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1. 发明授权

US5702580A Measuring sensor for determining the oxygen content of gas mixtures 失效
标题翻译：用于测定气体混合物氧含量的测量传感器
公开(公告)号：US5702580A
公开(公告)日：1997-12-30
申请号：US617873
申请日：1996-03-21
申请人： Hermann Dietz , Werner Gruenwald , Claudio De La Prieta , Gert Lindemann , Ulrich Eisele , Carmen Schmiedel
发明人： Hermann Dietz , Werner Gruenwald , Claudio De La Prieta , Gert Lindemann , Ulrich Eisele , Carmen Schmiedel
IPC分类号： G01N27/41 , G01N27/417 , G01N27/419 , G01N27/407
CPC分类号： G01N27/417
摘要： A measuring sensor for determining oxygen content in a gas mixture including exhaust gases of internal combustion engines, includes a base substrate which is comprised of a base material and which is electrically insulating; and an electrochemical measuring probe and an electrochemical reference probe arranged separate from each other on the base substrate. The measuring probe includes at least one internal electrode; at least one solid electrolyte island; and at least one external electrode. The measuring probe additionally includes a diffusion barrier. Further base material layers composed of the base material are provided so as to embed at least the diffusion barrier, the at least one internal electrodes for the measuring probe and the internal electrode for the reference probe. A diffusion hole is defined between the measuring probe and the reference probe which extends from the base substrate through the diffusion barrier and respective base material layers, and out to the gas mixture to be measured. Thermal stress and the accompanying tendency to cracking is reduced by providing the solid electrolyte as islands. Separate disposition of the measuring probe and the reference probe, i.e., without a common electrode, permits construction as individual layers using, for example, screen printing.
摘要翻译： PCT No.PCT / DE95 / 01305 Sec。 371日期1996年3月21日 102（e）日期1996年3月21日PCT提交1995年9月22日PCT公布。公开号WO96 / 11394 日期1996年04月18日用于测定包括内燃机废气的气体混合物中的氧含量的测量传感器包括由基材构成并且是电绝缘的基底，以及在基底基板上彼此分离设置的电化学测量探针和电化学参考探针。测量探头包括至少一个内部电极; 至少一个固体电解质岛; 和至少一个外部电极。测量探头还包括扩散阻挡层。提供由基材构成的其他基材层，以便至少嵌入扩散阻挡层，至少一个用于测量探针的内部电极和用于参考探针的内部电极。在测量探针和参考探针之间限定了扩散孔，该探针从基底基底通过扩散阻挡层和相应的基底层层延伸出来，并且进入待测量的气体混合物。通过提供固体电解质作为岛来减少热应力和伴随的开裂倾向。测量探针和参考探针的单独布置，即没有公共电极，可以使用例如丝网印刷将结构设计为单独的层。

2. 发明授权

US5885429A Electrochemical measuring sensor and method for producing an electrochemical measuring sensor 失效
标题翻译：电化学测量传感器及电化学测量传感器的制造方法
公开(公告)号：US5885429A
公开(公告)日：1999-03-23
申请号：US860661
申请日：1997-08-08
申请人： Karl-Hermann Friese , Werner Gruenwald , Kurt Schmid , Claudio De La Prieta , Gerhard Schneider , Hans-Joerg Renz , Harald Neumann , Uwe Glanz , Stefan Kuschel , Ralf Haug , Manfred Moser , Kurt Bayha , Annette Seibold , Carmen Schmiedel , Reiner Schuetz
发明人： Karl-Hermann Friese , Werner Gruenwald , Kurt Schmid , Claudio De La Prieta , Gerhard Schneider , Hans-Joerg Renz , Harald Neumann , Uwe Glanz , Stefan Kuschel , Ralf Haug , Manfred Moser , Kurt Bayha , Annette Seibold , Carmen Schmiedel , Reiner Schuetz
IPC分类号： G01N27/409 , G01N27/407 , G01N27/26
CPC分类号： G01N27/4075
摘要： An electrochemical measuring sensor having a solid electrolyte, a first electrode exposed to a gas to be measured and a second electrode exposed to a reference gas, with the electrodes preferably being arranged on opposite sides of the solid electrolyte. At least one of the electrodes (16, 20) is provided with a contouring (24) on its side (22) that is exposed to the gas to be measured or to the reference gas, with the contouring being a trench-shaped groove (26) embossed into the surface of the electrode such that the electrode is pressed into the adjacent solid electrolyte in the region of the groove. According to the method, the embossing is done while the electrode and the solid electrolyte are in the non-sintered state, and the sensor is subsequently sintered.
摘要翻译： PCT No.PCT / DE96 / 01753 Sec。 371日期：1997年8月8日 102（e）日期1997年8月8日PCT提交1996年9月17日PCT公布。公开号WO97 / 17608 日期1997年5月15日具有固体电解质的电化学测量传感器，暴露于待测气体的第一电极和暴露于参考气体的第二电极，电极优选布置在固体电解质的相对侧上。电极（16,20）中的至少一个在其侧面（22）处设置有暴露于待测量气体或参考气体的轮廓（24），其中轮廓是沟槽形凹槽 26）压印到电极的表面中，使得电极在凹槽的区域中被压入相邻的固体电解质中。根据该方法，在电极和固体电解质处于非烧结状态下进行压花，随后将传感器烧结。

3. 发明授权

US5998012A Ceramic layer systems, particularly for gas sensors 失效
公开(公告)号：US5998012A
公开(公告)日：1999-12-07
申请号：US716376
申请日：1996-09-19
申请人： Karl-Hermann Friese , Lothar Weber , Werner Gruenwald , Gert Lindemann , Harald Neumann , Ulrich Eisele
发明人： Karl-Hermann Friese , Lothar Weber , Werner Gruenwald , Gert Lindemann , Harald Neumann , Ulrich Eisele
IPC分类号： G01N27/409 , B32B18/00 , C04B35/00 , C04B41/50 , C04B41/87 , G01N27/407 , B23B17/00
CPC分类号： C04B41/009 , B32B18/00 , C04B41/5042 , C04B41/87 , G01N27/4073 , G01N27/4075 , C04B2237/34 , C04B2237/341 , C04B2237/343 , C04B2237/348 , Y10T428/252 , Y10T428/256 , Y10T428/257
摘要： A ceramic layer system including at least two layers having respective ion conductivities which are substantially different includes a substrate layer composed of a ceramic material and having substantially no ion conductivity; and at least one conducting layer positioned adjacent to the substrate layer, containing coated ceramic particles composed of ceramic particles composed of a ceramic material having no substantial ion conductivity which are coated with a material having a substantial ion conductivity so that each conducting layer of the at least one conducting layer has a continuous phase after sintering composed of the material which has a substantial ion conductivity and so that the at least one conducting layer has an ion conductivity effective to conduct ions. A method of producing a gas sensor for detecting small quantities of at least one gas in gas mixtures includes providing a substrate layer composed of ceramic particles composed of a material having substantially no ion conductivity; applying a layer composed of coated ceramic particles onto the substrate layer, the coated ceramic particles being composed of ceramic particles composed of a material that has no substantial ion conductivity coated with a material which has a substantial ion conductivity at the operating temperature of the gas sensor; applying at least one functional layer onto the layer composed of coated ceramic particles to provide a green body; preheating the green body to remove binding agents, plastifying agents, and any additional organic constituents; and sintering the green body after preheating by heating to a temperature effective to sinter the green body so that the layer comprised of coated ceramic particles has a continuous phase comprised of the material which has a substantial ion conductivity.

4. 发明授权

US5545301A Sensor element for the determination of concentration of gas constituent(s) 失效
标题翻译：用于测定气体成分浓度的传感器元件
公开(公告)号：US5545301A
公开(公告)日：1996-08-13
申请号：US360737
申请日：1994-12-23
申请人： Karl-Hermann Friese , Werner Gruenwald , Roland Stahl , Claudio de la Prieta , Gerhard Schneider , Harald Neumann
发明人： Karl-Hermann Friese , Werner Gruenwald , Roland Stahl , Claudio de la Prieta , Gerhard Schneider , Harald Neumann
IPC分类号： G01N27/41 , G01N27/407 , G01N27/26
CPC分类号： G01N27/4071
摘要： A sensor element for determining concentration of at least one constituent of a gas mixture operates on an electro-chemical measuring process and includes a gas measuring chamber; a pair of electrodes and an electrode chamber located between the pair of electrodes; and a diffusion conduit adjoining the electrode chamber and having a gas input which connects with the gas measuring chamber, having a gas output which connects with the electrode chamber, and having at least one cross-sectional area including a height, w, and a length, L, which height, w, has a preselected minimum value, and which length, L, has a value which is equal to or greater than the preselected minimum value of the height, w. The constituent of the gas mixture has a mean free path length through the sensor element, the gas measuring chamber has a cross-sectional area including a height and a length each of which are at least as large as the minimum height, w, of the diffusion conduit, and the height, w, of respective ones of the at least one cross-sectional area of the diffusion conduit is at least a multiple of the mean free path length of the constituent of the gas mixture to be measured. Advantageously, substantially only gaseous phase diffusion occurs when the predetermined minimum value of the height, w, is at least a multiple of a minimum value of the mean free path length for the gas constituent measured.
摘要翻译：用于确定气体混合物的至少一种组分的浓度的传感器元件在电化学测量过程中运行，并且包括气体测量室; 位于所述一对电极之间的一对电极和电极室; 以及邻接所述电极室并具有与所述气体测量室连接的气体输入的扩散管道，具有与所述电极室连接的气体输出，并且具有包括高度w和长度的至少一个横截面区域，L，其高度w具有预选的最小值，并且长度L具有等于或大于预定的最小值的最小值w的值。气体混合物的组分具有通过传感器元件的平均自由路径长度，气体测量室具有包括高度和长度的横截面积，每个高度和长度至少与最小高度w一样大，扩散管道的扩散管道，并且扩散管道的至少一个横截面积中相应的一个的高度w至少为要测量的气体混合物的成分的平均自由程长度的倍数。有利地，当高度的预定最小值w至少为测量的气体成分的平均自由程长度的最小值的倍数时，基本上仅发生气相扩散。

5. 发明授权

US5773894A Insulation layer system for the electrical isolation circuits 失效
标题翻译：绝缘层系统用于电气隔离电路
公开(公告)号：US5773894A
公开(公告)日：1998-06-30
申请号：US769182
申请日：1996-12-18
申请人： Karl-Hermann Friese , Heinz Geier , Werner Gruenwald , Claudio De La Prieta
发明人： Karl-Hermann Friese , Heinz Geier , Werner Gruenwald , Claudio De La Prieta
IPC分类号： B32B18/00 , G01N27/406 , G01N27/407 , H01B3/12 , C04B35/48
CPC分类号： G01N27/407 , B32B18/00 , C04B37/001 , C04B37/021 , G01N27/4067 , G01N27/4071 , G01N27/4075 , H01B3/12 , C04B2237/064 , C04B2237/068 , C04B2237/32 , C04B2237/341 , C04B2237/343 , C04B2237/348 , C04B2237/40 , C04B2237/401 , C04B2237/68 , C04B2237/704 , C04B2237/708 , C04B2237/72 , C04B2237/76 , C04B2237/86
摘要： An insulation layer system, in particular for gas sensors, is proposed, having at least one electrically conductive solid-electrolyte layer (10), an electrically conductive layer (20) and at least one electrically insulating layer (13) between the solid-electrolyte layer (10) and the electrically conductive layer (20). The material of the insulating layer (13) contains, prior to sintering, pentavalent metal oxides of niobium or tantalum as an additive, it being possible for the additive to diffuse into the adjoining solid-electrolyte layer (10) during sintering.
摘要翻译：提出了一种特别用于气体传感器的绝缘层系统，其具有至少一个导电固体电解质层（10），导电层（20）和固体电解质之间的至少一个电绝缘层（13）层（10）和导电层（20）。绝缘层（13）的材料在烧结之前含有铌或钽的五价金属氧化物作为添加剂，在烧结期间添加剂可能扩散到相邻的固体电解质层（10）中。

6. 发明授权

US5474665A Measuring sensor for determining the oxygen content of gas mixtures 失效
标题翻译：用于测定气体混合物氧含量的测量传感器
公开(公告)号：US5474665A
公开(公告)日：1995-12-12
申请号：US306572
申请日：1994-09-15
申请人： Karl-Hermann Friese , Hermann Dietz , Hermann Fischer , Manfred Koeder , Werner Gruenwald , Ulrich Eisele
发明人： Karl-Hermann Friese , Hermann Dietz , Hermann Fischer , Manfred Koeder , Werner Gruenwald , Ulrich Eisele
IPC分类号： F02B1/04 , F02D41/14 , G01N27/409 , G01N27/419 , G01N27/407
CPC分类号： G01N27/419 , F02B1/04
摘要： The invention relates to a measuring sensor having pump reference for measuring the oxygen content of gas mixtures, particularly exhaust gases of internal combustion engines. The sensor includes a measuring cell (A) and a reference cell (B) each having a pair of electrodes, with one of each respective pairs of electrodes being common to the two cells, and having a fixed electrolyte. Reference cell (B) has defined therein an internal oxygen reference zone which is hermetically sealed from the gas mixture and which is connected to the atmosphere by way of a pressure-equalization line. The measuring cell (A) and the reference cell (B) can be heated by heating apparatus to a temperature at which the fixed electrolyte has an ionic conductivity which is sufficiently high. The heating apparatus and a porous insulation are advantageously disposed in the vicinity of the electrode of the reference cell which is not in common with the measuring cell and which is porous so that the porous insulation, together with the porous electrode, form the internal oxygen reference zone and, together with the porous electrode and its porous conductor track, form the pressure-equalization line.
摘要翻译：本发明涉及一种具有用于测量气体混合物，特别是内燃机废气的氧含量的泵参考的测量传感器。传感器包括测量单元（A）和参考单元（B），每个参考单元具有一对电极，每对电极中的每一对电极与两个单元共用，并具有固定的电解液。参考电池（B）在其中限定了内部氧参考区，其内部氧参考区与气体混合物气密密封，并通过压力平衡线连接到大气。测量单元（A）和参考单元（B）可以通过加热装置加热至固定电解质具有足够高的离子电导率的温度。加热装置和多孔绝缘体有利地设置在参比单元的电极附近，其与测量池不相同，并且是多孔的，使得多孔绝缘体与多孔电极一起形成内部氧参考并且与多孔电极及其多孔导体轨道一起形成压力平衡线。

7. 发明授权

US5628848A Process for the production of composite systems having at least two inorganic ceramic layers 失效
标题翻译：用于生产具有至少两个无机陶瓷层的复合体系的方法
公开(公告)号：US5628848A
公开(公告)日：1997-05-13
申请号：US367141
申请日：1995-01-09
申请人： Karl-Hermann Friese , Werner Gruenwald , Ulrich Eisele
发明人： Karl-Hermann Friese , Werner Gruenwald , Ulrich Eisele
IPC分类号： B32B18/00 , C04B37/00 , G01N27/407 , B32B31/26
CPC分类号： B32B18/00 , C04B37/001 , G01N27/4073 , C04B2237/343 , C04B2237/348 , C04B2237/36 , C04B2237/586 , C04B2237/76
摘要： The invention relates to composite systems having at least two layers which comprise different inorganic, ceramic phases and are produced by cosintering of different, finely divided inorganic materials arranged in layers. The composite systems are characterized in that at least two adjacent layers comprise a dense phase largely free of macropores. The layers are durably bonded to one another by sintering together of particles of the different materials at the phase boundary or boundaries. The composite systems and the processes for the production thereof are used, for example, in the manufacture of gas sensors.
摘要翻译： PCT No.PCT / DE94 / 00520 Sec。 371日期1995年1月9日 102（e）1995年1月9日PCT PCT 1994年5月6日PCT公布。第WO94 / 27819号公报日期1994年12月8日本发明涉及具有至少两层的复合体系，它们包含不同的无机陶瓷相，并通过不同细分的无机材料以层间顺序的同步化而产生。复合体系的特征在于至少两个相邻的层包含大部分不含大孔的密相。这些层通过在相边界或边界处将不同材料的颗粒烧结在一起而相互粘合在一起。复合系统及其制造方法例如用于气体传感器的制造中。

8. 发明授权

US06518323B1 Polymer compound, the production and use thereof, and sintered compacts produced therefrom 失效
标题翻译：高分子化合物，其制造和使用以及由其制造的烧结体
公开(公告)号：US06518323B1
公开(公告)日：2003-02-11
申请号：US09622018
申请日：2000-10-11
申请人： Gerd Scheying , Johannes Kanters , Ingrid Wuehrl , Ulrich Eisele , Horst Boeder , Lutz Dorfmueller , Werner Gruenwald
发明人： Gerd Scheying , Johannes Kanters , Ingrid Wuehrl , Ulrich Eisele , Horst Boeder , Lutz Dorfmueller , Werner Gruenwald
IPC分类号： C08J900
CPC分类号： H05K1/0373 , C04B35/46 , C04B35/486 , C04B35/63404 , C08K3/34 , H05K2201/0116 , H05K2201/0129 , H05K2201/0209
摘要： A polymer compound containing a ceramic powder and a polymer is described, the ceramic powder having a specific surface area of more than 1.8·108 m2/m3 and constituting more than 5 vol. % of the polymer compound, the polymer being shear resistant, and the pore sizes in the polymer compound being 3-15 nm. Furthermore, a method for manufacturing this polymer compound, its use, and a sintered body manufactured therefrom are also described.
摘要翻译：描述了含有陶瓷粉末和聚合物的高分子化合物，陶瓷粉末的比表面积大于1.8.108m 2 / m 3，构成大于5体积％高分子化合物的％，聚合物是抗剪切的，高分子化合物中的孔径为3-15nm。此外，还描述了制造该高分子化合物的方法，其用途和由其制造的烧结体。

9. 发明授权

US5879526A Electrochemical measuring sensor for determining nitrogen oxides in gas mixtures 失效
标题翻译：用于测定气体混合物中氮氧化物的电化学测量传感器
公开(公告)号：US5879526A
公开(公告)日：1999-03-09
申请号：US822510
申请日：1997-03-24
申请人： Hermann Dietz , Werner Gruenwald
发明人： Hermann Dietz , Werner Gruenwald
IPC分类号： G01N33/00 , G01N27/41
CPC分类号： G01N33/0037
摘要： An electrochemical measuring sensor for selectively determining nitrogen oxides in a gas mixture including oxygen and nitrogen oxides, includes a solid electrolyte layer; a cover layer; and a diffusion channel which is defined between the solid electrolyte layer and the cover layer, and through which the gas mixture diffuses in a diffusion direction. The solid electrolyte layer has provided on a surface thereof a first cathode and a second cathode disposed one after the other in the diffusion direction of the gas mixture within the diffusion channel and exposed to the gas mixture in the order recited, and has provided on an opposite surface thereof at least one anode. The diffusion channel forms a diffusion barrier for the second cathode. The first and second cathodes and the at least one anode are gas permeable and consist of one of a precious metal or a precious metal alloy. The first cathode is provided with a coating which completely covers same, which is impermeable to nitrogen oxides (NO.sub.x), and which is permeable to oxygen. The first cathode, a portion of the solid electrolyte, and the at least one anode form a first pumping cell. The second cathode, another portion of the solid electrolyte, and the at least one anode form a second pumping cell. A measuring signal for determining NO.sub.x is measured between the second cathode of the second pumping cell and the at least one anode of the second pumping cell as a limiting current.
摘要翻译：一种用于选择性地确定包含氧和氮氧化物的气体混合物中的氮氧化物的电化学测量传感器包括固体电解质层; 覆盖层; 以及限定在固体电解质层和覆盖层之间的扩散通道，气体混合物通过该扩散通道沿扩散方向扩散。固体电解质层在其表面上设置有在扩散通道内的气体混合物的扩散方向上一个接一个地设置的第一阴极和第二阴极，并以所述顺序暴露于气体混合物，并且其相对表面具有至少一个阳极。扩散通道形成第二阴极的扩散阻挡层。第一和第二阴极和至少一个阳极是透气的，由贵金属或贵金属合金之一组成。第一阴极设置有完全覆盖的涂层，其对于氮氧化物（NOx）是不可渗透的，并且其是透氧的。第一阴极，固体电解质的一部分和至少一个阳极形成第一泵浦电池。第二阴极，固体电解质的另一部分和至少一个阳极形成第二泵浦电池。在第二泵浦电池的第二阴极和第二泵浦电池的至少一个阳极之间测量用于确定NOx的测量信号作为限制电流。

10. 发明授权

US5507174A Polarographic sensor 失效
标题翻译：极谱传感器
公开(公告)号：US5507174A
公开(公告)日：1996-04-16
申请号：US211569
申请日：1994-08-02
申请人： Karl-Hermann Friese , Hermann Dietz , Werner Gruenwald
发明人： Karl-Hermann Friese , Hermann Dietz , Werner Gruenwald
IPC分类号： G01N27/41 , F02B1/04 , G01N27/407 , G01N27/416 , G01M15/00 , G01N27/48
CPC分类号： G01N27/4071 , F02B1/04
摘要： A polarographic sensor for determining concentration of certain components including oxygen or combustible fractions, such as hydrocarbons, hydrogen and carbon monoxide, in the exhaust gas of an internal combustion engine, includes a pump cell having an anode, a cathode, and an oxygen ion-conducting solid electrolyte provided between the anode and the cathode, wherein the cathode is provided with a diffusion barrier, wherein the anode is provided with a diffusion barrier, and wherein the concentration of the certain components is determined by measurement of a limiting current through the electrolyte and across one of the diffusion barriers to the corresponding anode or cathode.
摘要翻译： PCT No.PCT / DE93 / 00674 Sec。 371日期1994年8月2日 102（e）日期1994年8月2日PCT提交1993年7月31日PCT公布。第WO94 / 04911号公报日本3月3日，1994.用于确定内燃机废气中某些组分（包括氧气或可燃组分）如烃，氢气和一氧化碳的浓度的极谱传感器包括具有阳极，阴极和设置在阳极和阴极之间的氧离子传导固体电解质，其中阴极设置有扩散阻挡层，其中阳极设置有扩散阻挡层，并且其中某些组分的浓度通过测量确定限制电流通过电解质，并穿过一个扩散屏障到相应的阳极或阴极。

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