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1. 发明授权

US06414214B1 Mechanically stable hydrogel-forming polymers 有权
标题翻译：机械稳定的水凝胶形成聚合物
公开(公告)号：US06414214B1
公开(公告)日：2002-07-02
申请号：US09411644
申请日：1999-10-04
申请人： Friedrich Engelhardt , Volker Frenz , Norbert Herfert , Ulrich Riegel , Matthias Weismantel , Wilfried Heide
发明人： Friedrich Engelhardt , Volker Frenz , Norbert Herfert , Ulrich Riegel , Matthias Weismantel , Wilfried Heide
IPC分类号： A61F1315
CPC分类号： C08F8/00 , C08J3/126 , C08J3/245 , C08F20/10
摘要： Hydrogel-forming polymers which have: (i) a Saline Flow Conductivity of at least 40×10−7 cm3s/g; (ii) an AUL 0.7 psi (4826.5 Pa) of at least 20 g/g; and (iii) a Frangibility Index of at least 60%, are useful in hygienic articles such as incontinence briefs for adults and diapers for infants.
摘要翻译：具有以下特征的水凝胶形成聚合物：（i）至少40×10 -7 cm 3 / g的盐水流动电导率;（ii）至少20g / g的AUL 0.7psi（4826.5Pa）; 和（iii）至少60％的易碎指数，可用于卫生用品，如成人尿失禁者和婴儿尿布。

2. 发明授权

US06849665B2 Absorbent compositions 有权
标题翻译：吸收剂组合物
公开(公告)号：US06849665B2
公开(公告)日：2005-02-01
申请号：US10028908
申请日：2001-12-28
申请人： Volker Frenz , Norbert Herfert , Ulrich Riegel , William E. Volz , Thomas H. Majette , James Hill
发明人： Volker Frenz , Norbert Herfert , Ulrich Riegel , William E. Volz , Thomas H. Majette , James Hill
IPC分类号： A61F13/53 , A61F13/00 , A61F13/15 , A61F13/49 , A61L15/60 , B01J20/26 , C08L101/14 , C08J9/28
CPC分类号： A61L15/60 , B01J20/26 , Y10T428/249953 , Y10T428/2991 , Y10T428/2998 , Y10T428/31971 , Y10T428/31975 , Y10T428/31978
摘要： Described is a water-absorbent composition containing from 30 to 100% by weight, based on the water-absorbent composition, of water-insoluble water-swellable hydrogels characterized by the following features: Centrifuge Retention Capacity (CRC) of at least 24 g/g, Saline Flow Conductivity (SFC) of at least 80×10−7 cm3 s/g and Free Swell Rate (FSR) of at least 0.15 g/g s and/or Vortex Time of not more than 160 s.
摘要翻译：描述了基于吸水性组合物含有30-100重量％的水不溶性水溶胀性水凝胶的吸水性组合物，其特征在于以下特征：离心保留容量（CRC）为至少24g / g，至少80×10 -7 cm 3 / s的盐水流动电导率（SFC）和至少0.15g / gs和/或不超过160s的涡旋时间的无膨胀速率（FSR）。

3. 发明授权

US07727586B2 Production of water-absorbing polymeric particles by dropletization polymerization in the gas phase 有权
标题翻译：在气相中通过液滴聚合制备吸水聚合物颗粒
公开(公告)号：US07727586B2
公开(公告)日：2010-06-01
申请号：US11814021
申请日：2006-01-24
申请人： Stefan Bruhns , Volker Frenz , Dennis Lösch , Volker Seidl , Uwe Stueven , Carolin Nadine Dücker , Matthias Weismantel , Wilfried Heide , Stefan Blei
发明人： Stefan Bruhns , Volker Frenz , Dennis Lösch , Volker Seidl , Uwe Stueven , Carolin Nadine Dücker , Matthias Weismantel , Wilfried Heide , Stefan Blei
IPC分类号： C08F2/10 , C08F2/00 , C08F2/01 , C08F2/04
CPC分类号： B01J8/388 , A61L15/60 , B01J8/0055 , B01J8/36 , B01J2208/00433 , B01J2208/0046 , B01J2208/00681 , C08F2/01 , C08F2/34 , C08F6/008 , F26B3/08 , Y10T428/2982
摘要： A process for producing water-absorbing polymeric particles by dropletization polymerization in the gas phase, which comprises drying the polymeric particles after the polymerization in a fluidized bed, the water-absorbing polymeric particles themselves, hygiene articles comprising these water-absorbing polymeric particles and also apparatus for implementing the process.
摘要翻译：在气相中通过液滴聚合制备吸水性聚合物颗粒的方法，其包括在流化床中聚合后干燥聚合物颗粒，吸水聚合物颗粒本身，包含这些吸水性聚合物颗粒的卫生制品，以及用于实施该过程的装置。

4. 发明申请

US20080188586A1 Production of Water-Absorbing Polymeric Particles by Dropletization Polymerization in the Gas Phase 有权
标题翻译：通过在气相中的液滴聚合制备吸水聚合物颗粒
公开(公告)号：US20080188586A1
公开(公告)日：2008-08-07
申请号：US11814021
申请日：2006-01-24
申请人： Stefan Bruhns , Volker Frenz , Dennis Losch , Volker Seidl , Uwe Stueven , Carolin Nadine Ducker , Matthias Weismantel , Wilfried Heide , Stefan Blei
发明人： Stefan Bruhns , Volker Frenz , Dennis Losch , Volker Seidl , Uwe Stueven , Carolin Nadine Ducker , Matthias Weismantel , Wilfried Heide , Stefan Blei
IPC分类号： C08F2/48 , C08F6/00
CPC分类号： B01J8/388 , A61L15/60 , B01J8/0055 , B01J8/36 , B01J2208/00433 , B01J2208/0046 , B01J2208/00681 , C08F2/01 , C08F2/34 , C08F6/008 , F26B3/08 , Y10T428/2982
摘要： A process for producing water-absorbing polymeric particles by dropletization polymerization in the gas phase, which comprises drying the polymeric particles after the polymerization in a fluidized bed, the water-absorbing polymeric particles themselves, hygiene articles comprising these water-absorbing polymeric particles and also apparatus for implementing the process.
摘要翻译：在气相中通过液滴聚合制备吸水性聚合物颗粒的方法，其包括在流化床中聚合后干燥聚合物颗粒，吸水聚合物颗粒本身，包含这些吸水性聚合物颗粒的卫生制品，以及用于实施该过程的装置。

5. 发明授权

US06472478B1 Process for crosslinking hydrogels with bis- and poly-2- oxazolidinones 有权
标题翻译：用双 - 和多 - 2-恶唑烷酮交联水凝胶的方法
公开(公告)号：US06472478B1
公开(公告)日：2002-10-29
申请号：US09601349
申请日：2000-08-18
申请人： Rüdiger Funk , Volker Frenz , Ulrich Riegel , Matthias Weismantel , Fritz Engelhardt , Thomas Daniel
发明人： Rüdiger Funk , Volker Frenz , Ulrich Riegel , Matthias Weismantel , Fritz Engelhardt , Thomas Daniel
IPC分类号： C08F830
CPC分类号： A61L15/60 , C08F8/30 , Y10S524/916 , Y10T442/699
摘要： The invention relates to a process for the gel or surface postcrosslinking of water-absorbing polymers in which the polymers are treated with a surface postcrosslinking solution and during or after the treatment are postcrosslinked and dried by means of an increase in temperature, the crosslinker being a compound of the formula in which R1 and R2 independently of one another are H, hydroxyl, phenyl or C1-C6-alkyl, R3 is hydrogen, C1-C12-alkyl, C1-C12-alkenyl or C6-C12-aryl and R4 and R5 independently of one another are C1-C12-alkyl, C1-C12-alkenyl, C6-C12-aryl, hydroxyl, C1-C12-alkoxy or hydrogen, dissolved in an inert solvent, to water-absorbing polymers which can be obtained by said process, and to their use in hygiene articles, packaging materials and nonwovens.
摘要翻译：本发明涉及一种吸水聚合物的凝胶或表面后交联方法，其中聚合物用表面后交联溶液处理，并且在处理之间或之后，通过温度升高进行后交联和干燥，交联剂为 R 1和R 2彼此独立地是H，羟基，苯基或C 1 -C 6烷基的化合物，R 3是氢，C 1 -C 12 - 烷基，C 1 -C 12 - 烯基或C 6 -C 12 - 芳基，R 4和R 5 彼此独立地是溶解在惰性溶剂中的C 1 -C 12烷基，C 1 -C 12 - 烯基，C 6 -C 12 - 芳基，羟基，C 1 -C 12 - 烷氧基或氢，可以通过所述过程，以及它们在卫生用品，包装材料和无纺布中的应用。

6. 发明授权

US06559239B1 Method for the secondary cross-linking of hydrogels with N-acyl-2-oxazolidinones 失效
标题翻译：水凝胶与N-酰基-2-恶唑烷酮二次交联的方法
公开(公告)号：US06559239B1
公开(公告)日：2003-05-06
申请号：US09831920
申请日：2001-05-29
申请人： Ulrich Riegel , Matthias Weismantel , Volker Frenz , Thomas Daniel , Fritz Engelhardt
发明人： Ulrich Riegel , Matthias Weismantel , Volker Frenz , Thomas Daniel , Fritz Engelhardt
IPC分类号： C08F830
CPC分类号： C08F8/30 , C08J3/245 , C08J2300/14 , C08J2333/02 , C08F220/06
摘要： Liquid-absorbent polymers are prepared by a process for the gel and/or surface postcrosslinking of water-absorbent polymers by the polymer being treated with a surface postcrosslinking solution and being postcrosslinked and dried during and after the treatment by raising the temperature, wherein the surface postcrosslinking solution comprises as crosslinker a compound of the formula I where R1, R2, R3 and R4 are independently hydrogen, C1-C12-alkyl, C1-C12-alkenyl, C6-C12-aryl or C1-C12-alkoxy, R5 is C1-C16-alkyl, C1-C4-hydroxyalkyl, C6-C12-aryl, C1-C16-alkenyl or a group of the formula —(CH2)n—COOH or —(CH2)n—SO3H in the form of the acid or a respective metal salt, ammonium salt or triethanolammonium salt thereof or —(CH2—CH2—O—)m—R6, R6 is hydrogen or C1-C16-alkyl, n is from 1 to 10, m is from 1 to 20 dissolved in an inert solvent, and are used in hygiene articles, packaging materials and nonwovens.
摘要翻译：通过用表面后交联溶液处理的聚合物进行凝胶和/或表面后吸附吸水性聚合物的方法制备液体吸收聚合物，并且在处理之间和之后通过升高温度进行后交联和干燥，其中表面后交联溶液包含作为交联剂的式I化合物，其中R 1，R 2，R 3和R 4独立地是氢，C 1 -C 12 - 烷基，C 1 -C 12 - 烯基，C 6 -C 12 - 芳基或C 1 -C 12 - 烷氧基，R 5是C 1 -C 16 - 烷基，C 1 -C 4 - 羟基烷基，C 6 -C 12 - 芳基，C 1 -C 16 - 烯基或式 - （CH 2）n -COOH或 - （CH 2）n -SO 3 H的基团，其形式为酸或相应的金属盐，铵盐或三乙醇铵盐或 - （CH 2 -CH 2 -O-）m -R 6，R 6是氢或C 1 -C 16 - 烷基，n为1至10，m为1至20，溶于惰性溶剂，用于卫生用品，包装材料和无纺布。

7. 发明授权

US06657015B1 Method for the secondary cross-linking of hydrogels with 2-oxotetrahydro-1,3-oxazines 有权
标题翻译：水凝胶与2-氧代四氢-1,3-恶嗪二次交联的方法
公开(公告)号：US06657015B1
公开(公告)日：2003-12-02
申请号：US09831382
申请日：2001-05-17
申请人： Ulrich Riegel , Matthias Weismantel , Volker Frenz , Thomas Daniel , Fritz Engelhardt
发明人： Ulrich Riegel , Matthias Weismantel , Volker Frenz , Thomas Daniel , Fritz Engelhardt
IPC分类号： C08F830
CPC分类号： C08F8/30 , C08J3/245 , C08J2300/14 , C08J2333/02 , C08F220/06
摘要： Liquid-absorbent polymers are prepared by a process for the gel and/or surface postcrosslinking of water-absorbent polymers by the polymer being treated with a surface postcrosslinking solution and being postcrosslinked and dried during and after the treatment by raising the temperature, wherein the crosslinker comprises a compound of the formula I where R1 is hydrogen, C1-C4-alkyl, C1-C4-hydroxyalkyl, trialkylsilyl or acetyl and R2, R2′, R3, R3′, R4, R4′ are each independently hydrogen, C1-C12-alkyl, C2-C12-alkenyl or C6-C12-aryl, dissolved in an inert solvent, and are used in hygiene articles, packaging materials and nonwovens.
摘要翻译：通过用表面后交联溶液处理的聚合物对吸水性聚合物进行凝胶和/或表面后交联的方法制备液体吸收性聚合物，并且在处理期间和之后通过升高温度进行后交联和干燥，其中交联剂包括其中R 1为氢，C 1 -C 4 - 烷基，C 1 -C 4 - 羟基烷基，三烷基甲硅烷基或乙酰基且R 2，R 2'，R 3，R 3'的式I化合物， >，R 4，R 4'各自独立地为氢，C 1 -C 12 - 烷基，C 2 -C 12 - 烯基或C 6 -C 12 - 芳基，溶于惰性溶剂中，并用于卫生用品，包装材料和无纺布。

8. 发明授权

US06503979B1 Method for cross-linking hydrogels with bis- and poly-2-oxazolidinones 失效
标题翻译：用双 - 和多 - 2-恶唑烷酮交联水凝胶的方法
公开(公告)号：US06503979B1
公开(公告)日：2003-01-07
申请号：US09622853
申请日：2000-08-28
申请人： Rüdiger Funk , Volker Frenz , Ulrich Riegel , Matthias Weismantel , Fritz Engelhardt , Thomas Daniel
发明人： Rüdiger Funk , Volker Frenz , Ulrich Riegel , Matthias Weismantel , Fritz Engelhardt , Thomas Daniel
IPC分类号： C08F830
CPC分类号： C08J3/245 , A61L15/60 , C08F8/30 , C08G73/06 , C08J2300/14 , Y10S524/916
摘要： The invention contains a process for the surface postcrosslinking of water-absorbing polymers in which the polymers are treated with a surface postcrosslinking solution and during or after the treatment are postcrosslinked by means of an increase in temperature and are dried, wherein the crossiinker comprises a bis-2-oxazolidinone or a poly-2-oxazolidinone comprising structural units of the formula in which R1 is branched or unbranched C1-C18-alkylene, branched or unbranched C2-C18-alkenylene, C5-C18-cycloalkylene, phenylene, naphthylene, anthracenylene, hydrocarbon-substituted phenylene, naphthylene or anthracenylene or another substituted or unsubstituted C6-C18-arylene radical, R2 is branched or unbranched C1-C18-alkylene and n is an integer from 1 to 50 or a mixture of bis-2-oxazolidinones and poly-2-oxazolidinones dissolved in an inert solvent.
摘要翻译：本发明包含用于表面后吸附聚合物的方法，其中聚合物用表面后交联溶液处理，并且在处理期间或之后通过温度升高进行后交联并干燥，其中交联剂包含双 -2-恶唑烷酮或包含结构单元的聚-2-恶唑烷酮，其中R1是支链或非支链C1-C18-亚烷基，支链或非支链C2-C18-亚烯基，C5-C18-亚环烷基，亚苯基，亚萘基，蒽亚基，烃取代的亚苯基，亚萘基或亚蒽基或其它取代或未取代的C 6 -C 18亚芳基，R 2是支链或非支链的C 1 -C 18 - 亚烷基，n是1至50的整数或双-2-恶唑烷酮和聚 -2-恶唑烷酮溶解在惰性溶剂中。

9. 发明申请

US20050085559A1 Process for the reduction of the residual monomer content of water-absorbent foam 失效
标题翻译：减少吸水泡沫的残留单体含量的方法
公开(公告)号：US20050085559A1
公开(公告)日：2005-04-21
申请号：US10502135
申请日：2003-01-30
申请人： Hans-Joachim Hahnle , Rudiger Funk , Wolfgang Heider , Gunnar Schornick , Volker Frenz
发明人： Hans-Joachim Hahnle , Rudiger Funk , Wolfgang Heider , Gunnar Schornick , Volker Frenz
IPC分类号： A61F13/53 , A61F13/00 , A61F13/49 , A61L15/16 , A61L15/60 , C08F6/00 , C08J9/00 , C08J9/36
CPC分类号： C08J9/36 , C08F6/006 , C08J2207/12 , C08J2300/14 , Y10T156/1011 , Y10T156/1084 , C08L33/02
摘要： A process for the reduction of the residual monomer content and enhancement of the wet strength of articles formed from water absorbent crosslinked polymer foams containing units derived from monoethylenically unsaturated acids, which comprises treating the formed articles with at least 0.5 % by weight of a polymer containing primary and/or secondary amino groups and having a molar mass of at least 300, the formed foam articles thus obtainable and use of the wet strength enhanced formed foam articles in hygiene articles.
摘要翻译：一种降低残留单体含量并提高由含有衍生自单烯属不饱和酸的单元的吸水性交联聚合物泡沫形成的制品的湿强度的方法，该方法包括用至少0.5重量％的含有初级和/或仲氨基并且摩尔质量至少为300，所形成的泡沫制品如此可获得，并且在卫生制品中使用湿强度增强的成形泡沫制品。

10. 发明授权

US06277900B1 Well cementing aids 有权
标题翻译：固井助剂
公开(公告)号：US06277900B1
公开(公告)日：2001-08-21
申请号：US09196668
申请日：1998-11-19
申请人： Reinhard Oswald , Volker Frenz , Juergen Tonhauser , Aranka Tardi , Pierre Maroy , Florence L'Alloret
发明人： Reinhard Oswald , Volker Frenz , Juergen Tonhauser , Aranka Tardi , Pierre Maroy , Florence L'Alloret
IPC分类号： C09K700
CPC分类号： C09K8/46 , C04B24/163 , C04B28/02 , C08F220/54 , C08F220/58 , C04B22/0026
摘要： The present invention relates to copolymers consisting of (a) 1-99% by weight of structural units of the formula (1) where R1 is hydrogen or methyl, R4 is C1-C22-alkylene, R5 is C1-C22-alkyl or hydrogen, and X is ammonium, lithium, sodium, potassium, an amine or a mixture of these substances, and (b) 99-1% by weight of structural units of the formula (2) where R1 is hydrogen or methyl, R2 and R3, independently of one another, are hydrogen, or C2-C22-alkyl, wherein component b) is not hydrolysed and the copolymers have been prepared by a solution precipitation polymerization in a nonaqueous solvent or a water-miscible, organic solvent having a low water content which is a precipitant for the copolymer. The invention furthermore relates to a process for cementing subterranean wells using a cement slurry comprising the following components: a) water of various salinity cement a novel copolymer in a concentration of 0.01-5% bwoc, preferably from 0.05 to 0.9% bwoc.
摘要翻译：本发明涉及由（a）1-99重量％的式（1）结构单元，其中R 1是氢或甲基，R 4是C 1 -C 22 - 亚烷基，R 5是C 1 -C 22 - 烷基或氢，和X是铵，锂，钠，钾，胺或这些物质的混合物，和（b）99-1重量％的式（2）的结构单元，其中R 1是氢或甲基，R 2和R 3 彼此独立地为氢或C 2 -C 22 - 烷基，其中组分b）未水解，并且该共聚物通过在非水溶剂或具有低水的水混溶性有机溶剂中的溶液沉淀聚合制备作为共聚物的沉淀剂的含量。本发明还涉及一种使用包含以下组分的水泥浆料固井地下井的方法：a）浓度为0.01-5％bwoc，优选0.05-0.9％bwoc的各种盐酸盐型新型共聚物的水。

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