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1. 发明授权

US4933167A Pesticide compositions 失效
标题翻译：农药组合物
公开(公告)号：US4933167A
公开(公告)日：1990-06-12
申请号：US271353
申请日：1988-11-14
申请人： Herbert B. Scher , Marius Rodson , Ronald L. Morgan
发明人： Herbert B. Scher , Marius Rodson , Ronald L. Morgan
IPC分类号： A01N25/28 , A01N25/32 , A01N57/22
CPC分类号： A01N25/32 , A01N25/28 , A01N57/22
摘要： Toxicant, especially pesticide compositions, having lowered dermal toxicity are provided. The compositions include a microencapsulated lipophilicpesticide, a hydrophilic surfactant and water. Methods for reducing the dermal toxicity of microencapsulated lipophilic toxicants, especially pesticides are provided. Methods for controlling insect pests using the disclosed compositions are provided.
摘要翻译：提供具有降低的皮肤毒性的毒性，特别是农药组合物。组合物包括微囊化的亲脂性杀虫剂，亲水性表面活性剂和水。提供了降低微胶囊化亲脂性毒物，特别是农药的皮肤毒性的方法。提供了使用所公开的组合物来控制害虫的方法。

2. 发明授权

US5120542A Pesticide compositions and method 失效
标题翻译：农药组合物和方法
公开(公告)号：US5120542A
公开(公告)日：1992-06-09
申请号：US638299
申请日：1991-01-03
申请人： Herbert B. Scher , Marius Rodson , Ronald L. Morgan
发明人： Herbert B. Scher , Marius Rodson , Ronald L. Morgan
IPC分类号： A01N25/12 , A01N25/22 , A01N25/32 , A01N57/12 , A01N57/22
CPC分类号： A01N57/12 , A01N25/12 , A01N25/22 , A01N25/32 , A01N57/22
摘要： Toxicant, especially pesticide compositions, having lowered dermal toxicity are provided. The compositions include a lipophilic-pesticide, a nonionic surfactant and a dry inert diluent carrier. Methods for reducing the dermal toxicity of lipophilic toxicants, especially pesticides are provided, as well as methods for controlling insect pests using the disclosed compositions.
摘要翻译：提供具有降低的皮肤毒性的毒性，特别是农药组合物。组合物包括亲脂性农药，非离子表面活性剂和干惰性稀释剂载体。提供了降低亲脂性毒物特别是农药的皮肤毒性的方法，以及使用所公开的组合物来控制害虫的方法。

3. 发明授权

US4994261A Pesticide compositions and method 失效
标题翻译：农药组合物和方法
公开(公告)号：US4994261A
公开(公告)日：1991-02-19
申请号：US232193
申请日：1988-08-15
申请人： Herbert B. Scher , Marius Rodson , Ronald L. Morgan
发明人： Herbert B. Scher , Marius Rodson , Ronald L. Morgan
IPC分类号： A01N25/12 , A01N25/22 , A01N25/32 , A01N57/12 , A01N57/22
CPC分类号： A01N57/12 , A01N25/12 , A01N25/22 , A01N25/32 , A01N57/22 , Y10S514/922 , Y10S514/974
摘要： Toxicant, especially pesticide compositions, having lowered dermal toxicity are provided. The compositions include a lipophilic-pesticide, a nonionic surfactant and a dry inert diluent carrier. Methods for reducing the dermal toxicity of lipophilic toxicants, especially pesticides are provided, as well as methods for controlling insect pests using the disclosed compositions.
摘要翻译：提供具有降低的皮肤毒性的毒性，特别是农药组合物。组合物包括亲脂性农药，非离子表面活性剂和干惰性稀释剂载体。提供了降低亲脂性毒物特别是农药的皮肤毒性的方法，以及使用所公开的组合物来控制害虫的方法。

4. 发明授权

US06340653B1 Microencapsulated acetochlor herbicidal composition 失效
标题翻译：微胶囊化乙草胺除草组合物
公开(公告)号：US06340653B1
公开(公告)日：2002-01-22
申请号：US08453611
申请日：1995-05-30
申请人： Herbert B. Scher , Marius Rodson
发明人： Herbert B. Scher , Marius Rodson
IPC分类号： A01N2528
CPC分类号： A01N37/26 , A01N25/28 , A01N2300/00
摘要： Microencapsulated compositions containing haloacetanilide herbicides, i.e., acetochlor, are produced by microencapsulation process. The microencapsulated composition performs comparably to nonencapsulated compositions of the same herbicide applied at the same application rates.
摘要翻译：含有卤代乙酰苯胺除草剂（即乙草胺）的微囊化组合物是通过微胶囊化方法生产的。微囊化组合物与以相同施用率施用的相同除草剂的非包封组合物相当地进行。

5. 发明授权

US5160529A Microcapsules and microencapsulation process 失效
标题翻译：微胶囊和微胶囊化方法
公开(公告)号：US5160529A
公开(公告)日：1992-11-03
申请号：US651836
申请日：1991-02-06
申请人： Herbert B. Scher , Marius Rodson
发明人： Herbert B. Scher , Marius Rodson
IPC分类号： A01N25/28 , A01N37/22 , A01N37/26 , A01P13/00 , B01J13/18
CPC分类号： A01N25/28 , A01N37/26 , B01J13/18 , Y10S514/963 , Y10T428/2985
摘要： Microcapsules containing a substantially water-insoluble liquid material, such as an anilide herbicide, and optionally also a herbicide antidote, within a porous shell to effect a slow rate of release of said herbicide (and optionally said antidote) through said shell, are produced by a process which comprises (a) providing an organic solution comprising said material and an etherified amino resin prepolymer dissolved therein which from about 50% to about 98% of the methylol groups of said prepolymer have been etherified with a C.sub.4 -C.sub.10 alcohol; (b) creating an emulsion of said organic solution in a continuous phase aqueous solution comprising water and a surface-active agent, wherein said emulsion comprises discrete droplets of said organic solution, there being formed thereby an interface between the discrete droplets of organic solution and the surrounding continuous phase aqueous solution; and (c) causing in situ self-condensation and curing of said amino resin prepolymer in the organic phase of said discrete droplets adjacent to said interface by simultaneously heating said emulsion to a temperature between about 20.degree. C. to about 100.degree. C., and adding to said emulsion an acidifying agent and maintaining said emulsion at a pH of between about 0 to about 4 for a sufficient period of time to allow substantial completion of in situ condensation of said resin prepolymers to convert the liquid droplets of said organic solution to capsules consisting of solid permeable polymer shells enclosing said liquid material.Also disclosed are the microcapsules formed by the above-described process.
摘要翻译：在多孔壳内含有基本上不溶于水的液体物质如苯胺除草剂和任选地除草剂解毒剂的微胶囊通过所述外壳来实现所述除草剂（和任选的所述解毒剂）的缓慢释放速率，由一种方法，其包括（a）提供包含所述材料的有机溶液和溶解在其中的醚化氨基树脂预聚物，其中约50％至约98％的所述预聚物的羟甲基已用C4-C10醇醚化; （b）在包含水和表面活性剂的连续相水溶液中产生所述有机溶液的乳液，其中所述乳液包含离散的所述有机溶液的液滴，由此形成离散的有机溶液液滴和周围连续相水溶液; 和（c）通过将所述乳液同时加热至约20℃至约100℃的温度，使所述氨基树脂预聚物在与所述界面相邻的所述离散液滴的有机相中原位自缩合和固化，并向所述乳液中加入酸化剂并将所述乳液保持在约0至约4的pH下足够的时间，以使基本上完成所述树脂预聚物的原位缩合以将所述有机溶液的液滴转化为胶囊由包围所述液体材料的固体可渗透聚合物壳组成。还公开了通过上述方法形成的微胶囊。

6. 发明授权

US4956129A Microencapsulation process 失效
标题翻译：微胶囊化方法
公开(公告)号：US4956129A
公开(公告)日：1990-09-11
申请号：US151048
申请日：1988-02-01
申请人： Herbert B. Scher , Marius Rodson
发明人： Herbert B. Scher , Marius Rodson
IPC分类号： A01N25/28 , B01J13/18
CPC分类号： B01J13/18 , A01N25/28 , Y10S514/963 , Y10T428/2985
摘要： A process is disclosed for the microencapsulation of a substantially water-insoluble liquid material within a porous shell to effect a slow rate of release of said material through said shell which comprises (a) providing an organic solution comprising said material and an etherified urea-formaldehyde prepolymer dissolved therein which from about 50% to about 98% of the methylol groups of said prepolymer have been etherified with a C.sub.4 -C.sub.10 alcohol; (b) creating an emulsion of said organic solution in an continuous phase aqueous solution comprising water and a surfaceactive agent, wherein said emulsion comprises discrete droplets of said organic solution dispersed in said continuous phase aqueous solution, there being formed thereby an interface between the discrete droplets of organic solution and the surrounding continuous phase aqueous solution; and (c) causing in situ self-condensation and curing of said ureaformaldehyde prepolymers in the organic phase of said discrete droplets adjacent to said interface by simultaneously heating said emulsion to a temperature between about 20.degree. C. to about 100.degree. C., and adding to said emulsion an acidifying agent and maintaining said emulsion at a pH of between about 0 to about 4 for a sufficient period of time to allow substantial completion of in situ condensation of said resin prepolymers to convert the liquid droplets of said organic solution to capsules consisting of solid permeable polymer shells enclosing said liquid material.Also disclosed are the microcapsules formed by the above-described process. f
摘要翻译：公开了一种用于在多孔壳体内微囊化基本上不溶于水的液体材料的方法，以实现所述材料通过所述壳体的缓慢释放速率，其包括（a）提供包含所述材料的有机溶液和醚化的脲 - 甲醛其中约50％至约98％的所述预聚物的羟甲基已经用C 4 -C 10醇醚化了; （b）在包含水和表面活性剂的连续相水溶液中产生所述有机溶液的乳液，其中所述乳液包含分散在所述连续相水溶液中的所述有机溶液的离散液滴，由此形成离散的有机溶液滴和周围连续相水溶液; 和（c）通过同时将所述乳液加热到约20℃至约100℃的温度，使所述脲甲醛预聚物在所述离子液滴的邻近所述界面的有机相中原位自缩合和固化，以及向所述乳液中加入酸化剂并将所述乳液保持在约0至约4的pH下足够的时间，以使基本上完成所述树脂预聚物的原位冷凝以将所述有机溶液的液滴转化成胶囊由包封所述液体材料的固体可渗透聚合物壳组成。还公开了通过上述方法形成的微胶囊。

7. 发明授权

US5332584A Microcapsules 失效
标题翻译：微胶囊
公开(公告)号：US5332584A
公开(公告)日：1994-07-26
申请号：US803870
申请日：1991-12-09
申请人： Herbert B. Scher , Marius Rodson
发明人： Herbert B. Scher , Marius Rodson
IPC分类号： A01N25/28 , B01J13/18 , A01N37/18
CPC分类号： B01J13/18 , A01N25/28 , Y10S514/963 , Y10T428/2985
摘要： A process is disclosed for the microencapsulation of a substantially water-insoluble liquid material within a porous shell to effect a slow rate of release of said material through said shell which comprises (a) providing an organic solution comprising said material and an etherified urea-formaldehyde prepolymer dissolved therein in which from about 50% to about 98% of the methylol groups of said prepolymer have been etherified with a C.sub.4 -C.sub.10 alcohol; (b) creating an emulsion of said organic solution in an continuous phase aqueous solution comprising water and a surfaceactive agent, wherein said emulsion comprises discrete droplets of said organic solution dispersed in said continuous phase aqueous solution, there being formed thereby an interface between the discrete droplets of organic solution and the surrounding continuous phase aqueous solution; and (c) causing in situ self-condensation and curing of said ureaformaldehyde prepolymers in the organic phase of said discrete droplets adjacent to said interface by simultaneously heating said emulsion to a temperature between about 20.degree. C. to about 100.degree. C., and adding to said emulsion an acidifying agent and maintaining said emulsion at a pH of between about 0 to about 4 for a sufficient period of time to allow substantial completion of in situ condensation of said resin prepolymers to convert the liquid droplets of said organic solution to capsules consisting of solid permeable polymer shells enclosing said liquid material.Also disclosed are the microcapsules formed by the above-described process.
摘要翻译：公开了一种用于在多孔壳体内微囊化基本上不溶于水的液体材料的方法，以实现所述材料通过所述壳体的缓慢释放速率，其包括（a）提供包含所述材料的有机溶液和醚化的脲 - 甲醛溶解在其中的预聚物，其中约50％至约98％的所述预聚物的羟甲基已用C4-C10醇醚化; （b）在包含水和表面活性剂的连续相水溶液中产生所述有机溶液的乳液，其中所述乳液包含分散在所述连续相水溶液中的所述有机溶液的离散液滴，由此形成离散的有机溶液滴和周围连续相水溶液; 和（c）通过同时将所述乳液加热到约20℃至约100℃的温度，使所述脲甲醛预聚物在所述离子液滴的邻近所述界面的有机相中原位自缩合和固化，以及向所述乳液中加入酸化剂并将所述乳液保持在约0至约4的pH下足够的时间，以使基本上完成所述树脂预聚物的原位冷凝以将所述有机溶液的液滴转化成胶囊由包封所述液体材料的固体可渗透聚合物壳组成。还公开了通过上述方法形成的微胶囊。

8. 发明授权

US5223477A Single-package agricultural formulations combining immediate and time-delayed delivery of thiocarbamate herbicides and dichlormid as safener 失效
标题翻译：单包装农药配方将硫代氨基甲酸酯除草剂和二氯甲烷的即时和时间延迟交付作为安全剂
公开(公告)号：US5223477A
公开(公告)日：1993-06-29
申请号：US724264
申请日：1991-07-01
申请人： Herbert B. Scher , Marius Rodson , Jose L. Calvo , Miguel Gimeno
发明人： Herbert B. Scher , Marius Rodson , Jose L. Calvo , Miguel Gimeno
IPC分类号： A01N25/28
CPC分类号： A01N25/28
摘要： Microcapsule formulations are combined with emulsions or particle dispersions in a single-package formulation which is storage-stable and provides substantially the full efficacy of each of the two forms as if applied individually. The single-package formulation is suspension having two dispersed phases--the first being an active species encapsulated in a shell of inert polymeric diffusion-limiting material (i.e., a microcapsule), and the second being an active species in water-insoluble form with no diffusion-limiting barrier at its surface. An appropriate suspension system is included to prevent the dispersed phases from agglomerating within themselves and with each other. The invention is useful in combining two different active ingredients as well as in combining immediate-delivery and delayed-delivery forms of the same active ingredient. The invention may for example involve combining a biocide with an activity modifier such as a safener, with the effect of lowering the needed amount of one or the other by removing it to a separate phase. In certain cases, a unique combination of surface-active agents maintains the phases in suspension.
摘要翻译：将微胶囊制剂与单一包装制剂中的乳剂或颗粒分散体组合，其是储存稳定的并且提供了两种形式中的每一种的基本上全部功效，如同单独应用。单包装制剂是具有两个分散相的悬浮液 - 第一种是包封在惰性聚合物扩散限制材料（即，微胶囊）的壳体中的活性物质，第二种是不溶于水的不活泼物质的活性物质扩散限制屏障在其表面。包括适当的悬浮系统以防止分散相在其内部和彼此之间附聚。本发明可用于组合两种不同的活性成分以及组合相同活性成分的即时递送和延迟递送形式。本发明可以例如包括将杀生物剂与活性改良剂（例如安全剂）组合，其作用是通过将一种或另一种除去所需量降低至单独的相。在某些情况下，表面活性剂的独特组合保持了悬浮状态。

9. 发明授权

US5049182A Single-package agricultural formulations combining immediate and time-delayed delivery 失效
标题翻译：单包装农业配方立即和延期交货
公开(公告)号：US5049182A
公开(公告)日：1991-09-17
申请号：US291723
申请日：1989-02-03
申请人： Herbert B. Scher , Marius Rodson , Jose L. Calvo , Miguel Gimeno
发明人： Herbert B. Scher , Marius Rodson , Jose L. Calvo , Miguel Gimeno
IPC分类号： A01N25/04 , A01N25/28
CPC分类号： A01N25/28 , Y10T428/2982 , Y10T428/2984 , Y10T428/2989
摘要： Microcapsule formulations are combined with emulsions or particle dispersions in a single-package formulation which is storage-stable and provides substantially the full efficacy of each of the two forms as if applied individually. The single-package formulation is suspension having two dispersed phases--the first being an active species encapsulated in a shell of inert polymeric diffusion-limiting material (i.e., a microcapsule), and the second being an active species in water-insoluble form with no diffusion-limiting barrier at its surface. An appropriate suspension system is included to prevent the dispersed phases from agglomerating within themselves and with each other. The invention is useful in combining two different active ingredients as well as in combining immediate-delivery and delayed-delivery forms of the same active ingredient. The invention may for example involve combining a biocide with an activity modifier such as a safener, with the effect of lowering the needed amount of one or the other by removing it to a separate phase. In certain cases, a unique combination of surface-active agents maintains the phases in suspension.
摘要翻译：将微胶囊制剂与单一包装制剂中的乳剂或颗粒分散体组合，其是储存稳定的并且提供了两种形式中的每一种的基本上全部功效，如同单独应用。单包装制剂是具有两个分散相的悬浮液 - 第一种是包封在惰性聚合物扩散限制材料（即，微胶囊）的壳体中的活性物质，第二种是不溶于水的不活泼物质的活性物质扩散限制屏障在其表面。包括适当的悬浮系统以防止分散相在其内部和彼此之间附聚。本发明可用于组合两种不同的活性成分以及组合相同活性成分的即时递送和延迟递送形式。本发明可以例如包括将杀生物剂与活性改良剂（例如安全剂）组合，其作用是通过将一种或另一种除去所需量降低至单独的相。在某些情况下，表面活性剂的独特组合保持了悬浮状态。

10. 发明授权

US06133197A Microencapsulated compositions 失效
标题翻译：微胶囊化组合物
公开(公告)号：US06133197A
公开(公告)日：2000-10-17
申请号：US861211
申请日：1997-05-21
申请人： Jin-Ling Chen , Marius Rodson , Herbert B. Scher , Kuo-Shin Lee, deceased
发明人： Jin-Ling Chen , Marius Rodson , Herbert B. Scher , Kuo-Shin Lee, deceased
IPC分类号： A01N25/28 , A01N43/40 , A01N53/00 , B01J20060101 , A01N3/02 , A01N57/00 , A01N59/24
CPC分类号： A01N25/28 , A01N43/40 , A01N53/00 , Y10S71/903
摘要： Polyurea microcapsules particularly suitable for foliar application are prepared by an interfacial polymerization process in which the polyurea is formed from an aromatic diisocyanate and optionally an aromatic polyisocyanate having 3 or more isocyanate groups, in a weight ratio (when both types of isocyanate are present) of polyisocyanate:diisocyanate of from about 1:100 to about 1:1.5, and in which the microcapsules are produced having an average particle size of from about 1 to about 5 microns.As compared to conventional liquid (e.g., emulsifiable concentrate) compositions of pesticides, the microcapsules can provide safer handling and higher loading of active ingredients, while providing substantially equivalent biological activity to the liquid compositions.
摘要翻译：特别适用于叶面施用的聚脲微胶囊通过界面聚合方法制备，其中聚脲由芳族二异氰酸酯和任选的具有3个或更多个异氰酸酯基团的芳族多异氰酸酯形成，其重量比（当存在两种类型的异氰酸酯时）为多异氰酸酯：约1:100至约1:1.5的二异氰酸酯，其中制备的平均粒度为约1至约5微米的微胶囊。与常规液体（例如可乳化浓缩物）农药组合物相比，微胶囊可以提供更安全的处理和更高的活性成分负载，同时为液体组合物提供基本相同的生物活性。

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