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1. 发明授权

US4271289A Oxygen-curable mercapto-functional organic compound compositions catalyzed by metal carbonyl compounds and method of forming higher molecular weight products therefrom 失效
标题翻译：由金属羰基化合物催化的可氧化巯基官能的有机化合物组合物和由其形成较高分子量产物的方法
公开(公告)号：US4271289A
公开(公告)日：1981-06-02
申请号：US99282
申请日：1979-12-03
申请人： Gary R. Homan , Chi-long Lee
发明人： Gary R. Homan , Chi-long Lee
IPC分类号： C08G75/00 , C08G75/02 , C08G75/04 , C08G75/14 , C08L81/00 , C08L81/04 , C08L83/08 , C09K3/10
CPC分类号： C08L81/04 , C08G75/14 , C09K3/1012
摘要： Compositions which are stable in the absence of oxygen are formed by mixing the following substantially in the absence of oxygen(A) 100 parts by weight of at least one mercapto-functional organic compound which contains at least two mercapto groups per molecule;(B) 0 to 200 parts by weight of at least one filler; and(C) a catalytic amount of a metal carbonyl compound selected from the group consisting of Fe(CO).sub.5, Fe.sub.2 (CO).sub.9, Fe.sub.3 (CO).sub.12, dicyclopentadienyldiiron tetracarbonyl, butadieneiron tricarbonyl, cyclohexadieneiron tricarbonyl, Ni(CO).sub.4, dicyclopentadienyldinickel dicarbonyl, Mn.sub.2 (CO).sub.10, methylcyclopentadienylmanganese tricarbonyl and cyclopentadienylcobalt dicarbonyl, preferably from 0.1 to 6 parts by weight of an iron carbonyl compound per 100 parts by weight of (A).Such compositions polymerize or cure upon exposure to oxygen. When used in layers of up to 3 millimeters thick, these compositions polymerize or cure at room temperature in a reasonable amount of time to form higher molecular weight products which are useful as coatings, impregnants or elastomeric sealants.
摘要翻译：在不存在氧的情况下稳定的组合物通过以下方式形成：基本上在不存在氧的情况下混合以下物质（A）100重量份的至少一种每分子含有至少两个巯基的巯基官能化有机化合物; （B）0〜200重量份的至少一种填料; 和（C）催化量的选自Fe（CO）5，Fe 2（CO）9，Fe 3（CO）12，四羰基二环戊二烯基二羰基，三羰基二丁基铁，三羰基环己二烯，Ni（CO）4）的金属羰基化合物，二环戊二烯基二羰基二羰基，Mn2（CO）10，甲基环戊二烯基锰三羰基和环戊二烯基钴二羰基，每100重量份的（A）优选为0.1至6重量份的羰基铁化合物。这样的组合物在暴露于氧气时聚合或固化。当以高达3毫米厚的层使用时，这些组合物在合适的时间内在室温下聚合或固化，以形成可用作涂料，浸渍剂或弹性体密封剂的较高分子量产品。

2. 发明授权

US4279792A Compositions including mercaptoorganopolysiloxanes and stannous salts of carboxylic acids 失效
标题翻译：组合物包括巯基有机聚硅氧烷和羧酸的亚锡盐
公开(公告)号：US4279792A
公开(公告)日：1981-07-21
申请号：US99301
申请日：1979-12-03
申请人： Gary R. Homan , Chi-long Lee
发明人： Gary R. Homan , Chi-long Lee
IPC分类号： B22D41/08 , B22D41/46 , C08G77/38 , C08K5/04 , C08K5/09 , C08K5/098 , C08K5/14 , C08L83/00 , C08L83/04 , C08L83/08 , C08L91/00
CPC分类号： C08K5/098 , B22D41/46 , C08K5/09 , C08K5/14
摘要： Mixing mercaptoorganopolysiloxanes with a stannous salt of a carboxylic acid, and optionally an organic peroxide and/or a filler, provides useful new compositions such as materials curable to elastomers at room temperature.
摘要翻译：将巯基有机聚硅氧烷与羧酸的亚锡盐和任选的有机过氧化物和/或填料混合，提供了有用的新组合物，例如在室温下可固化到弹性体的材料。

3. 发明授权

US4239674A Oxygen-curable mercaptoorganosiloxane compositions catalyzed by cobaltocene compounds and method of forming higher molecular weight products therefrom 失效
标题翻译：由可可可烯化合物催化的可氧化巯基有机硅氧烷组合物和由其形成较高分子量产物的方法
公开(公告)号：US4239674A
公开(公告)日：1980-12-16
申请号：US63017
申请日：1979-08-02
申请人： Gary R. Homan , Chi-long Lee
发明人： Gary R. Homan , Chi-long Lee
IPC分类号： C08L83/00 , C08G75/14 , C08G77/00 , C08G77/28 , C08K5/56 , C08L83/04 , C09K3/10 , C08L83/08
CPC分类号： C09K3/1018 , C08G75/14 , C08K5/56
摘要： Compositions stable in the absence of oxygen are formed by mixing the following substantially in the absence of oxygen(A) mercapto-functional organosiloxanes containing at least two mercapto groups per molecule,(B) optionally, a filler, and(C) a catalytic amount of a cobaltocene of the formula (R.sup.3 C.sub.5 H.sub.4)Co(C.sub.5 H.sub.4 R.sup.4), wherein each R.sup.3 and R.sup.4 is hydrogen or methyl, preferably, 0.01-6 parts by weight of (C.sub.5 H.sub.5).sub.2 Co per 100 parts by weight of (A) above.The compositions polymerize or cure upon exposure to oxygen. By utilizing various types and amounts of mercapto-functional organosiloxanes, higher molecular weight products useful as encapsulating gels, coating resins, or elastomeric sealants can be obtained by the method of exposing the compositions of the present invention to oxygen.
摘要翻译：在不存在氧的情况下稳定的组合物通过在不存在氧（A）每分子含有至少两个巯基的巯基官能的有机硅氧烷的情况下混合以下物质形成，（B）任选的填料，和（C）催化量的式（R 3 C 5 H 4）Co（C 5 H 4 R 4）的共轭二烯，其中每个R 3和R 4是氢或甲基，优选为每100重量份上述（A）为0.01-6重量份的（C 5 H 5）2 C 50。组合物在暴露于氧气时聚合或固化。通过使用各种类型和量的巯基官能的有机硅氧烷，可以通过将本发明的组合物暴露于氧气的方法获得用作包封凝胶，涂料树脂或弹性体密封剂的较高分子量产物。

4. 发明授权

US6040353A Radiation curable silicone compositions 失效
标题翻译：可辐射固化的硅酮组合物
公开(公告)号：US6040353A
公开(公告)日：2000-03-21
申请号：US199623
申请日：1998-11-25
申请人： Shedric Oneal Glover , Chi-long Lee , Wen-hong Tong
发明人： Shedric Oneal Glover , Chi-long Lee , Wen-hong Tong
IPC分类号： C08L83/07 , C08F2/46 , C08F2/50 , C08F16/12 , C08F16/32 , C08F290/00 , C08F299/08 , C09D4/00 , C09D183/04 , C09D183/06 , G03F7/039 , C08J3/28 , C08L83/06
CPC分类号： C08F16/32 , C08F16/12 , C09D183/06
摘要： This invention relates to a radiation curable silicone compositions. More particularly this invention relates to radiation curable silicone compositions comprising a vinyl ether functional silicon compound, a cationic photoinitiator, a free radical photoinitiator, and dodecylphenol. The compositions of this invention can further comprise a vinyl ether compound which is free of silicon atoms. The radiation curable silicone compositions of this invention are useful as release coating compositions which are especially suitable for release of pressure sensitive adhesives.
摘要翻译：本发明涉及可辐射固化的硅氧烷组合物。更具体地说，本发明涉及包含乙烯基醚官能的硅化合物，阳离子光引发剂，自由基光引发剂和十二烷基苯酚的可辐射固化的硅氧烷组合物。本发明的组合物还可以包含不含硅原子的乙烯基醚化合物。本发明的可辐射固化的硅氧烷组合物可用作特别适用于压敏粘合剂释放的脱模涂料组合物。

5. 发明授权

US5162560A Olefinic and acetylenic azasilacyclopentanes 失效
标题翻译：烯烃和炔属氮杂环戊烷
公开(公告)号：US5162560A
公开(公告)日：1992-11-10
申请号：US842914
申请日：1992-02-28
申请人： Russell K. King , Chi-long Lee
发明人： Russell K. King , Chi-long Lee
IPC分类号： C07F7/10 , C07F7/12 , C07F7/18
CPC分类号： C07F7/1844 , C07F7/10 , C07F7/12
摘要： Azasilacyclopentanes of the general formula ##STR1## are prepared by reacting a dialkoxyalkyl(3-chloro-2-alkylpropyl)silane with a Grignard reagent of the formula R.sup.1 MgBr in the presence of an ether, to make an alkoxyalkylalkenyl(3-chloro-2-alkylpropyl)silane which is reacted with acetyl chloride and a Lewis acid to make chloroalkylalkenyl(3-chloro-2-alkylpropyl)silane which is then reacted with an amine of the formula R.sup.3 NH.sub.2 to make the azasilacyclopentanes.
摘要翻译：通式（III-c）所示的亚氮杂环戊烷通过在醚存在下使二烷氧基烷基（3-氯-2-烷基丙基）硅烷与式R 1 MgBr的格氏试剂反应制得烷氧基烷基（3-氯-2- 烷基丙基）硅烷，其与乙酰氯和路易斯酸反应以制备氯烷基烯基（3-氯-2-烷基丙基）硅烷，然后与式R 3 NH 2的胺反应以制备氮杂环丙烷基。

6. 发明授权

US4923754A Fast ultraviolet radiation curing silicone composition 失效
公开(公告)号：US4923754A
公开(公告)日：1990-05-08
申请号：US187693
申请日：1988-04-29
申请人： Chi-long Lee , Michael A. Lutz
发明人： Chi-long Lee , Michael A. Lutz
IPC分类号： C03C25/10 , C08K5/00 , C08L83/04
CPC分类号： C08K5/00 , C03C25/106 , C08L83/04 , C08G77/20 , C08G77/24 , C08G77/28 , C08G77/70 , Y10T428/31612
摘要： Compositions which cure by UV radiation in less than one second are obtained by mixing an alkenyl containing polydiorganosiloxane, a mercapto functional crosslinker of the mercapto functional polyorganosiloxane or mercapto organic compounds, a photosensitizer, a viscosity stabilizer, and optionally a reinforcing agent. These compositions can be packaged in one container and can be used as the primary coating for optical fibers.

7. 发明授权

US4766176A Storage stable heat curable organosiloxane compositions containing microencapsulated platinum-containing catalysts 失效
标题翻译：储存稳定的可固化有机硅氧烷组合物，含有微囊化的含铂催化剂
公开(公告)号：US4766176A
公开(公告)日：1988-08-23
申请号：US75177
申请日：1987-07-20
申请人： Chi-long Lee , Donnie R. Juen , John C. Saam , Robin L. Willis, Jr.
发明人： Chi-long Lee , Donnie R. Juen , John C. Saam , Robin L. Willis, Jr.
IPC分类号： B01J13/02 , B01J31/28 , B01J35/02 , C08F8/42 , C08K9/10 , C08L83/05 , C08L83/07 , C08F8/00
CPC分类号： C08F8/42 , C08J3/241 , C08L83/04 , C08G77/12 , C08G77/20 , C08J2383/04
摘要： Storage stable, one part organosiloxane compositions that cure upon heating by a platinum-catalyzed hydrosilation reaction comprise, in addition to the organosiloxane reactants, a platinum-containing hydrosilation catalyst that is microencapsulated within one or two layers of thermoplastic organic polymers. The microcapsules are formed using known techniques.

8. 发明授权

US4584337A Aqueous emulsions containing hydrophilic silicone-organic copolymers 失效
标题翻译：含有亲水硅氧烷 - 有机共聚物的乳液
公开(公告)号：US4584337A
公开(公告)日：1986-04-22
申请号：US683303
申请日：1984-12-18
申请人： Chi-long Lee , Wen-Bin Shyu
发明人： Chi-long Lee , Wen-Bin Shyu
IPC分类号： C08F299/00 , B01D53/22 , B01D71/28 , B01D71/40 , B01D71/70 , B01D71/80 , C08F283/12 , C08F290/00 , C08F290/06 , C08F299/08 , C08G18/61 , C08G18/81 , C08L83/00 , C08L83/04 , C08L83/10 , C09D5/14 , C09D155/00 , C09D183/07 , C08L51/08
CPC分类号： C08G18/61 , C08F290/068 , C08G18/8116
摘要： This present invention provides aqueous emulsions which are capable of depositing coatings and membranes of hydrophilic, water-absorbing silicone-organic polymer elastomers. The elastomers are free radical polymerized copolymers of (A) from 50 to 95 parts by weight of block copolymers containing polydiorganosiloxane segments and polyalkyleneoxy segments which block copolymers contain terminal aliphatically unsaturated groups such as those derived from the reaction of isocyanatoethyl methacrylate with terminal free hydroxyl groups present on the polyalkyleneoxy segments and (B) from 5 to 50 parts by weight of at least one substantially water insoluble aliphatically unsaturated organic monomer which is compatible with (A) such as methyl methacrylate. The aqueous emulsions are useful for forming coatings and membranes of the above elastomers and also provide a vehicle for the deposition of coatings of such elastomers which are capable of controllably releasing bioactive agents such as insecticides or herbicides which are dispersed within the elastomer film deposited from the aqueous emulsion.
摘要翻译：本发明提供了能够沉积亲水性，吸水性有机硅聚合物弹性体的涂层和膜的水性乳液。弹性体是（A）50至95重量份的含聚二有机硅氧烷链段和聚亚烷基氧基链段的嵌段共聚物的自由基聚合共聚物，所述嵌段共聚物含有末端脂族不饱和基团，例如衍生自甲基丙烯酸异氰酸根合乙酯与末端游离羟基的反应存在于聚亚烷基氧基部分和（B）5至50重量份的与（A）如甲基丙烯酸甲酯相容的至少一种基本上不溶于水的不饱和有机单体。水乳液可用于形成上述弹性体的涂层和膜，并且还提供用于沉积这种弹性体的涂层的载体，其能够可控地释放生物活性剂如杀虫剂或除草剂，其分散在由水乳液。

9. 发明授权

US5254645A Cluster azasilacycloalkyl functional polysiloxanes 失效
标题翻译：聚氮杂环烷基官能聚硅氧烷
公开(公告)号：US5254645A
公开(公告)日：1993-10-19
申请号：US938743
申请日：1992-09-02
申请人： Russell K. King , Chi-long Lee
发明人： Russell K. King , Chi-long Lee
IPC分类号： C08G81/00 , C08G77/50 , C08G77/54 , C08K5/5425 , C08L83/04 , C08L83/05 , C08L83/07 , C08G77/26
CPC分类号： C08G77/54 , C08G77/50 , C08L83/04 , C08G77/12 , C08G77/20 , C08G77/24
摘要： Cluster azasilacycloalkyl functional polysiloxanes are prepared by combining vinyl-containing polysiloxane, polyfunctional hydrogen polysiloxane, and a platinum catalyst; reacting the combination to produce .tbd.Si--CH.sub.2 CH.sub.2 --Si.tbd. linkages and substantial amounts of unreacted Si--H groups remain in the reaction product. The Si--H groups in the reaction product are reacted with aliphatically unsaturated azasilacycloalkane forming the cluster compound. These cluster azasilacycloalkyl functional polysiloxanes cure when exposed to moisture to elastomers, sealants, encapsulants, and resins products.

10. 发明授权

US5169879A Fast ultraviolet radiation curing silicone composition 失效
标题翻译：快速紫外线固化硅胶组合物
公开(公告)号：US5169879A
公开(公告)日：1992-12-08
申请号：US495824
申请日：1990-04-19
申请人： Chi-long Lee , Michael A. Lutz
发明人： Chi-long Lee , Michael A. Lutz
IPC分类号： C03C25/10 , C08F2/50 , C08K5/00 , C08L83/04
CPC分类号： C08K5/00 , C03C25/106 , C08L83/04 , C08G77/16 , C08G77/20 , C08G77/24 , C08G77/28 , C08G77/70 , Y10S522/901
摘要： Compositions which cure by UV radiation in less than one second are obtained by mixing an alkenyl containing polydiorganosiloxane, a mercapto functional crosslinker of the mercapto functional polyorganosiloxane or mercapto organic compounds, a photosensitizer, a viscosity stabilizer, and optionally a reinforcing agent. These compositions can be packaged in one container and can be used as the primary coating for optical fibers.
摘要翻译：通过混合含有聚二有机硅氧烷的链烯基，巯基官能聚有机硅氧烷或巯基有机化合物的巯基官能交联剂，光敏剂，粘度稳定剂和任选的增强剂，可得到通过UV辐射固化少于1秒的组合物。这些组合物可以包装在一个容器中，并且可以用作光纤的主要涂层。

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