07D209/86 , C07F5/025 , C07F9/5407 , C07F9/5442 , C07F9/5456 , C07F9/5728 , C08G61/12 , C08G2261/1424 , C08G2261/312 , C08G2261/3162 , C08G2261/411 , C08G2261/512 , C08G2261/91 , C08G2261/92 , C08G2261/95 , H01L51/5056 , Y02E10/549 , Y02P70/521
摘要： The present invention provides: a layered structure having a substrate and a hole injection and/or hole transport layer comprising an aromatic compound having, on a side chain, at least one type of group having a cationic center; an electronic device having the layered structure; an aromatic compound having, on a hydrocarbon side chain, at least one type of group having a cationic center; an aromatic compound having a leaving group on a hydrocarbon side chain; and a method for manufacturing the aromatic compound having, on a hydrocarbon side chain, at least one type of group having a cationic center, the method comprising reacting the aromatic compound having a leaving group on a hydrocarbon side chain with a specific nitrogen compound, phosphorus compound, sulfur compound, or a combination of two or more of these compounds, thereby converting the aromatic compound into an onium salt thereof. When used as an electronic device material, and particularly as a hole transport and/or hole injection material, the aromatic compound can achieve a higher current density at a given voltage.
摘要翻译：本发明提供：具有基材和空穴注入和/或空穴传输层的层状结构，所述空穴注入和/或空穴传输层包含芳族化合物，所述芳族化合物在侧链上具有至少一种具有阳离子中心的基团; 具有层状结构的电子设备; 在烃侧链上具有至少一种具有阳离子中心的基团的芳族化合物; 在烃侧链上具有离去基团的芳族化合物; 以及在烃侧链具有至少一种具有阳离子中心的基团的芳香族化合物的制造方法，其特征在于，使烃侧链上具有离去基团的芳香族化合物与特定的氮化合物反应，化合物，硫化合物或两种或更多种这些化合物的组合，从而将芳族化合物转化成其鎓盐。当用作电子器件材料，特别是用作空穴传输和/或空穴注入材料时，芳族化合物可以在给定电压下实现更高的电流密度。

8. 发明授权

US08951646B2 Layered structure comprising a layer containing a conjugated polymer compound 有权
标题翻译：包含含有共轭高分子化合物的层的层状结构
公开(公告)号：US08951646B2
公开(公告)日：2015-02-10
申请号：US12921108
申请日：2009-03-05
申请人： Masanobu Tanaka , Kenta Tanaka , Shohgo Yamauchi , Hideyuki Higashimura
发明人： Masanobu Tanaka , Kenta Tanaka , Shohgo Yamauchi , Hideyuki Higashimura
IPC分类号： H01L51/54 , C09K11/06 , C08G63/00 , H01L51/00 , C08G61/02 , C08G61/12 , H01L51/50
CPC分类号： H01L51/0039 , C08G61/02 , C08G61/12 , C08G61/122 , C08G2261/124 , C08G2261/1426 , C08G2261/3142 , C08G2261/316 , C08G2261/3221 , C08G2261/5222 , C08G2261/80 , H01L51/5048 , Y02E10/549 , Y10S428/917
摘要： A layered structure including a first electrode and a second electrode, a light-emitting layer or a charge separation layer between the first electrode and the second electrode, and a layer containing a conjugated polymer compound between the light-emitting layer or the charge separation layer and the first electrode, wherein the conjugated polymer compound contains a repeating unit selected from the group consisting of a repeating unit of formula (1).
摘要翻译：包括第一电极和第二电极的层状结构，在第一电极和第二电极之间的发光层或电荷分离层，以及在发光层或电荷分离层之间含有共轭高分子化合物的层和第一电极，其中共轭高分子化合物含有选自式（1）的重复单元的重复单元。

9. 发明申请

US20130099224A1 LIGHT-EMITTING DEVICE AND PHOTOVOLTAIC CELL, AND METHOD FOR MANUFACTURING THE SAME 有权
标题翻译：发光装置和光电池及其制造方法
公开(公告)号：US20130099224A1
公开(公告)日：2013-04-25
申请号：US13807226
申请日：2011-06-24
申请人： Takayuki Iljima , Kenta Tanaka , Masanobu Tanaka , Hideyuki Higashimura
发明人： Takayuki Iljima , Kenta Tanaka , Masanobu Tanaka , Hideyuki Higashimura
IPC分类号： H01L51/50 , H01L51/00 , H01L51/42
CPC分类号： H01L51/5012 , C07D471/04 , C08G61/02 , C08G2261/1424 , C08G2261/1426 , C08G2261/149 , C08G2261/3142 , C08G2261/411 , C08G2261/412 , C08G2261/95 , H01L51/0002 , H01L51/0003 , H01L51/0037 , H01L51/0039 , H01L51/42 , H01L51/424 , H01L51/4253 , H01L51/5076 , H01L51/5092 , H05B33/22 , Y02E10/549 , Y02P70/521
摘要： Provided are a light-emitting device and a photovoltaic cell having excellent characteristics. A light-emitting device (10) includes a cathode (34), an anode (32), a light-emitting layer (50) interposed between the cathode (34) and the anode (32), and an electron injection layer (44) provided between the cathode (34) and the light-emitting layer (50) and connected to the cathode (34), in which at least one of the anode (32) and the cathode (34) contains a conductive material having an aspect ratio of 1.5 or more, and the electron injection layer (44) contains an organic compound having at least one of an ionic group and a polar group.
摘要翻译：提供了具有优异特性的发光器件和光伏电池。发光装置（10）包括阴极（34），阳极（32），介于阴极（34）和阳极（32）之间的发光层（50）和电子注入层（44））设置在阴极（34）和发光层（50）之间并连接到阴极（34），其中阳极（32）和阴极（34）中的至少一个包含具有一方面的导电材料比例为1.5以上，电子注入层（44）含有具有离子性基团和极性基团中的至少一种的有机化合物。

10. 发明申请

US20120168693A1 SILVER-(CONJUGATED COMPOUND) COMPOSITE 有权
标题翻译：银（复合）复合材料
公开(公告)号：US20120168693A1
公开(公告)日：2012-07-05
申请号：US13496611
申请日：2010-09-17
申请人： Takayuki Iijima , Masahiro Fujioka , Hideyuki Higashimura
发明人： Takayuki Iijima , Masahiro Fujioka , Hideyuki Higashimura
IPC分类号： H01B1/02 , C08G79/00 , C08G73/06
CPC分类号： H01B1/22 , B22F1/00 , B22F1/0062 , B22F1/02 , B22F9/00 , B22F9/24 , B22F2001/0092 , B82Y30/00 , C08G73/06 , C08G79/00 , C08G2261/1424 , C08G2261/1432 , C08G2261/148 , C08G2261/3142 , C08G2261/3162 , C08G2261/514 , C08G2261/95 , C08K3/08 , C08L65/00 , H01B1/00
摘要： A silver-(conjugated compound) composite comprising silver particles having a number-average Feret diameter of not more than 1,000 nm, and a conjugated compound having a weight-average molecular weight of not less than 3.0×102 adsorbed to the silver particles. The composite exhibits excellent conductivity and charge injection properties, and excellent dispersibility within non-polar solvents.
摘要翻译：包含平均Feret直径不大于1000nm的银颗粒的银 - （共轭化合物）复合物和吸附在银颗粒上的重均分子量不小于3.0×102的共轭化合物。该复合材料具有优异的导电性和电荷注入性能，并且在非极性溶剂中具有优异的分散性。

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