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1. 发明授权

US06770187B1 Method for electrochemically producing an alkali metal from an aqueous solution 失效
标题翻译：从水溶液中电化学制造碱金属的方法
公开(公告)号：US06770187B1
公开(公告)日：2004-08-03
申请号：US10069369
申请日：2002-02-25
申请人： Hermann Pütter , Günther Huber , Kerstin Schierle-Arndt , Dieter Schläfer , Josef Guth
发明人： Hermann Pütter , Günther Huber , Kerstin Schierle-Arndt , Dieter Schläfer , Josef Guth
IPC分类号： C25C102
CPC分类号： C25C1/02
摘要： The invention relates to an electrolysis cell comprising an anode compartment which comprises an aqueous solution of at least one alkali metal salt, a cathode compartment and a solid electrolyte which separates the anode compartment and the cathode compartment from one another, wherein that part of the surface of the solid electrolyte which is in contact with the anode compartment and/or that part of the surface of the solid electrolyte which is in contact with the cathode compartment has/have at least one further ion-conducting layer.
摘要翻译：本发明涉及一种电解槽，其包括阳极室，该室包含至少一种碱金属盐的水溶液，阴极室和将阳极室和阴极隔室相互分离的固体电解质，其中该部分表面与阳极室接触的固体电解质和/或与阴极室接触的固体电解质的表面部分具有至少一个另外的离子传导层。

2. 发明授权

US06409908B1 Electrochemical production of alkali metal from an alkali metal amalgam 有权
标题翻译：从碱金属汞合金电化学生产碱金属
公开(公告)号：US06409908B1
公开(公告)日：2002-06-25
申请号：US09459726
申请日：1999-12-13
申请人： Günther Huber , Hermann Pütter , Kerstin Schierle-Arndt , Dieter Schläfer , Josef Guth , Bernd Schube , Diethard Lenz
发明人： Günther Huber , Hermann Pütter , Kerstin Schierle-Arndt , Dieter Schläfer , Josef Guth , Bernd Schube , Diethard Lenz
IPC分类号： C25B100
CPC分类号： C25C3/02
摘要： In a process for producing an alkali metal from alkali metal amalgam by electrolysis using an alkali metal amalgam as anode, a solid electrolyte which conducts alkali metal ions and a liquid alkali metal as cathode, the alkali metal amalgam as anode is kept in motion.
摘要翻译：在碱金属汞齐作为阳极通过电解制造碱金属的方法中，将碱金属离子和液态碱金属作为阴极进行电解的固体电解质，作为阳极的碱金属汞齐保持运动。

3. 发明授权

US06287448B1 Electrochemical production of lithium using a lithium amalgam anode 失效
标题翻译：使用锂二极体阳极电化学生产锂
公开(公告)号：US06287448B1
公开(公告)日：2001-09-11
申请号：US09531471
申请日：2000-03-20
申请人： Kerstin Schierle-Arndt , Hermann Pütter , Günther Huber , Dieter Schläfer , Josef Guth
发明人： Kerstin Schierle-Arndt , Hermann Pütter , Günther Huber , Dieter Schläfer , Josef Guth
IPC分类号： C25C100
CPC分类号： C25C1/02 , C25C3/02
摘要： A process for producing metallic lithium starting from an aqueous solution of at least one lithium salt comprises the following steps: (I) Production of a lithium amalgam from an aqueous solution of at least one lithium salt; and (II) Electrolysis using an anode comprising the lithium amalgam, a solid electrolyte which conducts lithium ions, and liquid lithium as cathode, wherein the lithium amalgam as anode is kept in motion.
摘要翻译：从至少一种锂盐的水溶液开始制造金属锂的方法包括以下步骤：（I）从至少一种锂盐的水溶液制备锂汞齐; 和（II）使用包含锂汞齐的阳极，导电锂离子的固体电解质和液体锂作为阴极的电解，其中作为阳极的锂汞齐保持运动。

4. 发明授权

US06368487B1 Electrolytic cell for producing an alkali metal 有权
标题翻译：用于生产碱金属的电解槽
公开(公告)号：US06368487B1
公开(公告)日：2002-04-09
申请号：US09589163
申请日：2000-06-08
申请人： Günther Huber , Hermann Pütter , Kerstin Schierle-Arndt , Dieter Schläfer , Josef Guth
发明人： Günther Huber , Hermann Pütter , Kerstin Schierle-Arndt , Dieter Schläfer , Josef Guth
IPC分类号： C25C302
CPC分类号： C25C3/02
摘要： An electrolytic cell comprises an agitated, alkali metal amalgam-containing anode, an alkali metal ion-conducting solid electrolyte and a cathode, wherein the solid electrolyte and the cathode are separated from one another by a liquid electrolyte.
摘要翻译：电解槽包括搅拌的碱金属汞齐阳极，碱金属离子导电固体电解质和阴极，其中固体电解质和阴极通过液体电解质彼此分离。

5. 发明授权

US06402910B1 Electrolytic cell 失效
标题翻译：电解池
公开(公告)号：US06402910B1
公开(公告)日：2002-06-11
申请号：US09567210
申请日：2000-05-09
申请人： Hermann Pütter , Günther Huber , Luise Spiske , Hans Stark , Dieter Schläfer , Gerhard Pforr
发明人： Hermann Pütter , Günther Huber , Luise Spiske , Hans Stark , Dieter Schläfer , Gerhard Pforr
IPC分类号： C25C300
CPC分类号： C25C3/02
摘要： A process for preparing sodium and aluminum chloride electrochemically is described in which, in an electrolytic cell containing aluminum as an anode and sodium as a cathode which are separated from one another by a sodium ion-conducting solid electrolyte, a fused electrolyte essentially containing sodium tetrachloroaluminate is electrolyzed in the anode compartment, aluminum chloride formed in this process is evaporated from the electrolytic cell and sodium is removed from the cathode compartment.
摘要翻译：描述了一种电化学制备钠和氯化铝的方法，其中在含有作为阳极的铝和作为阴极的钠通过钠离子导电固体电解质彼此分离的电解池中，基本上含有四氯铝酸钠的熔融电解质在阳极室中进行电解，在该方法中形成的氯化铝从电解槽中蒸发，从阴极室除去钠。

6. 发明授权

US06235183B1 Electrolytic method for the production of sodium and aluminum chloride 失效
标题翻译：用于生产氯化钠和氯化铝的电解方法
公开(公告)号：US06235183B1
公开(公告)日：2001-05-22
申请号：US09000276
申请日：1998-01-27
申请人： Hermann Pütter , Günther Huber , Luise Spiske , Hans Stark , Dieter Schläfer , Gerhard Pforr
发明人： Hermann Pütter , Günther Huber , Luise Spiske , Hans Stark , Dieter Schläfer , Gerhard Pforr
IPC分类号： C25B124
CPC分类号： C25C3/02
摘要： A process for preparing sodium and aluminum chloride electrochemically is described in which, in an electrolytic cell containing aluminum as an anode and sodium as a cathode which are separated from one another by a sodium ion-conducting solid electrolyte, a fused electrolyte essentially containing sodium tetrachloroaluminate is electrolyzed in the anode compartment, aluminum chloride formed in this process is evaporated from the electrolytic cell and sodium is removed from the cathode compartment.
摘要翻译：描述了电化学制备钠和氯化铝的方法，其中在以铝为阳极的电解池和通过钠离子导电固体电解质彼此分离的钠作为阴极的电解槽中，基本上含有四氯铝酸钠的熔融电解质在阳极室中进行电解，在该方法中形成的氯化铝从电解槽中蒸发，从阴极室除去钠。

7. 发明授权

US06776894B1 Method for producing carbonyl compounds which are oxidized in position alpha 失效
标题翻译：在α位置氧化的羰基化合物的制备方法
公开(公告)号：US06776894B1
公开(公告)日：2004-08-17
申请号：US10030173
申请日：2002-01-31
申请人： Hermann Pütter , Kerstin Schierle-Arndt , Jörg Botzem
发明人： Hermann Pütter , Kerstin Schierle-Arndt , Jörg Botzem
IPC分类号： C25B300
CPC分类号： C25B3/00
摘要： A method for producing compounds which are oxidized in an alpha position by electrochemical reaction with alcohol in the presence of an auxiliary electrolyte and catalytic amounts of a metal salt.
摘要翻译：一种在辅助电解质和催化量的金属盐存在下通过与醇的电化学反应在α位置氧化的化合物的方法。

8. 发明授权

US06822124B2 Method for producing alcoxylated carbonyl compounds by an anodic oxidation method using a cathodic coupled reaction for organic synthesis 失效
公开(公告)号：US06822124B2
公开(公告)日：2004-11-23
申请号：US10432249
申请日：2003-05-22
申请人： Hermann Pütter , Andreas Fischer
发明人： Hermann Pütter , Andreas Fischer
IPC分类号： C07C4702
CPC分类号： C25B3/00
摘要： A method for producing alcoxylated carbonyl compounds of general formula (I) (compounds I): R1aR2C(OR3)b wherein R1, R2 represent hydrogen or C1-C6-alkyl, R3 independently means C1-C6-alkyl, a is 0 or 1, b 2 or 3 with the proviso that the sum of a and b is 3, by means of anodic oxidation of germinal dialcoxy compounds of general formula (II) (compounds II) wherein R4, R5, R6, R7 represent hydrogen or C1-C6-alkyl, R5, R6 represent C1-C6-alkyl or C1-C6-alcoxy, in the presence of a C1-C6-alkyl alcohol (compounds III). A usual compound (compound IV) is used as a cathodic depolarizer suitable for electrochemical oxidation. The anodic oxidation and cathodic reduction is carried out in an undivided electrolyte cell in the presence of C1-C6-alkyl alcohols.

9. 发明授权

US06713656B2 Preparation of diacetals of glyoxal 失效
标题翻译：乙二醛二缩醛的制备
公开(公告)号：US06713656B2
公开(公告)日：2004-03-30
申请号：US10262980
申请日：2002-10-03
申请人： Gunnar Heydrich , Nicola Christiane Aust , Hermann Pütter , Andreas Fischer , Jörg Botzem
发明人： Gunnar Heydrich , Nicola Christiane Aust , Hermann Pütter , Andreas Fischer , Jörg Botzem
IPC分类号： C07C4330
CPC分类号： C07C41/56 , C07C43/303 , C07C47/198
摘要： A process is described for preparing diacetals of glyoxal by reacting from 40 to 75% by weight aqueous glyoxal with monohydric alcohols in the presence of an acid catalyst, which comprises leaving a liquid mixture which, at the beginning of the reaction, comprises alcohol and glyoxal in a molar ratio of at least 15:1 and also water in a concentration of not more than 8% by weight in contact with the acid catalyst until concentration in the reaction mixture of the diacetal formed reaches at least 70% of the equilibrium concentration without more than 5% by weight of the alcohol used having already been distilled off.
摘要翻译：描述了一种通过在酸催化剂的存在下使40至75重量％的乙二醛与一元醇反应来制备乙二醛的二缩醛的方法，其包括在反应开始时包含醇和乙二醛的液体混合物至少15:1的摩尔比和与酸催化剂接触的浓度不超过8重量％的水，直到形成的二缩醛的反应混合物中的浓度达到平衡浓度的至少70％而没有超过5％（重量）所用的醇已被蒸馏掉。

10. 发明授权

US06245945B1 Selective hydrolysis of acetals or ketals in the presence of phthalides 失效
标题翻译：在苯酞中存在下缩醛或缩酮的选择性水解
公开(公告)号：US06245945B1
公开(公告)日：2001-06-12
申请号：US09623059
申请日：2000-08-25
申请人： Andreas Weiper-Idelmann , Heinz Hannebaum , Hermann Pütter
发明人： Andreas Weiper-Idelmann , Heinz Hannebaum , Hermann Pütter
IPC分类号： C07C4542
CPC分类号： C07C45/515 , C07C45/59 , C07D307/88
摘要： A process for the selective hydrolysis of acetals in the presence of phthalides comprises reacting a mixture (M) comprising a) a phthalide of the formula (I) where: R1,R2,R3 and R4: are independently hydrogen, C1-C4-alkyl or halogen, and b) an acetal or ketal of the formula (II) where: R5 and R6: are independently C1-C6-alkyl, C6-C10-aryl or together ethylene, and R7 and R8: are independently C1-C6-alkyl, or one radical is a hydrogen and the other is a phenyl radical where from 1 to 3 hydrogen atoms of the phenyl radical may be replaced by C1-C6-alkyl radicals or C1-C4-alkoxy radicals, or R7 and R8 are together C3-C6-alkanediyl, and a hydrogen atom may be replaced by a hydroxyl group, at from 10 to 200° C. in the presence of from 1 to 10 mol of water, based on the amount of acetal or ketal of the formula (II), to hydrolyze the acetal or ketal of the formula (II) to the corresponding aldehyde or ketone.
摘要翻译：在含有苯并呋喃存在下选择性水解缩醛的方法包括使包含a）式（I）的苯酞的混合物（M）反应，其中：R1，R2，R3和R4独立地是氢，C1-C4-烷基或卤素和b）式（II）的缩醛或缩酮，其中：R 5和R 6独立地为C 1 -C 6烷基，C 6 -C 10 - 芳基或一起为乙烯，R 7和R 8独立地为C 1 -C 6烷基，或一个基团是氢，另一个是苯基，其中苯基的1至3个氢原子可以被C 1 -C 6 - 烷基或C 1 -C 4 - 烷氧基取代，或者R 7和R 8一起是C 3 -C 6 （II）的缩醛或缩酮的量，可以在10〜200℃的存在下，在1〜10摩尔的水的存在下，用羟基代替氢原子，以将式（II）的缩醛或缩酮水解成相应的醛或酮。

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