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1. 发明授权

US6099636A N,N'-dimethylperylene-3,4,9,10-tetracarboxylic acid diimide pigments suitable for water-based paints 失效
标题翻译：适用于水性涂料的N，N'-二甲基亚丙基-3,4,9,10-四羧酸二酰亚胺颜料
公开(公告)号：US6099636A
公开(公告)日：2000-08-08
申请号：US101444
申请日：1998-07-16
申请人： Georg Henning , Peter Blaschka , Arno Bohm
发明人： Georg Henning , Peter Blaschka , Arno Bohm
IPC分类号： C09B5/62 , C09B67/08 , C09B67/22 , C09D7/00 , C09D5/02
CPC分类号： C09B67/0008 , C09B5/62 , C09D7/007
摘要： A N,N'-dimethylperylene-3,4,9,10-tetracarboxylic diimide pigment suitable for aqueous basecoats is obtainable by coating the diimide, suspended in an aqueous medium, with a carboxyl-carrying resin in the presence of 3,4-dicarboximidoperylene-9-sulfonic acid or salts thereof and with a C.sub.8 -C.sub.8 -alkyl- or-alkenylamine, isolating and drying the coated dimide and then subjecting it to dry milling.
摘要翻译： PCT No.PCT / EP97 / 00064 Sec。 371日期：1998年7月16日 102（e）1998年7月16日PCT 1997年1月9日PCT PCT。公开号WO97 / 26301 日期1997年7月24日适用于底漆水溶液的N，N'-二甲基亚丙基-3,4,9,10-四羧酸二酰亚胺颜料可通过在存在下将羧基载体树脂悬浮于含水介质中的二酰亚胺的3,4-二羧基亚苯基-9-磺酸或其盐和C8-C8-烷基 - 或 - 链烯基胺，分离并干燥涂覆的二聚体，然后将其进行干研磨。

2. 发明授权

US6063181A 1,7-disubstituted perylene-3,4,9, 10-tetracarboxylic acids, their dianhydrides and diimides of said acids 失效
标题翻译： 1,7-二取代的苝-3,4,9,10-四羧酸，它们的二酸酐和所述酸的二酰亚胺
公开(公告)号：US6063181A
公开(公告)日：2000-05-16
申请号：US91263
申请日：1998-06-18
申请人： Arno Bohm , Harald Arms , Georg Henning , Peter Blaschka
发明人： Arno Bohm , Harald Arms , Georg Henning , Peter Blaschka
IPC分类号： C07D471/06 , C07C65/15 , C07C65/19 , C07D493/06 , C09B5/02 , C09B5/62 , C09D7/00 , C09D11/037 , C09K11/06 , C09B3/14
CPC分类号： C07D493/06 , C07C65/15 , C07C65/19 , C09B5/024 , C09B5/62 , C09D11/037 , C09D7/007 , C09K11/06
摘要： 1,7-Disubstituted perylene-3,4,9,10-tetracarboxylic dianhydrides I and perylere-3,4,9,10-tetracarboxylic acids Ia ##STR1## where L.sup.1, L.sup.2 independently of one another are 1,2-ethylene, 1,2-ethenylene and 1,2-ethynylene, andR.sup.1, R.sup.2 independently of one another are hydrogen or substituted or unsubstituted C.sub.1 -C.sub.30 -alkyl,their preparation and use as pigments, laser dyes and precursors for preparing fluorescent dyes, polymeric colorants, pigments and pigment additives, and also 1,7-disubstituted perylene-3,4,9,10-tetracarboxylic diimides (VI) as their intermediates.
摘要翻译： PCT No.PCT / EP96 / 05525 Sec。 371日期1998年6月18日 102（e）1998年6月18日PCT 1996年12月11日PCT PCT。出版物WO97 / 22608 日期1996年6月26日7,7-二取代苝-3,4,9,10-四羧酸二酐I和萜烯-3,4,9,10-四羧酸Ia，其中L1，L2彼此独立地为1,2- 乙烯，1,2-亚乙烯基和1,2-亚乙炔基，R 1，R 2彼此独立地是氢或取代或未取代的C 1 -C 30烷基，它们作为颜料的制备和用途，激光染料和用于制备荧光染料的前体，聚合物着色剂，颜料和颜料添加剂，以及作为其中间体的1,7-二取代的苝-3,4,9,10-四羧酸二酰亚胺（VI）。

3. 发明授权

US6143905A 1,7-diaroxy- or 1,7-arylthio-substituted perylene-3,4,9,10-tetracarboxylic acids, their dianhydrides and diimides 失效
标题翻译： 1,7-二氧基 - 或1,7-芳硫基取代的二萘嵌苯-3,4,9,10-四羧酸，它们的二酐和二酰亚胺
公开(公告)号：US6143905A
公开(公告)日：2000-11-07
申请号：US091262
申请日：1998-06-18
申请人： Arno Bohm , Harald Arms , Georg Henning , Peter Blaschka
发明人： Arno Bohm , Harald Arms , Georg Henning , Peter Blaschka
IPC分类号： C07D471/06 , C07C65/15 , C07C65/24 , C07D493/06 , C09B3/14 , C09B5/02 , C09B5/62 , C09K11/06 , C07C63/48
CPC分类号： C07D493/06 , C07C65/15 , C07C65/24 , C09B5/024 , C09B5/62 , C09K11/06
摘要： 1,7-Disubstituted perylene-3,4,9,10-tetracarboxylic dianhydrides I and perylene-3,4,9,10-tetracarboxylic acids Ia ##STR1## where R is substituted or unsubstituted aryloxy, arylthio, hetaryloxy or hetarylthio,their preparation and use as pigments, laser dyes and precursors for preparing fluorescent dyes, polymeric colorants, pigments and pigment additives, and 1,7-disubstituted perylene-3,4,9,10-tetracarboxylic diimides (VI) as intermediates thereof.
摘要翻译： PCT No.PCT / EP96 / 05519 371日期1998年6月18日 102（e）1998年6月18日PCT 1996年12月11日PCT PCT。公开号WO97 / 22607 日期：1996年6月26日7,7-二取代的苝-3,4,9,10-四羧酸二酐I和苝-3,4,9,10-四羧酸Ia，其中R是取代或未取代的芳氧基，芳硫基，苯氧基或杂芳硫基，它们作为颜料的制备和用途，用于制备荧光染料的激光染料和前体，聚合物着色剂，颜料和颜料添加剂以及作为其中间体的1,7-二取代的二萘嵌苯-3,4,9,10-四羧酸二酰亚胺（VI）。

4. 发明申请

US20050131220A1 Method for the production of perylen-3,4:9,10-tetracarboxylic acid diimides and perylen-3,4:9,10-tetracarboxylic acid dianhydride and naphtalene-1,8-dicarboxylimides 有权
公开(公告)号：US20050131220A1
公开(公告)日：2005-06-16
申请号：US10510579
申请日：2003-04-15
申请人： Bernhard Dung , Felix Muller , Arno Bohm , Willi Helfer , Volker Wevrauch , Georg Henning
发明人： Bernhard Dung , Felix Muller , Arno Bohm , Willi Helfer , Volker Wevrauch , Georg Henning
IPC分类号： C07D221/14 , C07D487/06 , C09B5/62 , C09B57/08 , C07D471/02
CPC分类号： C09B5/62 , C09B57/08
摘要： A process for preparing perylene-3,4:9,10-tetracarboxylic diimides of the general formula I where R is C1-C30-alkyl whose carbon chain may be interrupted by one or more —O— moieties and/or which may be substituted by one or more substituents selected from the group consisting of C5-C8-cycloalkyl (which may be substituted by one or more C1-C6-alkyl substituents), phenyl or phenyl-C1-C6-alkyl (which may each be substituted by one or more C1-C18-alkyl and/or C1-C6-alkoxy substituents), —OCOR1, —N(R1)2, —SO2NH2, —SO2N(R1)2, —CON(R1)2 and —COOR1; C5-C8-cycloalkyl whose carbon skeleton may be interrupted by one or more moieties selected from the group consisting of —O—, —S— and —NR2- and/or which may be substituted by one or more C1-C6-alkyl substituents; phenyl, phenyl-C1-C6-alkyl, naphthyl or hetaryl, which may each be substituted by one or more substituents selected from the group consisting of C1-C18-alkyl, C1-C6-alkoxy, phenylazo, naphthylazo, pyridylazo, pyrimidylazo, cyano, —N(R1)2, —CON(R1)2 and —COOR1; R1 is C1-C6-alkyl, C5-C8-cycloalkyl, phenyl or phenyl-C1-C6-alkyl; R2 is C1-C6-alkyl, phenyl or phenyl-C1-C6-alkyl, by dimerizing a naphthalene-1,8-dicarboximide of the formula II comprises effecting said dimerizing in a reaction medium consisting essentially of an a polar aprotic organic solvent and an alkali metal base and subsequently reoxidizing the resulting alkali metal salt of the leuco form of the perylene-3,4:9,10-tetracarboxylic diimide in the presence of a polar solvent, and also preparation of perylene-3,4:9,10-tetracarboxylic dianhydride and naphthalene-1,8-dicarboximides.

5. 发明申请

US20080161569A1 PREPARATION OF PERYLEN-3,4:9,10-TETRACARBOXYLIC DIANHYDRIDE AND ALSO OF NAPHTALENE-1,8-DICARBOXIMIDES 有权
标题翻译：季戊四醇3,4：9,10-四羧酸二乙酰胺的制备以及壬二酮-1,8-二氧杂环己酮的制备
公开(公告)号：US20080161569A1
公开(公告)日：2008-07-03
申请号：US11955605
申请日：2007-12-13
申请人： Bernhard DUNG , Felix Mueller , Arno Bohm , Willi Helfer , Volker Weyrauch , Georg Henning
发明人： Bernhard DUNG , Felix Mueller , Arno Bohm , Willi Helfer , Volker Weyrauch , Georg Henning
IPC分类号： C07D471/00 , C07D221/14
CPC分类号： C09B5/62 , C09B57/08
摘要： A process for preparing perylene-3,4:9,10-tetracarboxylic dianhydride, comprising: dimerizing a naphthalene-1,8-dicarboximide of the formula IIa; reoxidizing the resulting alkali metal salt of the leuco form of the perylene-3,4:9,10-tetracarboxylic diimide of the formula Ia; hydrolyzing the diimide to the tetraalkali metal salt of perylene-3,4:9,10-tetracarboxylic acid in the presence of an inert organic solvent, of an alkali metal base and of water; and subjecting the tetraalkali metal salt of perylene-3,4:9,10-tetracarboxylic acid to the action of an aqueous inorganic acid to convert it into perylene-3,4:9,10-tetracarboxylic dianhydride; wherein R3 is cyclohexyl or phenyl which may each be substituted by up to three C1-C4-alkyl radicals, and the dimerizing is in a substantially homogeneous reaction medium consisting essentially of an apolar aprotic organic solvent and an alkali metal base.
摘要翻译：一种制备苝-3,4：9,10-四羧酸二酐的方法，包括：使式IIa的萘-1,8-二甲酰亚胺二聚化; 重新氧化得到的无水形式的式Ia的苝-3,4：9,10-四羧酸二酰亚胺的碱金属盐; 在惰性有机溶剂，碱金属碱和水的存在下将二酰亚胺水解成苝-3,4：9,10-四羧酸的四碱金属盐; 并将苝-3,4：9,10-四羧酸的四碱金属盐作为无机酸水溶液的作用，将其转化成苝-3,4：9,10-四羧酸二酐; 其中R 3是可以被至多三个C 1 -C 4 - 烷基取代的环己基或苯基，二聚是在基本均匀的反应介质中，基本上由非极性非质子有机溶剂和碱金属碱组成。

6. 发明授权

US06326494B1 1,7-Diaroxy- or 1,7-arylthio-substituted perylene-3,4,9,10-tetracarboxylic acids, their dianhydrides and diimides 有权
标题翻译： 1,7-二氧基 - 或1,7-芳硫基取代的二萘嵌苯-3,4,9,10-四羧酸，它们的二酐和二酰亚胺
公开(公告)号：US06326494B1
公开(公告)日：2001-12-04
申请号：US09631291
申请日：2000-08-02
申请人： Arno Böhm , Harald Arms , Georg Henning , Peter Blaschka
发明人： Arno Böhm , Harald Arms , Georg Henning , Peter Blaschka
IPC分类号： C07D31473
CPC分类号： C07D493/06 , C07C65/15 , C07C65/24 , C09B5/024 , C09B5/62 , C09K11/06
摘要： A 1,7-disubstituted perylene-3,4,9,10-tetracarboxylic diimide of the general formula VI: Compositions or products comprising the compound of formula VI. Compositions comprising 1,7-diaroxy- or 1,7-diarylthio-substituted perylene-3,4,9,10-tetracarboxylic dianhydrides (I) or 1,7-diaroxy- or 1,7-diarylthio-substituted perylene-3,4,9,10-tetracarboxylic acids (Ia).
摘要翻译：通式VI的1,7-二取代的二萘嵌苯-3,4,9,10-四羧酸二酰亚胺：包含式VI化合物的组合物或产物。包含1,7-二芳氧基或1,7-二芳基硫代取代的二萘嵌苯-3,4,9,10-四羧酸二酐（I）或1,7-二芳氧基或1,7-二芳硫基取代的二萘嵌苯-3的组合物， 4,9,10-四羧酸（Ia）。

7. 发明授权

US06184378B2 1,7-disubstituted perylene-3,4,9,10-tetracarboxylic acids, their dianhydrides and diimides 有权
标题翻译： 1,7-二取代的苝-3,4,9,10-四羧酸，它们的二酸酐和二酰亚胺
公开(公告)号：US06184378B2
公开(公告)日：2001-02-06
申请号：US09404534
申请日：1999-09-24
申请人： Arno Böhm , Harald Arms , Georg Henning , Peter Blaschka
发明人： Arno Böhm , Harald Arms , Georg Henning , Peter Blaschka
IPC分类号： C07D47106
CPC分类号： C07D493/06 , C07C65/15 , C07C65/19 , C09B5/024 , C09B5/62 , C09D7/41 , C09D11/037 , C09K11/06
摘要： A 1,7-disubstituted perylene-3,4,9,10-tetracarboxylic diimide of the general formula VI where X1 and X1 re independently bromine or —L—R, where L is 1,2-ethylene, 1,2-ethenylene or 1,2-ethynylene and R is hydrogen or C1-C30-alkyl whose carbon chain can be interrupted by one or more groups —O—, —S—, —NR3—, —CO— and/or —SO2— and/or which can be substituted one or more times by —COOR3, —SO3R3, hydroxyl, cyano, C1-C6-alkoxy, C5-C8-cycloalkyl or aryl or by a 5- to 7-membered heterocyclic radical which is attached via a nitrogen atom and can include further heteroatoms and/or can be aromatic, R3 being hydrogen or C1-C6-alkyl.
摘要翻译：通式VI的1,7-二取代的二萘嵌苯-3,4,9,10-四羧酸二酰亚胺X 1和X 1独立地为溴或-LR，其中L为1,2-亚乙基，1,2-亚乙烯基或1,2-亚乙基，亚乙炔基，R是氢或C 1 -C 30 - 烷基，其碳链可被一个或多个-O - ， - S - ， - NR 3 - ， - CO-和/或-SO 2 - 基团间隔，和/或可被一个或更多次通过-COOR 3，-SO 3 R 3，羟基，氰基，C 1 -C 6 - 烷氧基，C 5 -C 8 - 环烷基或芳基或通过氮原子连接的5-至7-元杂环基，并且可以包括另外的杂原子和/或可以是芳族的，R 3是氢或C 1 -C 6 - 烷基。

8. 发明授权

US07807836B2 Preparation of perylen-3,4:9,10-tetracarboxylic dianhydride and also of naphtalene-1,8-dicarboximides 有权
标题翻译：苝-3,4：9,10-四羧酸二酐以及萘-1,8-二羧酰亚胺的制备
公开(公告)号：US07807836B2
公开(公告)日：2010-10-05
申请号：US11955605
申请日：2007-12-13
申请人： Bernhard Dung , Felix Mueller , Arno Boehm , Willi Helfer , Volker Weyrauch , Georg Henning
发明人： Bernhard Dung , Felix Mueller , Arno Boehm , Willi Helfer , Volker Weyrauch , Georg Henning
IPC分类号： C07D471/16 , C07D471/00
CPC分类号： C09B5/62 , C09B57/08
摘要： A process for preparing perylene-3,4:9,10-tetracarboxylic dianhydride, comprising: dimerizing a naphthalene-1,8-dicarboximide of the formula IIa; reoxidizing the resulting alkali metal salt of the leuco form of the perylene-3,4:9,10-tetracarboxylic diimide of the formula Ia; hydrolyzing the diimide to the tetraalkali metal salt of perylene-3,4:9,10-tetracarboxylic acid in the presence of an inert organic solvent, of an alkali metal base and of water; and subjecting the tetraalkali metal salt of perylene-3,4:9,10-tetracarboxylic acid to the action of an aqueous inorganic acid to convert it into perylene-3,4:9,10-tetracarboxylic dianhydride; wherein R3 is cyclohexyl or phenyl which may each be substituted by up to three C1-C4-alkyl radicals, and the dimerizing is in a substantially homogeneous reaction medium consisting essentially of an apolar aprotic organic solvent and an alkali metal base.
摘要翻译：一种制备苝-3,4：9,10-四羧酸二酐的方法，包括：使式IIa的萘-1,8-二甲酰亚胺二聚化; 重新氧化得到的无水形式的式Ia的苝-3,4：9,10-四羧酸二酰亚胺的碱金属盐; 在惰性有机溶剂，碱金属碱和水的存在下将二酰亚胺水解成苝-3,4：9,10-四羧酸的四碱金属盐; 并将苝-3,4：9,10-四羧酸的四碱金属盐作为无机酸水溶液的作用，将其转化成苝-3,4：9,10-四羧酸二酐; 其中R 3是可以被至多三个C 1 -C 4 - 烷基取代的环己基或苯基，二聚在基本上均匀的反应介质中，其基本上由非极性非质子有机溶剂和碱金属碱组成。

9. 发明授权

US4594411A Sulfonated monoazo colorant lake obtained by di-azo coupling of 5-acetylamino-2-aminobenzene-1-sulfonic acid with 1-(3'-sulfophenyl)-3-methylphyrazol-5-one 失效
标题翻译：通过5-乙酰氨基-2-氨基苯-1-磺酸与1-（3'-磺基苯基）-3-甲基吡唑-5-酮的偶氮偶合获得的磺化单偶氮染料色淀
公开(公告)号：US4594411A
公开(公告)日：1986-06-10
申请号：US617155
申请日：1984-06-06
申请人： Georg Henning
发明人： Georg Henning
IPC分类号： C09B29/01 , C09B29/50 , C09B63/00 , C09B29/03 , C09B29/10 , C09B29/36 , D06P1/39
CPC分类号： C09B29/366 , C09B29/0007 , C09B63/00 , Y10S534/01 , Y10S534/04
摘要： This invention relates to a method of dyeing thermoplastics with sulfonated monoazo colorant lakes having a sulfophenyl pyrazole substituent, of general formula ##STR1## wherein R is CH.sub.3 or COO.sup.- ; X is Cl, CH.sub.3, CH.sub.3 O, C.sub.2 H.sub.5 O, C.sub.2 H.sub.5 CONH, NH.sub.2 CONH, C.sub.6 H.sub.5 CONH, CH.sub.3 SO.sub.2 NH, C.sub.6 H.sub.5 SO.sub.2 NH, CH.sub.3 CONH, or hydrogen; Y is hydrogen, Cl, or CH.sub.3 ; Z is hydrogen or Cl, n is 0, 1 or 2; and Me.sup.+ is one equivalent of a cation selected from the group consisting of NH.sub.4.sup.+, Li.sup.+, K.sup.+, Na.sup.+, 1/2Sr.sup.2+, 1/2Mn.sup.2+, 1/2Ni.sup.2+, 1/2Ba.sup.2+, 1/2Mg.sup.2+ and 1/2Ca.sup.2+ ; with the proviso that if R is COO.sup.-, the additional equivalent charge is compensated by a further equivalent of said or another cation. These compounds, which are insoluble in organic solvents and sparingly soluble in water, are useful as lakes with good pigmentary characteristics and possessing very good lightfastness in plastics, such as polyolefins, polyvinyl chloride, polystyrene, and ABS. They are also useful in surface coatings, and particularly suitable for coloring thermoplastics. Noteworthy is their good plasticizer fastness, their high stability to heat and the absence of blooming they produce when used.
摘要翻译：本发明涉及一种通过具有通式（I）的磺酰基苯基吡唑取代基的磺化单偶氮染料盐染色热塑性塑料的方法，其中R是CH 3或COO-; X是Cl，CH 3，CH 3 O，C 2 H 5 O，C 2 H 5 CONH，NH 2 CONH，C 6 H 5 CONH，CH 3 SO 2 NH，C 6 H 5 SO 2 NH，CH 3 CONH或氢; Y是氢，Cl或CH 3; Z是氢或Cl，n是0,1或2; 和Me +是选自NH4 +，Li +，K +，Na +，1 / 2Sr2 +，1 / 2Mn2 +，1 / 2Ni2 +，1 / 2Ba2 +，1 / 2Mg2 +和1 / 2Ca2 +的阳离子的1当量。条件是如果R是COO-，则额外的等效电荷由另外的等价的所述阳离子补偿。这些不溶于有机溶剂并微溶于水的化合物可用作具有良好颜料特征的湖泊，并且在塑料如聚烯烃，聚氯乙烯，聚苯乙烯和ABS中具有非常好的耐光性。它们也可用于表面涂层，特别适用于着色热塑性塑料。值得注意的是它们具有良好的增塑剂坚牢度，它们对热的高稳定性和使用时不产生起霜。

10. 发明授权

US5131981A Coloring paper 失效
标题翻译：彩色纸
公开(公告)号：US5131981A
公开(公告)日：1992-07-21
申请号：US711378
申请日：1991-06-06
申请人： Erwin Hahn , Georg Henning , Manfred Mielke , Hans-Juergen Degen , Sigberg Pfohl
发明人： Erwin Hahn , Georg Henning , Manfred Mielke , Hans-Juergen Degen , Sigberg Pfohl
IPC分类号： D21H17/34 , D21H17/37 , D21H17/49 , D21H17/55 , D21H17/56 , D21H21/28
CPC分类号： D21H21/28 , D21H17/375
摘要： The wet-end coloring of paper with pigments and fixers is carried out by a process in which the pigment and fixer are added simultaneously to the paper pulp to be colored, and the fixer used is a cationic fixer, in an amount of from 0.01 to 3% by weight, based on the dry paper pulp to be colored.
摘要翻译：用颜料和定影剂进行的纸的湿端着色通过其中将颜料和定影剂同时加入到纸浆中以着色的方法进行，并且所使用的定影剂是阳离子定影剂，其量为0.01至基于要着色的干纸浆3％（重量）。

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