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1. 发明授权

US6149843A Microcapsules containing suspensions of biologically active compounds and ultraviolet protectant 失效
公开(公告)号：US6149843A
公开(公告)日：2000-11-21
申请号：US120965
申请日：1998-07-22
申请人： Herbert B. Scher , Jin Ling Chen
发明人： Herbert B. Scher , Jin Ling Chen
IPC分类号： A01N25/04 , A01N25/22 , A01N25/28 , A01N25/30 , A01N37/38 , A01N41/10 , A01N43/70 , A01N53/00 , B01J13/02 , B01J13/04 , B01J13/18 , A01N25/34
CPC分类号： B01J13/18 , A01N25/04 , A01N25/22 , A01N25/28 , A01N37/38 , A01N41/10 , A01N43/70 , A01N53/00 , B01J13/02 , B01J13/04
摘要： Microcapsules containing a biologically active material which is sensitive to ultraviolet light are prepared which contain an ultraviolet light protectant selected from titanium dioxide, zinc oxide and mixtures thereof, suspended and thoroughly dispersed in a liquid.

2. 发明授权

US5993842A Microcapsules containing suspensions of biologically active compounds 失效
标题翻译：含有生物活性化合物的悬浮液的微胶囊
公开(公告)号：US5993842A
公开(公告)日：1999-11-30
申请号：US835265
申请日：1997-04-08
申请人： Herbert B. Scher , Jin Ling Chen
发明人： Herbert B. Scher , Jin Ling Chen
IPC分类号： A01N25/04 , A01N25/22 , A01N25/28 , A01N53/00 , B01J13/02 , B01J13/04 , B01J13/18
CPC分类号： B01J13/18 , A01N25/04 , A01N25/22 , A01N25/28 , A01N53/00 , B01J13/02 , B01J13/04
摘要： Microcapsules containing a suspension of a solid, biologically active compound in an organic, water-immiscible liquid and processes for their preparation.
摘要翻译：含有固体，生物活性化合物在有机，水不混溶液体中的悬浮液的微胶囊及其制备方法。

3. 发明授权

US06133197A Microencapsulated compositions 失效
标题翻译：微胶囊化组合物
公开(公告)号：US06133197A
公开(公告)日：2000-10-17
申请号：US861211
申请日：1997-05-21
申请人： Jin-Ling Chen , Marius Rodson , Herbert B. Scher , Kuo-Shin Lee, deceased
发明人： Jin-Ling Chen , Marius Rodson , Herbert B. Scher , Kuo-Shin Lee, deceased
IPC分类号： A01N25/28 , A01N43/40 , A01N53/00 , B01J20060101 , A01N3/02 , A01N57/00 , A01N59/24
CPC分类号： A01N25/28 , A01N43/40 , A01N53/00 , Y10S71/903
摘要： Polyurea microcapsules particularly suitable for foliar application are prepared by an interfacial polymerization process in which the polyurea is formed from an aromatic diisocyanate and optionally an aromatic polyisocyanate having 3 or more isocyanate groups, in a weight ratio (when both types of isocyanate are present) of polyisocyanate:diisocyanate of from about 1:100 to about 1:1.5, and in which the microcapsules are produced having an average particle size of from about 1 to about 5 microns.As compared to conventional liquid (e.g., emulsifiable concentrate) compositions of pesticides, the microcapsules can provide safer handling and higher loading of active ingredients, while providing substantially equivalent biological activity to the liquid compositions.
摘要翻译：特别适用于叶面施用的聚脲微胶囊通过界面聚合方法制备，其中聚脲由芳族二异氰酸酯和任选的具有3个或更多个异氰酸酯基团的芳族多异氰酸酯形成，其重量比（当存在两种类型的异氰酸酯时）为多异氰酸酯：约1:100至约1:1.5的二异氰酸酯，其中制备的平均粒度为约1至约5微米的微胶囊。与常规液体（例如可乳化浓缩物）农药组合物相比，微胶囊可以提供更安全的处理和更高的活性成分负载，同时为液体组合物提供基本相同的生物活性。

4. 发明授权

US06077522A Microcapsules containing suspensions of biologically active compounds and ultraviolet protectant 失效
标题翻译：含有生物活性化合物和紫外线防护剂的悬浮液的微胶囊
公开(公告)号：US06077522A
公开(公告)日：2000-06-20
申请号：US122218
申请日：1998-07-23
申请人： Herbert B. Scher , Jin Ling Chen
发明人： Herbert B. Scher , Jin Ling Chen
IPC分类号： A01N25/04 , A01N25/22 , A01N25/28 , A01N25/30 , A01N37/38 , A01N41/10 , A01N43/70 , A01N53/00 , B01J13/02 , B01J13/04 , B01J13/18 , A01N25/08
CPC分类号： B01J13/18 , A01N25/04 , A01N25/22 , A01N25/28 , A01N37/38 , A01N41/10 , A01N43/70 , A01N53/00 , B01J13/02 , B01J13/04
摘要： Microcapsules containing a biologically active material which is sensitive to ultraviolet light are prepared which contain an ultraviolet light protectant selected from titanium dioxide, zinc oxide and mixtures thereof, suspended and thoroughly dispersed in a liquid.
摘要翻译：制备含有对紫外线敏感的生物活性物质的微胶囊，其含有悬浮并充分分散在液体中的选自二氧化钛，氧化锌及其混合物的紫外线防护剂。

5. 发明授权

US06015571A Microcapsules containing suspensions of biologically active compounds 失效
标题翻译：含有生物活性化合物的悬浮液的微胶囊
公开(公告)号：US06015571A
公开(公告)日：2000-01-18
申请号：US354409
申请日：1994-12-12
申请人： Herbert B. Scher , Jin Ling Chen
发明人： Herbert B. Scher , Jin Ling Chen
IPC分类号： A01N25/04 , A01N25/22 , A01N25/28 , A01N25/30 , A01N37/22 , A01N37/26 , A01N41/10 , A01N43/70 , A01N53/00 , A01N57/12 , A01P13/00 , B01J13/02 , B01J13/04 , B01J13/18
CPC分类号： B01J13/18 , A01N25/04 , A01N25/22 , A01N25/28 , A01N41/10 , A01N43/70 , A01N53/00 , B01J13/02 , B01J13/04 , Y10T428/2989
摘要： Microcapsules containing a suspension of a soild, biologically active compound in an organic, water-immiscible liquid and processes for their preparation.
摘要翻译：微胶囊含有有机，水不混溶性液体中的生物活性化合物的悬浮液，以及其制备方法。

6. 发明授权

US5846554A Microcapsules containing suspensions of biologically active compounds and ultraviolet protectant 失效
公开(公告)号：US5846554A
公开(公告)日：1998-12-08
申请号：US430030
申请日：1995-04-27
申请人： Herbert B. Scher , Jin Ling Chen
发明人： Herbert B. Scher , Jin Ling Chen
IPC分类号： A01N25/04 , A01N25/22 , A01N25/28 , A01N25/30 , A01N37/38 , A01N41/10 , A01N43/70 , A01N53/00 , B01J13/02 , B01J13/04 , B01J13/18
CPC分类号： B01J13/18 , A01N25/04 , A01N25/22 , A01N25/28 , A01N37/38 , A01N41/10 , A01N43/70 , A01N53/00 , B01J13/02 , B01J13/04
摘要： Microcapsules containing a biologically active material which is sensitive to ultraviolet light are prepared which contain an ultraviolet light protectant selected from titanium dioxide, zinc oxide and mixtures thereof, suspended and thoroughly dispersed in a liquid.

7. 发明申请

US20100286019A1 Spray Drying Process 审中-公开
标题翻译：喷雾干燥过程
公开(公告)号：US20100286019A1
公开(公告)日：2010-11-11
申请号：US12522733
申请日：2008-01-11
申请人： Herbert B. Scher , Deborah S. Winetzky
发明人： Herbert B. Scher , Deborah S. Winetzky
IPC分类号： C11D3/386 , B29B9/00 , C11D3/22 , C11D3/37
CPC分类号： C11D3/38672 , C11D3/225 , C11D3/3707
摘要： The present invention generally relates to particulate compositions and methods for making the compositions. It specifically relates to improved spray drying methods that substantially reduce the production of small particles that pose industrial hygiene concerns for factory workers and product consumers. In a composition aspect, the present invention provides an atomized aqueous composition. The composition is formed using a spray-drying apparatus. It includes 0.001 to 0.10 weight percent of a polymer, which is selected from a group consisting of a cellulose-based polymer, a gum, and a synthetic polymer. It further includes at least one polypeptide, which is present in the aqueous composition at a concentration greater than 0.01 weight percent.
摘要翻译：本发明一般涉及制备组合物的颗粒组合物和方法。它具体涉及改进的喷雾干燥方法，其显着降低了造成工厂工人和产品消费者的工业卫生问题的小颗粒的生产。在组合物方面，本发明提供雾化的水性组合物。使用喷雾干燥装置形成组合物。它包括0.001至0.10重量％的聚合物，其选自纤维素基聚合物，胶和合成聚合物。它还包括至少一种多肽，其以大于0.01重量％的浓度存在于水性组合物中。

8. 发明授权

US06514439B2 Acid-triggered microcapsules 有权
标题翻译：酸触发微胶囊
公开(公告)号：US06514439B2
公开(公告)日：2003-02-04
申请号：US10013433
申请日：2001-12-11
申请人： Juanita E. Van Koppenhagen , Herbert B. Scher , Kuo-shin Lee , Ian M. Shirley , Philip Wade , Richard Follows
发明人： Juanita E. Van Koppenhagen , Herbert B. Scher , Kuo-shin Lee , Ian M. Shirley , Philip Wade , Richard Follows
IPC分类号： B01J1302
CPC分类号： B01J13/16 , A01N25/28 , C08G18/006 , C08G2310/00 , Y10T428/2985 , Y10T428/2989
摘要： Microcapsules of a microcapsule formed of a polyurea shell wall and an encapsulated ingredient or ingredients enclosed within the wall, the wall comprising at least one oligomeric acetal having the moiety in which R is (a) a moiety containing a chain of from 5 to about 40 optionally substituted carbon atoms, (b) a moiety containing a chain of from 4 to about 40 carbon atoms and one or more internally linked oxygen or sulfur atoms or —NH-groups, or (c) an optionally substituted ethylene or propylene moiety Z is (a) an optionally substituted phenyl group, (b) an optionally substituted C1-C20 alkyl, C2-C20 alkenyl, C3-C8 cycloalkyl or C5-C8 cycloalkenyl group, or (c) benzoyl, and n is 1 if R is (a) or (b), or is 2-20 if R is (c). The microcapsules are acid-sensitive and the capsule walls are relatively readily degraded or disintegrated by contacting the microcapsules with an acidic substance, preferably an organic or inorganic acid whereby the encapsulated ingredient or ingredients are released into the surrounding environment. The invention is particularly suitable for encapsulation of biologically active substances and agrochemicals, and most preferably pesticides for foliar treatment.
摘要翻译：由聚脲壳壁和包封的成分或包封在壁内的成分形成的微胶囊的微胶囊，所述壁包含至少一个具有部分的低聚缩醛，其中R是（a）含有约5至约40个链的部分，任选地取代的碳原子，（b）含有4至约40个碳原子的链和一个或多个内部连接的氧或硫原子或-NH-基团的部分，或（c）任选取代的乙烯或丙烯部分Z是（ a）任选取代的苯基，（b）任选取代的C 1 -C 20烷基，C 2 -C 20烯基，C 3 -C 8环烷基或C 5 -C 8环烯基，或（c）苯甲酰基，如果R是（a ）或（b），或如果R是（c），则为2-20。微胶囊是酸敏感的，并且胶囊壁通过使微胶囊与酸性物质（优选有机或无机酸）接触而相对容易地降解或分解，从而将包封的成分或成分释放到周围环境中。本发明特别适用于生物活性物质和农用化学品的包封，最优选用于叶面处理的农药。

9. 发明授权

US06358520B1 Dry water-dispersible compositions of microencapsulated pesticides 失效
公开(公告)号：US06358520B1
公开(公告)日：2002-03-19
申请号：US09118513
申请日：1998-07-17
申请人： Ray J. Lo , Jin L. Chen , Herbert B. Scher
发明人： Ray J. Lo , Jin L. Chen , Herbert B. Scher
IPC分类号： A01N2528
CPC分类号： A01N25/28 , A01N25/14
摘要： Solid water-dispersible compositions containing microencapsulated pesticides are produced by spray-drying an aqueous suspension of said pesticides in the presence of a water-soluble polymer, preferably polyvinyl alcohol.

10. 发明授权

US5160529A Microcapsules and microencapsulation process 失效
标题翻译：微胶囊和微胶囊化方法
公开(公告)号：US5160529A
公开(公告)日：1992-11-03
申请号：US651836
申请日：1991-02-06
申请人： Herbert B. Scher , Marius Rodson
发明人： Herbert B. Scher , Marius Rodson
IPC分类号： A01N25/28 , A01N37/22 , A01N37/26 , A01P13/00 , B01J13/18
CPC分类号： A01N25/28 , A01N37/26 , B01J13/18 , Y10S514/963 , Y10T428/2985
摘要： Microcapsules containing a substantially water-insoluble liquid material, such as an anilide herbicide, and optionally also a herbicide antidote, within a porous shell to effect a slow rate of release of said herbicide (and optionally said antidote) through said shell, are produced by a process which comprises (a) providing an organic solution comprising said material and an etherified amino resin prepolymer dissolved therein which from about 50% to about 98% of the methylol groups of said prepolymer have been etherified with a C.sub.4 -C.sub.10 alcohol; (b) creating an emulsion of said organic solution in a continuous phase aqueous solution comprising water and a surface-active agent, wherein said emulsion comprises discrete droplets of said organic solution, there being formed thereby an interface between the discrete droplets of organic solution and the surrounding continuous phase aqueous solution; and (c) causing in situ self-condensation and curing of said amino resin prepolymer in the organic phase of said discrete droplets adjacent to said interface by simultaneously heating said emulsion to a temperature between about 20.degree. C. to about 100.degree. C., and adding to said emulsion an acidifying agent and maintaining said emulsion at a pH of between about 0 to about 4 for a sufficient period of time to allow substantial completion of in situ condensation of said resin prepolymers to convert the liquid droplets of said organic solution to capsules consisting of solid permeable polymer shells enclosing said liquid material.Also disclosed are the microcapsules formed by the above-described process.
摘要翻译：在多孔壳内含有基本上不溶于水的液体物质如苯胺除草剂和任选地除草剂解毒剂的微胶囊通过所述外壳来实现所述除草剂（和任选的所述解毒剂）的缓慢释放速率，由一种方法，其包括（a）提供包含所述材料的有机溶液和溶解在其中的醚化氨基树脂预聚物，其中约50％至约98％的所述预聚物的羟甲基已用C4-C10醇醚化; （b）在包含水和表面活性剂的连续相水溶液中产生所述有机溶液的乳液，其中所述乳液包含离散的所述有机溶液的液滴，由此形成离散的有机溶液液滴和周围连续相水溶液; 和（c）通过将所述乳液同时加热至约20℃至约100℃的温度，使所述氨基树脂预聚物在与所述界面相邻的所述离散液滴的有机相中原位自缩合和固化，并向所述乳液中加入酸化剂并将所述乳液保持在约0至约4的pH下足够的时间，以使基本上完成所述树脂预聚物的原位缩合以将所述有机溶液的液滴转化为胶囊由包围所述液体材料的固体可渗透聚合物壳组成。还公开了通过上述方法形成的微胶囊。

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