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1. 发明授权

US07816392B2 Crystalline modifications to pyraclostrobin 有权
标题翻译：结晶修饰的pyraclostrobin
公开(公告)号：US07816392B2
公开(公告)日：2010-10-19
申请号：US11917976
申请日：2006-06-19
申请人： Hans Ziegler , Winfried Mayer , Thomas Kröhl , Karl-Heinrich Schneider , Gerhard Cox , Peter Erk , Uwe Josef Vogelbacher , Rainer Noack , Roland Götz , Jörg Wuckelt , Matthias Rauls
发明人： Hans Ziegler , Winfried Mayer , Thomas Kröhl , Karl-Heinrich Schneider , Gerhard Cox , Peter Erk , Uwe Josef Vogelbacher , Rainer Noack , Roland Götz , Jörg Wuckelt , Matthias Rauls
IPC分类号： A01N43/56 , A01P3/00 , C07D231/18
CPC分类号： A01N47/24 , C07D231/22 , A01N25/04 , A01N25/02 , A01N2300/00
摘要： The present invention relates to novel crystalline modifications of pyraclostrobin, to processes for their preparation and to the use of the novel modifications for preparing crop protection compositions.
摘要翻译：本发明涉及嘧菌酯的新结晶改性，其制备方法以及用于制备作物保护组合物的新型修饰用途。

2. 发明授权

US08404734B2 Crystalline modifications of pyraclostrobin 有权
标题翻译：吡喹酮的结晶修饰
公开(公告)号：US08404734B2
公开(公告)日：2013-03-26
申请号：US12883216
申请日：2010-09-16
申请人： Hans Ziegler , Winfried Mayer , Thomas Kroehl , Karl-Heinrich Schneider , Gerhard Cox , Peter Erk , Uwe Josef Vogelbacher , Rainer Noack , Roland Goetz , Joerg Wuckelt , Matthias Rauls
发明人： Hans Ziegler , Winfried Mayer , Thomas Kroehl , Karl-Heinrich Schneider , Gerhard Cox , Peter Erk , Uwe Josef Vogelbacher , Rainer Noack , Roland Goetz , Joerg Wuckelt , Matthias Rauls
IPC分类号： A01N43/56 , C07D231/22 , A01P3/00
CPC分类号： A01N47/24 , C07D231/22 , A01N25/04 , A01N25/02 , A01N2300/00
摘要： The present invention relates to novel crystalline modifications of pyraclostrobin, to processes for their preparation and to the use of the novel modifications for preparing crop protection compositions.
摘要翻译：本发明涉及嘧菌酯的新结晶改性，其制备方法以及用于制备作物保护组合物的新型修饰用途。

3. 发明申请

US20080234350A1 Crystalline Modifications to Pyraclostrobin 有权
标题翻译：结晶修饰吡喹酮
公开(公告)号：US20080234350A1
公开(公告)日：2008-09-25
申请号：US11917976
申请日：2006-06-19
申请人： Hans Ziegler , Winfried Mayer , Thomas Krohl , Karl-Heinrich Schneider , Gerhard Cox , Peter Erk , Uwe Josef Vogelbacher , Rainer Noack , Roland Gotz , Jorg Wuckelt , Matthias Rauls
发明人： Hans Ziegler , Winfried Mayer , Thomas Krohl , Karl-Heinrich Schneider , Gerhard Cox , Peter Erk , Uwe Josef Vogelbacher , Rainer Noack , Roland Gotz , Jorg Wuckelt , Matthias Rauls
IPC分类号： A01N43/56 , C07D231/18 , A01P3/00
CPC分类号： A01N47/24 , C07D231/22 , A01N25/04 , A01N25/02 , A01N2300/00
摘要： The present invention relates to novel crystalline modifications of pyraclostrobin, to processes for their preparation and to the use of the novel modifications for preparing crop protection compositions.
摘要翻译：本发明涉及嘧菌酯的新结晶改性，其制备方法以及用于制备作物保护组合物的新型修饰用途。

4. 发明申请

US20050176967A1 Preparation for the production of 1,2,4-triazolymethyl-oxiranes 失效
标题翻译：制备1,2,4-三唑甲基环氧乙烷
公开(公告)号：US20050176967A1
公开(公告)日：2005-08-11
申请号：US10516727
申请日：2003-06-06
申请人： Rainer Noack , Michael Sander , Michael Henningsen
发明人： Rainer Noack , Michael Sander , Michael Henningsen
IPC分类号： C07D405/06 , C07D521/00 , C07D45/02
CPC分类号： C07D249/08 , C07D231/12 , C07D233/56
摘要： The present invention relates to a process for the preparation of 1,2,4-triazol-1-ylmethyloxiranes of the formula I in which A and B are identical or different and, independently of one another, are C1-C4-alkyl, phenyl-C1-C2-alkyl, C3-C6-cycloalkyl, C3-C6-cycloalkenyl, tetrahydropyranyl, tetrahydrofuranyl, dioxanyl or phenyl, where the phenyl radical can carry one to three substituents chosen from the group: halogen, nitro, C1-C4-alkyl, Cl-C4-alkyloxy, phenoxy, amino, C1-C2-haloalkyl or phenylsulfonyl, which comprises reacting a) an oxirane of the formula II in which A and B have the meanings given above and L is a nucleophilically substitutable leaving group, with 4-amino-1,2,4-triazole of the formula III to give 4-amino-1,2,4-triazolium salts of the formula IV and b) deaminating the 4-amino-1,2,4-triazolium salts IV with alkali metal nitrites and acid or organic nitrites to give 1,2,4-triazol-1-ylmethyloxiranes of the formula I, and to 4-aminotriazolium salts of the formula IV as intermediates.
摘要翻译：本发明涉及制备式I的1,2,4-三唑-1-基甲基环氧烷的方法，其中A和B相同或不同，且彼此独立地为C 1〜 C 1 -C 4 - 亚烷基，苯基-C 1 -C 2 - 烷基，C 3 -C C 6 -C 6 - 环烷基，C 3 -C 6 - 环烯基，四氢吡喃基，四氢呋喃基，二烷基或苯基，其中苯基可以携带一至三个选自以下的取代基：卤素，硝基，C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基，苯氧基，氨基，C 1 -C 2 - 卤代烷基或苯基磺酰基，其包括使a）式A的环氧乙烷与A和B具有式 L是具有式III的4-氨基-1,2,4-三唑的亲核可取代的离去基团，得到式IV的4-氨基-1,2,4-三唑鎓盐，和b）脱氨基具有碱金属元素的4-氨基-1,2,4-三唑鎓盐IV l亚硝酸盐和酸或有机亚硝酸盐，得到式I的1,2,4-三唑-1-基甲基环氧乙烷和作为中间体的式IV的4-氨基三唑鎓盐。

5. 发明授权

US4599425A Bis-[2,5-dithio-1,3,4-thiadiazole] and a process for its production 失效
标题翻译：双[2,5二硫代-1,3,4-噻二唑]及其制备方法
公开(公告)号：US4599425A
公开(公告)日：1986-07-08
申请号：US662141
申请日：1984-10-18
申请人： Peter Hugo , Rainer Noack
发明人： Peter Hugo , Rainer Noack
IPC分类号： C07D341/00 , C07D513/18
CPC分类号： C07D513/18
摘要： Bis-[2,5-dithio-1,3,4-thiadiazole] corresponding to the following formula: ##STR1## is obtained by reacting 2,5-dimercapto-1,3,4-thiadiazole and hydrogen peroxide in the absence of other reactants.
摘要翻译：对应于下式的双 - [2,5-二硫代-1,3,4-噻二唑]：通过使2,5-二巯基-1,3,4-噻二唑和过氧化氢在不存在其他反应物。

6. 发明授权

US4347113A Oxygen content exhaust gas sensor, and method of its manufacture 失效
标题翻译：含氧废气传感器及其制造方法
公开(公告)号：US4347113A
公开(公告)日：1982-08-31
申请号：US133811
申请日：1980-03-25
申请人： Hermann Fischer , Karl-Hermann Friese , Hans-Ulrich Gruber , Wolfgang Heinemann , Gunter Knoll , Ernst Linder , Helmut Maurer , Rainer Noack , Leo Steinke , Lothar Weber , Helmut Weyl
发明人： Hermann Fischer , Karl-Hermann Friese , Hans-Ulrich Gruber , Wolfgang Heinemann , Gunter Knoll , Ernst Linder , Helmut Maurer , Rainer Noack , Leo Steinke , Lothar Weber , Helmut Weyl
IPC分类号： G01N27/409 , G01N27/407 , G01N27/413 , H01M4/88 , H01M8/12 , G01N27/58
CPC分类号： G01N27/4075 , G01N27/4078 , H01M4/881 , H01M4/8885 , H01M4/9066 , H01M8/1213 , H01M4/905 , Y02P70/56
摘要： To improve operation and output voltage, particularly at 400.degree. C. and less, an oxygen sensor, especially adapted to determine oxygen content of automotive exhaust gases, is constructed by utilizing two electrodes applied on a body of stabilized zirconium dioxide, for example a closed tube, by making an electrode exposed to the exhaust gases in form of a mixture of finely dispersed ceramic material and a platinum-rhodium alloy, the ceramic material being present at about 40% (by volume) and 60% (by volume) platinum-rhodium alloy of 50-94% platinum and 50-6% rhodium (by weight). The second electrode, exposed to a reference gas comprises an alloy of palladium and another noble metal in a ratio of about 19-90% (by weight) Pd and 81-10% (by weight) noble metal. This electrode may also contain up to 40% (by volume) finely dispersed ceramic material. The electrode exposed to the exhaust gases is covered with a porous coating. The electrodes can be applied as aqueous or organic solutions of soluble noble metal compounds or suspensions, colloidal suspensions, with organic solvents, and the like, and subsequent sintering.
摘要翻译：为了提高操作和输出电压，特别是在400℃以下，特别适用于测定汽车废气氧含量的氧气传感器是通过利用施加在稳定二氧化锆体上的两个电极构成的，例如封闭的通过使电极以细分散的陶瓷材料和铂 - 铑合金的混合物的形式暴露于废气，陶瓷材料以约40％（体积）和60％（体积）的铂 - 铑合金为50-94％铂和50-6％铑（重量）。暴露于参考气体的第二电极包括钯和另一贵金属的合金，其比例为约19-90％（重量）的Pd和81-10％（重量）的贵金属。该电极还可以含有高达40％（体积）的细分散的陶瓷材料。暴露于废气的电极被多孔涂层覆盖。电极可以作为可溶性贵金属化合物或悬浮液，胶体悬浮液，有机溶剂等的水溶液或有机溶液，以及随后的烧结。

7. 发明授权

US08604071B2 Method for producing hydroxymethyl diphenyloxiranes and corresponding 1-azolylmethyl-1,2-diphenyloxiranes 失效
标题翻译：羟甲基二苯基环氧乙烷和相应的1-吡唑基甲基-1,2-二苯基环氧乙烷的制备方法
公开(公告)号：US08604071B2
公开(公告)日：2013-12-10
申请号：US13147648
申请日：2010-02-04
申请人： Rainer Noack , Clemens Palm , Carsten Groening , Gunter Lipowsky
发明人： Rainer Noack , Clemens Palm , Carsten Groening , Gunter Lipowsky
IPC分类号： A61K31/41 , A61K31/415 , C07D207/00 , C07D249/00
CPC分类号： C07D303/14 , C07D303/08 , C07D405/06
摘要： The present invention relates to a method for producing 1-hydroxymethyl-1,2-diphenyloxiranes from 2,3-diphenylpropenals by means of epoxidation and reduction. The formation of objectionable by-products can be suppressed in that the reduction is started before the 2,3-5 diphenylpropenal is completely converted. The hydroxymethyl diphenyloxiranes represent valuable intermediate products for producing 1-azolylmethyl-1,2-diphenyloxiranes, wherein the latter can be easily produced from said intermediate products by introducing the azolyl group.
摘要翻译：本发明涉及通过环氧化和还原从2,3-二苯基丙烷生产1-羟甲基-1,2-二苯基环氧乙烷的方法。可以抑制令人反感的副产物的形成，因为在2,3,5-二苯基丙烷完全转化之前还原开始。羟甲基二苯基环氧乙烷代表产生1-噻唑基甲基-1,2-二苯基环氧乙烷的有价值的中间产物，其中后者可以通过引入唑基来容易地从所述中间产物产生。

8. 发明申请

US20110295019A1 Method for Producing Hydroxymethyl Diphenyloxiranes and Corresponding 1-azolylmethyl-1,2-diphenyloxiranes 失效
标题翻译：生产羟甲基双苯环氧乙烷的方法及相应的1-吖唑基甲基-1,2-二苯基环氧乙烷
公开(公告)号：US20110295019A1
公开(公告)日：2011-12-01
申请号：US13147648
申请日：2010-02-04
申请人： Rainer Noack , Clemens Palm , Carsten Gröning , Gunter Lipowsky
发明人： Rainer Noack , Clemens Palm , Carsten Gröning , Gunter Lipowsky
IPC分类号： C07D249/08 , C07D233/64 , C07D301/19
CPC分类号： C07D303/14 , C07D303/08 , C07D405/06
摘要： The present invention relates to a method for producing 1-hydroxymethyl-1,2-diphenyloxiranes from 2,3-diphenylpropenals by means of epoxidation and reduction. The formation of objectionable by-products can be suppressed in that the reduction is started before the 2,3-5 diphenylpropenal is completely converted. The hydroxymethyl diphenyloxiranes represent valuable intermediate products for producing 1-azolylmethyl-1,2-diphenyloxiranes, wherein the latter can be easily produced from said intermediate products by introducing the azolyl group.
摘要翻译：本发明涉及通过环氧化和还原从2,3-二苯基丙烷生产1-羟甲基-1,2-二苯基环氧乙烷的方法。可以抑制令人反感的副产物的形成，因为在2,3,5-二苯基丙烷完全转化之前还原开始。羟甲基二苯基环氧乙烷代表产生1-噻唑基甲基-1,2-二苯基环氧乙烷的有价值的中间产物，其中后者可以通过引入唑基来容易地从所述中间产物产生。

9. 发明申请

US20070093681A1 Method for the production of 2,3-cis-substituted 2-aryl propenals 失效
标题翻译： 2,3-顺式取代的2-芳基丙烯醛的制备方法
公开(公告)号：US20070093681A1
公开(公告)日：2007-04-26
申请号：US10581033
申请日：2004-12-14
申请人： Rainer Noack , Lothar Rub , Clemens Palm
发明人： Rainer Noack , Lothar Rub , Clemens Palm
IPC分类号： C07C45/72
CPC分类号： C07C47/24 , C07C45/74
摘要： The present invention relates to a process for preparing 2,3-cis-substituted 2-arylpropenals by condensing a 2-arylacetaldehyde I with a nonenolizable aldehyde compound II in the presence of a base, which comprises carrying out the reaction in a solvent mixture which includes at least one water-miscible solvent and water in a Vsolvent:Vwater ratio of from 10:1 to 0.5:1.
摘要翻译：本发明涉及通过在碱的存在下将2-芳基乙醛I与不可烯化的醛化合物II缩合制备2,3-顺式取代的2-芳基丙酮的方法，该方法包括在溶剂混合物中进行反应包括至少一种水混溶性溶剂和10:1至0.5:1的VTA溶剂：V / S水比的水。

10. 发明授权

US07368464B2 Preparation for the production of 1,2,4-triazolylmethyl-oxiranes 失效
标题翻译：制备1,2,4-三唑基甲基环氧乙烷
公开(公告)号：US07368464B2
公开(公告)日：2008-05-06
申请号：US10516727
申请日：2003-06-06
申请人： Rainer Noack , Michael Sander , Michael Henningsen
发明人： Rainer Noack , Michael Sander , Michael Henningsen
IPC分类号： A61K31/41 , C07D249/08
CPC分类号： C07D249/08 , C07D231/12 , C07D233/56
摘要： The present invention relates to a process for the preparation of 1,2,4-triazol-1-ylmethyloxiranes of the formula I in which A and B are identical or different and, independently of one another, are C1-C4-alkyl, phenyl-C1-C2-alkyl, C3-C6-cycloalkyl, C3-C6-cycloalkenyl, tetrahydropyranyl, tetrahydrofuranyl, dioxanyl or phenyl, where the phenyl radical can carry one to three substituents chosen from the group: halogen, nitro, C1-C4-alkyl, Cl-C4-alkyloxy, phenoxy, amino, C1-C2-haloalkyl or phenylsulfonyl, which comprises reacting a) an oxirane of the formula II in which A and B have the meanings given above and L is a nucleophilically substitutable leaving group, with 4-amino-1,2,4-triazole of the formula III to give 4-amino-1,2,4-triazolium salts of the formula IV and b) deaminating the 4-amino-1,2,4-triazolium salts IV with alkali metal nitrites and acid or organic nitrites to give 1,2,4-triazol-1-ylmethyloxiranes of the formula I, and to 4-aminotriazolium salts of the formula IV as intermediates.
摘要翻译：本发明涉及制备式I的1,2,4-三唑-1-基甲基环氧烷的方法，其中A和B相同或不同，且彼此独立地为C 1〜 C 1 -C 4 - 亚烷基，苯基-C 1 -C 2 - 烷基，C 3 -C C 6 -C 6 - 环烷基，C 3 -C 6 - 环烯基，四氢吡喃基，四氢呋喃基，二烷基或苯基，其中苯基可以携带一至三个选自以下的取代基：卤素，硝基，C 1 -C 4 - 烷基，C 1 -C 4 - 烷氧基，苯氧基，氨基，C 1 -C 2 - 卤代烷基或苯基磺酰基，其包括使a）式A的环氧乙烷与A和B具有式 L是具有式III的4-氨基-1,2,4-三唑的亲核可取代的离去基团，得到式IV的4-氨基-1,2,4-三唑鎓盐，和b）脱氨基具有碱金属元素的4-氨基-1,2,4-三唑鎓盐IV l亚硝酸盐和酸或有机亚硝酸盐，得到式I的1,2,4-三唑-1-基甲基环氧乙烷和作为中间体的式IV的4-氨基三唑鎓盐。

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