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1. 发明授权

US4997911A Method of recovering polymer agglomerates as dry powders or granules 失效
标题翻译：以干燥粉末或颗粒形式回收聚合物附聚物的方法
公开(公告)号：US4997911A
公开(公告)日：1991-03-05
申请号：US241178
申请日：1988-09-07
申请人： Hideo Yasui , Wataru Okada , Yasuhiro Miki , Toragoro Mitani
发明人： Hideo Yasui , Wataru Okada , Yasuhiro Miki , Toragoro Mitani
IPC分类号： C08F6/22 , C08J3/16
CPC分类号： C08J3/16 , C08F6/22
摘要： The present invention provides a method for recovering polymer agglomerates in the form of dry powders or granules comprising steps of:(A) coagulating a polymer latex obtained by emulsion polymerization or suspension polymerization to thereby form hydrous agglomerates in which latex particles are not fused together,(B) immersing the hydrous agglomerates in an organic liquid insoluble or hardly soluble in water which wets but does not dissolve or swell said agglomerates at a temperature lower than the temperature at which the latex particles constituting the agglomerates are fused together, to thereby substitute said organic liquid for the water contained in the agglomerates with the organic liquid,(C) thereby forming two phases; a water phase expelled from the agglomerates and an organic liquid phase in which the agglomerates are immersed,(D) separating the agglomerates from the organic liquid phase, and(E) removing by evaporation the organic liquid attached to the agglomerates, whereby the agglomerates are recovered as dry particles. Further, this invention provides a method of recovering polymer agglomerates having additional impurities removed therefrom by immersing the aforementioned agglomerates, after having been separated from the organic liquid phase, in a second organic liquid which effects dissolution and extraction of impurities from the aforementioned agglomerates. According to this invention, the drying energy may be greatly cut back, and high purity polymer agglomerates are obtained in the form of dry powders or granules.

2. 发明授权

US4904309A Chemical cleaning method of the interior of polymerization reactor 失效
标题翻译：聚合反应器内部的化学清洗方法
公开(公告)号：US4904309A
公开(公告)日：1990-02-27
申请号：US263956
申请日：1988-10-26
申请人： Takamichi Komabashiri , Toragoro Mitani , Hiroaki Yamauchi , Hideo Yasui
发明人： Takamichi Komabashiri , Toragoro Mitani , Hiroaki Yamauchi , Hideo Yasui
IPC分类号： C11D3/02 , C11D3/06 , C11D3/08 , C11D3/10
CPC分类号： C11D11/0041 , C11D3/044 , C11D3/06 , C11D3/08 , C11D3/10
摘要： A chemical cleaning method for removing scales and other substances deposited on the interior of a polymerization reactor used in emulsion polymerization or suspension polymerization. This method comprises chemically cleaning the interior using an aqueous solution or dispersion of an alkali agent and a surfactant. According to this method of cleaning, scales deposited on the interior of a polymerization reactor, in particular, scales deposited during polymerization on the inside surface, an agitator and baffle-plates of the reactor are completely removed.
摘要翻译：用于除去沉积在用于乳液聚合或悬浮聚合的聚合反应器内部的垢和其它物质的化学清洗方法。该方法包括使用碱剂和表面活性剂的水溶液或分散体对内部进行化学清洗。根据这种清洁方法，沉积在聚合反应器内部的鳞片，特别是聚合过程中沉积的鳞片在内表面上，反应器的搅拌器和挡板被完全去除。

3. 发明授权

US4863524A Method of cleaning the interior of polymerization reactor 失效
标题翻译：清洗聚合反应器内部的方法
公开(公告)号：US4863524A
公开(公告)日：1989-09-05
申请号：US241771
申请日：1988-09-07
申请人： Takamichi Komabashiri , Toragoro Mitani , Hiroaki Yamauchi , Hideo Yasui
发明人： Takamichi Komabashiri , Toragoro Mitani , Hiroaki Yamauchi , Hideo Yasui
IPC分类号： C08F6/00 , B01J19/00 , C11D3/08 , C11D3/10 , C11D3/43 , C11D17/00
CPC分类号： C11D3/43 , B01J19/002 , C11D10/04 , C11D3/08 , C11D3/10 , B01J2219/00252
摘要： A cleaning method for removing scales, etc., deposited on the interior of a polymerization reactor which has been used in emulsion or suspension polymerization. This method uses a chemical cleanser comprising a soap builder an, alkali agent, an aqueous solution or dispersion of a surfactant, and an organic solvent and/or polymerizable monomer. This system may further contain a plastic packing such as tellerettes. By this method, scales deposited on the interior of a polymerization reactor, particularly, scales deposited on the inside surface, agitator, and baffle-plates of the reactor, are compeltely removed.
摘要翻译：一种用于去除已经用于乳液或悬浮聚合的聚合反应器内部沉积的鳞屑等的清洁方法。该方法使用包含肥皂助剂a，碱剂，表面活性剂的水溶液或分散体以及有机溶剂和/或可聚合单体的化学清洁剂。该系统可以进一步包含塑料包装，例如tellerettes。通过该方法，沉积在聚合反应器内部的鳞片，特别是沉积在反应器的内表面，搅拌器和挡板上的鳞片被强制去除。

4. 发明授权

US4805650A Apparatus for cleaning a tank-like vessel 失效
标题翻译：用于清洗罐状容器的装置
公开(公告)号：US4805650A
公开(公告)日：1989-02-21
申请号：US46366
申请日：1987-05-06
申请人： Hideo Yasui , Toragoro Mitani , Takamichi Komabashiri
发明人： Hideo Yasui , Toragoro Mitani , Takamichi Komabashiri
IPC分类号： B08B9/08 , B08B9/093 , B08B3/04 , B66C13/18
CPC分类号： B08B9/093
摘要： An apparatus for cleaning a tank-like vessel comprising(a) a supporting arm attached to a fixing plate, which can perpendicularly extend downward,(b) a folding arm of which base portion is rotatably attached to the lower end of the supporting arm, a position of the folding arm being changeable between a housed position and a position in use wherein the folding arm is approximately horizontally stretched out,(c) a rope winded up and winded down by a hoist, and(d) a cleaning nozzle capable of injecting jet water in a two-dimensional direction or three-dimensional direction.
摘要翻译：一种用于清洁罐状容器的装置，包括：（a）附接到固定板的支撑臂，其可以垂直向下延伸;（b）折叠臂，其基部可旋转地附接到支撑臂的下端，折叠臂的位置可在容纳位置和使用中的位置之间改变，其中折叠臂大致水平地伸展，（c）绳索由起重机卷起并卷起，以及（d）能够在二维方向或三维方向注射射流水。

5. 发明授权

US4517344A Process for polymerization of acrylate or methacrylate 失效
标题翻译：丙烯酸酯或甲基丙烯酸酯聚合方法
公开(公告)号：US4517344A
公开(公告)日：1985-05-14
申请号：US634067
申请日：1984-07-25
申请人： Toragoro Mitani , Hideo Yasui , Hisashi Morikawa
发明人： Toragoro Mitani , Hideo Yasui , Hisashi Morikawa
IPC分类号： C08F2/00 , C08F20/12
CPC分类号： C08F2/004 , C08F20/12
摘要： In a process of emulsion-polymerization in a polymerization system containing an acrylate or a methacrylate monomer at least 60%; the improvement which comprises carrying out the emulsion polymerization in a polymerization vessel having a film of a quinone-amine compound of not less than 3000 in average molecular weight on the inner vessel wall, said quinone-amine compound being prepared by addition-reacting an aromatic quinone and an aromatic diamine in a solvent medium having a solubility parameter of 9.0 to 12.2. According to the process, the polymer scale deposition can be prevented in the acrylate or methacrylate polymerization system.
摘要翻译：在含有至少60％的丙烯酸酯或甲基丙烯酸酯单体的聚合体系中进行乳液聚合的方法; 所述改进包括在内容器壁上具有平均分子量为3000以上的醌 - 胺化合物的聚合容器中的乳液聚合，所述醌 - 胺化合物通过将芳族化合物醌和芳族二胺在溶剂介质中的溶解度参数为9.0〜12.2。根据该方法，可以在丙烯酸酯或甲基丙烯酸酯聚合体系中防止聚合物垢沉积。

6. 发明授权

US4713443A Process for removing organic compound having high boiling point from a floatable polymer 失效
标题翻译：从可漂浮聚合物中除去具有高沸点的有机化合物的方法
公开(公告)号：US4713443A
公开(公告)日：1987-12-15
申请号：US809107
申请日：1985-12-16
申请人： Toshimitsu Nakashima , Wataru Okada , Toragoro Mitani
发明人： Toshimitsu Nakashima , Wataru Okada , Toragoro Mitani
IPC分类号： C08F6/00 , C08F6/24
CPC分类号： C08F6/00
摘要： A process for removing an organic compound having a high boiling point from a floatable polymer containing the organic compound, which comprises contacting a slurry of the polymer with a non-condensable gas at a high temperature by strongly agitating with an agitator at an impeller Reynolds number of not less than 10.sup.5. According to the process, the organic compound having a high boiling point can be readily removed down to not more than 10 ppm.
摘要翻译：一种从含有有机化合物的可漂浮聚合物中除去具有高沸点的有机化合物的方法，该方法包括通过用搅拌器在叶轮上强烈搅拌将聚合物的浆料与不可冷凝气体在高温下接触。雷诺数不低于105.根据该方法，可以容易地将具有高沸点的有机化合物除去至不超过10ppm。

7. 发明授权

US4970278A Method of preventing polymer scale deposition 失效
标题翻译：防止聚合物垢沉积的方法
公开(公告)号：US4970278A
公开(公告)日：1990-11-13
申请号：US270997
申请日：1988-11-14
申请人： Takamichi Komabashiri , Masahiro Tsujinaka , Toragoro Mitani
发明人： Takamichi Komabashiri , Masahiro Tsujinaka , Toragoro Mitani
IPC分类号： C08F2/00 , C08G73/02
CPC分类号： C08F2/004
摘要： Polymer scale deposition on polymerization reactor inside surfaces in the polymerization of a monomer or monomers having an ethylenic double bond and/or a monomer or monomers having diolefinic double bonds is prevented, peelability or removability of polymer scales deposited on such surface, if any, is improved and the scale inhibitor adherence to the wall surface of glass-lined polymerization reactors is improved by coating the inside surfaces of the reactor in advance with a coating composition comprising a quinone-amine compound having a molecular weight of at least 3,000 as obtained by subjecting at least one aromatic diamine and at least one aromatic quinone to addition reaction in at least one solvent having a solubility parameter of 8.5 to 24.0 and/or a reduced form of said quinone-amine compound and at least one silica organosol or a mixture of at least one silica organosol and at least one alkyl silicate to thereby form a hydrophilic coat film on the surfaces.

8. 发明授权

US4795800A Scale deposition preventing agent 失效
标题翻译：鳞屑沉积防止剂
公开(公告)号：US4795800A
公开(公告)日：1989-01-03
申请号：US52392
申请日：1987-05-21
申请人： Hiroaki Yamauchi , Toragoro Mitani , Takamichi Komabashiri
发明人： Hiroaki Yamauchi , Toragoro Mitani , Takamichi Komabashiri
IPC分类号： C08F2/00 , C08F20/00 , C08F20/10 , C08F20/12 , C08G73/02 , C08G12/00
CPC分类号： C08F20/12 , C08F2/004
摘要： A process for preparing a scale deposition preventing agent of a quinone-amine compound suitable for use in a polymerization of acrylic or methacrylic acid ester monomers, which comprises (A) subjecting an aromatic quinone and an aromatic diamine to addition reaction in a solvent having a solubility parameter of 8.5 to 24.0 to give an addition product, and (B) converting the addition product into a high molecular weight compound within 24 hours after beginning the addition reaction (A) by adding an oxidizing agent to the addition reaction mixture or by subjecting the addition reaction mixture to anodic oxidation with an electrode to give a quinone-amine compound. According to the present invention, the preparation rate of the scale deposition preventing agent of the quinone-amine compound can be remarkably increased, the yield can be increased, and the obtained compound has excellent properties.

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