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1. 发明授权

US5182353A Method for bonding an analyte-sensitive dye compound to an addition-cure silicone 失效
标题翻译：将分析物敏感染料化合物与加成固化的硅氧烷结合的方法
公开(公告)号：US5182353A
公开(公告)日：1993-01-26
申请号：US557624
申请日：1990-07-24
申请人： Henry K. Hui , George A. Divers, III , Carmen Soikowski
发明人： Henry K. Hui , George A. Divers, III , Carmen Soikowski
IPC分类号： C07F7/08 , C08G77/38 , G01N31/22
CPC分类号： C07F7/0849 , C08G77/38 , G01N31/223 , G01N31/225
摘要： A method for covalently bonding an analyte sensitive dye compound to an addition-cure silicone is disclosed. The method includes a first step of functionalizing the dye compound to provide a linker arm with an isolated multiple bond. A second step include hydrosilylating the functionalized dye with polymethylhydrosiloxane. The resulting compound is cross-linked with vinyl-terminated polysiloxane in a third and final step.
摘要翻译：公开了一种将分析物敏感染料化合物共价键合到加成固化硅氧烷上的方法。该方法包括使染料化合物官能化以提供具有分离的多键的连接臂的第一步骤。第二步包括用聚甲基氢硅氧烷将官能化染料加氢化硅烷化。所得化合物在第三步和最终步骤中与乙烯基封端的聚硅氧烷交联。

2. 发明授权

US5155046A System and method for measuring oxygen in the presence of halothane 失效
标题翻译：用于测定氧气存在的氧气的系统和方法
公开(公告)号：US5155046A
公开(公告)日：1992-10-13
申请号：US565511
申请日：1990-08-10
申请人： Henry K. Hui , Samuel D. Riccitelli , Terry J. Lumsden , George A. Divers, III
发明人： Henry K. Hui , Samuel D. Riccitelli , Terry J. Lumsden , George A. Divers, III
IPC分类号： G01N21/64 , G01N31/22
CPC分类号： G01N21/643 , G01N21/7703 , G01N2021/6421 , G01N2021/6432 , G01N2021/6434 , G01N2021/6484 , G01N2021/772 , G01N2021/775 , G01N2021/7786 , Y10T436/207497 , Y10T436/209163
摘要： The system for measuring the concentration of oxygen in a fluid sample which may also contain halothane includes a sensor having a matrix containing a first indicator dye which fluoresces at a known wavelength when irradiated with light of a specific wavelength and containing a second indicator dye which fluoresces at a different emission wavelength upon irradiation with light of a similar or different specific wavelength. The fluorescence of the first and second indicator dyes are quenched to a different degree by the presence of oxygen, but the fluorescence of the indicator dyes is quenched to the same degree by halothane. Means are provided for irradiating the indicator dyes in the matrix with the appropriate wavelengths of light, and means are provided for measuring the resultant intensity of fluorescence of the indicator dyes at the different wavelengths of fluorescence. Means are also provided for determining the ratio of the intensity of the different wavelengths of the fluorescence of the indicator dyes, to provide an indication of the concentration of oxygen in the sample measured.

3. 发明授权

US4693851A Purification of acid halides 失效
标题翻译：酰卤的纯化
公开(公告)号：US4693851A
公开(公告)日：1987-09-15
申请号：US834703
申请日：1986-02-28
申请人： Mark A. Bannick , George A. Divers, III , Viktors Jansons
发明人： Mark A. Bannick , George A. Divers, III , Viktors Jansons
IPC分类号： C07C51/64
CPC分类号： C07C51/64
摘要： A method of purifying an aromatic carboxylic acid halide, for example p-phenoxybenzoyl chloride, comprising the steps of: (a) adding an acidic catalyst, for example a molecular sieve, to the acid halide; (b) heating the resulting mixture of the acidic catalyst and the acid halide to a temperature of about 180.degree. C. to about 250.degree. C. for a period of at least 0.5 hours; (c) distilling the mixture to obtain acid halide substantially free of aldehyde and the halo derivative thereof. Optionally, a reactive aromatic compound may be added to the mixture of the acid halide and the acidic catalyst before the heating step. The process is particularly useful for providing aromatic acid halides of sufficient purity for preparing melt stable aromatic polyketones.
摘要翻译：一种纯化芳族羧酸卤化物的方法，例如对苯氧基苯甲酰氯，包括以下步骤：（a）向酸式卤化物中加入酸性催化剂，例如分子筛; （b）将所得酸性催化剂和酰卤的混合物加热至约180℃至约250℃的温度至少0.5小时; （c）蒸馏混合物以获得基本上不含醛的酰卤及其卤代衍生物。任选地，可以在加热步骤之前将反应性芳族化合物加入到酰卤和酸性催化剂的混合物中。该方法特别可用于提供足够纯度的用于制备熔融稳定的芳族聚酮的芳族酰卤。

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