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1. 发明授权

US3531456A 5-arylazo-pyrimidine monoazo dyestuffs 失效
标题翻译： 5-ARYLAZO-PYRIMIDINE MONOAZO DYESTUFFS
公开(公告)号：US3531456A
公开(公告)日：1970-09-29
申请号：US3531456D
申请日：1967-11-08
申请人： GEIGY AG J R
发明人： ACKERMANN HANS , BOSSARD WERNER , VOLTZ JACQUES , WEGMULLER HANS
IPC分类号： C07D239/48 , C07D239/50 , C09B29/00 , C09B31/14 , C09B43/20 , D06P1/02
CPC分类号： C07D239/48 , C07D239/50 , C09B29/3669 , C09B31/14 , C09B43/202 , Y10S8/921 , Y10S8/922 , Y10S534/01
摘要： 1,188,610. Mono- and dis-azo dyestuffs. J. R. GEIGY A.G. 26 April, 1968 [28 April, 1967], No. 19864/68. Addition to 1,109,628. Heading C4P. The invention comprises dyestuffs containing no ionic groups forming salts in water and having the general formula wherein A is a carbocyclic or heterocyclic aromatic radical which may contain an arylazo group, one of X 1 , X 1 and X 3 is -O-, -S- or -NH- and each other X is -NH-, at least one of R 1 , R 2 and R 3 is a radical -alk -O-Z wherein alk is an optionally substituted alkylene radical and Z is H, an acyl radical or an optionally substituted hydrocarbon radical and the other R's each represent an optionally substituted alkyl, cycloalkyl, or aralkyl group or a phenyl radical bound by -O- or -S- to the pyrimidine nucleus. Preferably A is a phenyl radical having a nitro group in the o- and/or pposition to the azo link which may be further substituted or a benzthiazolyl-(2)- radical optionally substituted by chlorine, bromine, nitro, cyano, thiocyano, alkyl, alkoxy or alkylsulphonyl. Other values of A specified include naphthalene, pyrazole, thiazole, oxadiazole, thiodiazole, triazole, pyridine, benzothiazole, indazole or quinoline. They are prepared by diazotization and coupling or by acylation of the corresponding compound where at least one R 1 , R 2 and R 3 is -alk-OH. Coupling may take place in presence of methanol, D.M.F., ethylene glycol monoethylether or cetyl or oleyl polyglycol ethers. The dyestuffs give yellow, orange, red and brown shades on hydrophobic organic textile fibres e.g. polyesters, cellulose 2¢ and triacetates.

2. 发明授权

US3527748A 5-arylazo-pyrimidine dyestuffs 失效
标题翻译： 5-ARYLAZO-PYRIMIDINE DYESTUFFS
公开(公告)号：US3527748A
公开(公告)日：1970-09-08
申请号：US3527748D
申请日：1967-11-08
申请人： GEIGY AG J R
发明人： ACKERMANN HANS , BOSSARD WERNER , VOLTZ JACQUES , WEGMULLER HANS
IPC分类号： C07D239/50 , C09B29/00 , C09B29/52 , C09B31/14 , C09B29/36 , D06P1/02
CPC分类号： C07D239/50 , C09B29/00 , C09B29/3669 , C09B31/14 , Y10S8/921 , Y10S8/922

3. 发明授权

US3531458A 5-arylazo-pyrimidine monoazo dyestuffs 失效
公开(公告)号：US3531458A
公开(公告)日：1970-09-29
申请号：US3531458D
申请日：1967-11-08
申请人： GEIGY AG J R
发明人： ACKERMANN HANS , BOSSARD WERNER , VOLTZ JACQUES , WEGMULLER HANS
IPC分类号： C07D239/48 , C09B43/20 , D06P1/02
CPC分类号： C07D239/48 , C09B43/202 , Y10S8/921 , Y10S8/922 , Y10S534/01

4. 发明授权

US3531457A 5-arylazo-pyrimidine monoazo dyestuffs 失效
公开(公告)号：US3531457A
公开(公告)日：1970-09-29
申请号：US3531457D
申请日：1967-11-08
申请人： GEIGY AG J R
发明人： ACKERMANN HANS , BOSSARD WERNER , VOLTZ JACQUES , WEGMULLER HANS
IPC分类号： C07D239/48 , C07D239/50 , C09B29/00 , C09B31/14 , C09B43/20 , D06P1/02
CPC分类号： C07D239/48 , C07D239/50 , C09B29/3669 , C09B31/14 , C09B43/202 , Y10S8/921 , Y10S8/922 , Y10S534/01
摘要： 1,188,610. Mono- and dis-azo dyestuffs. J. R. GEIGY A.G. 26 April, 1968 [28 April, 1967], No. 19864/68. Addition to 1,109,628. Heading C4P. The invention comprises dyestuffs containing no ionic groups forming salts in water and having the general formula wherein A is a carbocyclic or heterocyclic aromatic radical which may contain an arylazo group, one of X 1 , X 1 and X 3 is -O-, -S- or -NH- and each other X is -NH-, at least one of R 1 , R 2 and R 3 is a radical -alk -O-Z wherein alk is an optionally substituted alkylene radical and Z is H, an acyl radical or an optionally substituted hydrocarbon radical and the other R's each represent an optionally substituted alkyl, cycloalkyl, or aralkyl group or a phenyl radical bound by -O- or -S- to the pyrimidine nucleus. Preferably A is a phenyl radical having a nitro group in the o- and/or pposition to the azo link which may be further substituted or a benzthiazolyl-(2)- radical optionally substituted by chlorine, bromine, nitro, cyano, thiocyano, alkyl, alkoxy or alkylsulphonyl. Other values of A specified include naphthalene, pyrazole, thiazole, oxadiazole, thiodiazole, triazole, pyridine, benzothiazole, indazole or quinoline. They are prepared by diazotization and coupling or by acylation of the corresponding compound where at least one R 1 , R 2 and R 3 is -alk-OH. Coupling may take place in presence of methanol, D.M.F., ethylene glycol monoethylether or cetyl or oleyl polyglycol ethers. The dyestuffs give yellow, orange, red and brown shades on hydrophobic organic textile fibres e.g. polyesters, cellulose 2¢ and triacetates.

5. 发明授权

US3496214A Condensation products of cyanoacetyl urea and amine complexes 失效
标题翻译：氰尿酸尿素和胺类复合物的冷凝产物
公开(公告)号：US3496214A
公开(公告)日：1970-02-17
申请号：US3496214D
申请日：1966-04-04
申请人： GEIGY AG J R
发明人： MEINDL HUBERT , ACKERMANN HANS , KAENEL FRED VON
IPC分类号： C07C275/50 , C07D239/54 , C07D239/557 , C07C127/12 , C07C97/02 , C07C121/08
CPC分类号： C07D239/557 , C07C275/50

6. 发明授权

US3627749A Mono-and disazo dyestuffs containing triazinylureylene groups 失效
标题翻译：含有三亚乙烯基组合的单和二氧化二氮
公开(公告)号：US3627749A
公开(公告)日：1971-12-14
申请号：US3627749D
申请日：1968-11-08
申请人： GEIGY AG J R
发明人： ACKERMANN HANS , SEILER HERBERT , MEINDL HUBERT
IPC分类号： C09B62/04 , H01R13/523 , H01R13/703 , C09B62/06 , C09B62/08
CPC分类号： C09B62/04 , Y10S8/917 , Y10S8/918
摘要： Reactive dyestuffs of the formula

R is a member selected from the group consisting of H and lower alkyl; D is an azo dyestuff chromophoric radical Hal is F, C1, or Br; N IS ONE OF THE INTEGERS 1 OR 2; AND X is a monovalent electron-donnor substituent, selected from the group of lower alkoxy, phenoxy, halogen-substituted phenoxy, lower alkyl-substituted phenoxy, lower alkoxy-substituted phenoxy, lower alkylthio, phenylthio, halogen-substituted phenylthio, lower alkyl-substituted phenylthio, lower alkoxysubstituted phenylthio, lower alkylamino, di(lower)alkylamino, phenylamino, N-lower alkyl-N-phenylamino, N-lower alkyl-Nhalogen-phenylamino, N-lower alkyl-N-lower alkylphenylamino, Nlower alkyl-N-lower alkoxyphenylamino, piperidino or morpholino, halogen being chloro or bromo. These dyes are suitable for the dyeing of natural and synthetic polyamide fibers as well as for textile fibers containing hydroxyl groups, particularly for natural or regenerated cellulose fibers. The obtained dyeings and prints are distinguished by excellent wet fastness properties and good fastness to light.

7. 发明授权

US3598801A Water-soluble azo-pyrimidine dyestuffs 失效
标题翻译：水溶性AZO-PYRIMIDINE DYESTUFFS
公开(公告)号：US3598801A
公开(公告)日：1971-08-10
申请号：US3598801D
申请日：1968-01-08
申请人： GEIGY AG J R
发明人： BEFFA FABIO , LIENHARD PAUL , SEILER HERBERT , ACKERMANN HANS , WEGMULLER HANS E
IPC分类号： C09B33/12 , C09B35/02 , C09B35/03 , C09B62/006 , C09B29/36 , C09B62/24 , D06P1/06
CPC分类号： C09B62/006 , C09B33/12 , C09B35/02 , C09B35/03 , C09B62/0067
摘要： WATER-SOLUBLE AZO-PYRIMIDINE DYESTUFFS OBTAINED BY COUPLING DIAZO OR TETRAZO COMPOUNDS DERIVED FROM AROMATIC MONOAMINES OR DIAMINES IN AN EQUIVALENT RATIO OF ABOUT 1:1 WITH AN OPTIONALLY SUBSTITUTED 2.4.6-TRIAMINOPYRIMIDINE COMPOUND WHICH CAN BE COUPLED IN THE 5-POSITION, OR IN AN EQUIVALENT RATIO OF 1:2 WITH IDENTICAL OR DIFFERENT 2,4,6-TRIAMINO-PYRIMIDINE COMPOUNDS OF THIS TYPE, OR WITH ONE EQUIVALENT OF SUCH A TRIAMINO-PYRIMIDINE COMPOUND AND ONE EQUIVALENT OF ANOTHER COUPLING COMPONENT AND, IN THE CASE OF COUPLING COMPONENTS CONTAINING DIAZOTIZABLE AMINO BROUPS, THE DISAZO DYESTUFFS RESULTING FROM COUPLING SUCH DIAZOTIZED AMINOAZO-PYRIMIDINE DYESTUFFS WITH ANOTHER COUPLING COMPONENT, OR DYESTUFFS OBTAINED BY COUPLING TWO EQUIVALENTS OF THE AFORESAID DIAZOTIZED MONOAMINES WITH A COUPLING COMPONENT COMPRISING TWO PYRIMIDYL NUCLEI LINKED TOGETHER VIA A HYDRAZINO BRIDGE OR VIA CERTAIN ORGANIC BRIDGE MEMBERS, THE COMPONENTS BEING SO CHOSEN THAT THE FINAL DYESTUFF CONTAINS AT LEAST ONE SALT-FORMING, WATER SOLUBILIZING GROUP WHICH DIS SOCIATES ACID IN WATER AND AT LEAST THREE RINGS PER MOLECULE, WHICH ARE NOT FUSED WITH ONE ANOTHER, AND OF WHICH PREFERABLY AT LEAST TWO ARE CARBOCYCLIC OR HETEROCYCLIC AND OF AROMATIC CHARACTER AND THE THIRD CAN BE AROMATIC, OR A PARTLY UNSATURATED OR A SATURATED ALICYCLIC RING. SAID DYE STUFFS PRODUCE POLYAMIDE DYEINGS HAVING GOOD FASTNESS TO LIGHT AND ABRASION AND EXCELLLENT WET-FASTNESS PROPERTIES AND WHEN THEY CONTAIN FIBER-REACTIVE SUBSTITUENTS, THE AZOPYRIMIDINE DYESTUFFS CAN ALSO BE USED FOR THE DYEING OF CELLULOSE FIBERS ON WHICH THEY AFFORD DYEINGS HAVING GOOD WET-FASTNESS PROPERTIES, ESPECIALLY FASTNESS TO WASHING.

8. 发明授权

US3565881A Fiber-reactive,heavy metal-containing formazane dyestuffs 失效
标题翻译：纤维反应性，重金属含金属试剂
公开(公告)号：US3565881A
公开(公告)日：1971-02-23
申请号：US3565881D
申请日：1969-01-28
申请人： GEIGY AG J R
发明人： DUSSY PAUL , MEINDL HUBERT , ACKERMANN HANS
IPC分类号： C09B62/006 , C09B62/24 , C09B45/00 , C09B45/48
CPC分类号： C09B62/0068 , C09B62/242
摘要： FIBER-REACTIVE, HEAVY METAL-CONTAINING FORMAZANES DYES WHICH ARE CHARACTERIZED BY BEING SUBSTITUTED AT THE CARBON ATOM IN MESO-POSITION IN THE FORMAZINE BRIDGE BY THE RADICAL OF A MONOAZO DYESTUFF ARE PROVIDED; THESE NEW DYES WHEN FREE FROM ACID DISSOCIATING, SALT-FORMING WATER-SOLUBILIZING GROUPS AND METALLIZED WITH A HEAVY METAL ARE USEFUL FOR DYEING LACQUERS, VARNISHES, SPINNING MASSES OF ACETYL CELLULOSE AND SYNTHETIC POLYAMIDES; THE NEW DYES WHICH CONTAIN WATER-SOLUBILIZING GROUPS AND ARE METALLIZED WITH A HEAVY METAL ATOM ARE USEFUL IN THE DYEING AND PRINTING OF LEATHER, PAPER AND NATURAL AND SYNTHETIC POLYPEPTIDE FIBER MATERIALS INCLUDING WOOL, SILK, NYLON AND POLYURETHANE FIBERS; DYES OF THE ABOVE-MENTIONED LATTER SUBCLASS WHICH BEAR ONE OR TWO FIBER-REACTIVE GROUPINGS ARE EXPECIALLY USEFUL IN DYEING CELLULOSIC FIBERS. IN THOSE COMPOUNDS IN WHICH THIS FIBER REACTIVE SUBSTITUENT IS A PYRIMIDYL RADICAL CONTAINING AT LEAST ONE FLUORINE ATOM, THESE DYES ARE FURTHER DISTINGUISHED BY THEIR HIGH REACTIVITY; THE DYEINGS OR PRINTINGS OBTAINED THEREWITH ARE VERY STABLE VIS-A-VIS ACID OR ALKALINE HYDROLYSIS AND EXHIBIT VERY GOOD FASTNESS TO LIGHT, MILLING AND WET TREATMENTS.

9. 发明授权

US3433781A 2,4-dihalogeno-pyrimidine-5-carbamyl-substituted reactive dyes 失效
标题翻译： 2,4-二羟基 - 吡咯烷-5-羧酸取代的反应性染料
公开(公告)号：US3433781A
公开(公告)日：1969-03-18
申请号：US3433781D
申请日：1964-02-26
申请人： GEIGY AG J R
发明人： ACKERMANN HANS , FREI HERMANN , MEINDL HUBERT
IPC分类号： C09B62/20 , C09B62/26 , C09B62/22 , C09B62/24
CPC分类号： C09B62/20

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