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1. 发明授权

US5522972A Nickel hypophosphite manufacture 失效
标题翻译：次磷酸镍制造
公开(公告)号：US5522972A
公开(公告)日：1996-06-04
申请号：US277339
申请日：1994-07-19
申请人： Fred I. Nobel , William Brasch , Donald Thomson , Luis H. Garay
发明人： Fred I. Nobel , William Brasch , Donald Thomson , Luis H. Garay
IPC分类号： B01D61/44 , C25B1/00 , C25B1/22
CPC分类号： B01D61/44 , C25B1/00
摘要： A method for preparing nickel hypophosphite by contacting a nickel anode with a solution of hypophosphite anions and applying a current through the anode to a counter-electrode in contact with the solution to anodically dissolve the nickel of the anode into the hypophosphite solution, thereby forming a nickel hypophosphite solution. A one-compartment electrolysis cell and a three-or-more-compartment electrodialysis cell embodying the method of the invention are described.
摘要翻译：一种通过使镍阳极与次磷酸盐阴离子溶液接触并将电流通过阳极施加到与溶液接触的对电极来制备次磷酸镍的方法，以使阳极的镍阳极溶解到次磷酸盐溶液中，由此形成次磷酸镍溶液。描述了体现本发明方法的单室电解池和三室或更多室电渗析池。

2. 发明授权

US5480517A Electrolytic production of hypophosphorous acid 失效
公开(公告)号：US5480517A
公开(公告)日：1996-01-02
申请号：US307923
申请日：1994-09-16
申请人： Fred I. Nobel , William Brasch , Donald Thomson , Luis H. Garay
发明人： Fred I. Nobel , William Brasch , Donald Thomson , Luis H. Garay
IPC分类号： B01D61/44 , C01B25/165 , C25B1/22
CPC分类号： C25B1/22 , B01D61/44 , C01B25/165
摘要： Methods for preparing hypophosphorous acid are disclosed comprising contacting an insoluble anode with an aqueous solution of hypophosphite anions and applying a current through the insoluble anode to a cathode in electrical contact with the aqueous solution to generate H+ ions in the aqueous solution thereby forming a hypophosphorous acid solution.

3. 发明授权

US5378347A Reducing tin sludge in acid tin plating 失效
标题翻译：在酸性锡镀层中减少锡污泥
公开(公告)号：US5378347A
公开(公告)日：1995-01-03
申请号：US65104
申请日：1993-05-19
申请人： Donald Thomson , David A. Luke , Claudia Mosher
发明人： Donald Thomson , David A. Luke , Claudia Mosher
IPC分类号： C25D3/32 , C25D3/30 , C25D3/60 , C25D21/18
CPC分类号： C25D3/30
摘要： The present invention relates to a solution for use in the electroplating of tin and tin alloys comprising a basis solution which includes fluoboric acid or an organic sulfonic acid or one of their salts, divalent tin ions, and an antioxidant compound which includes a transition metal selected from the elements of Group IV B, V B or VI B of the Periodic Table in an amount effective to assist in maintaining the tin ions in the divalent state. Another aspect of the invention relates to a method for preventing, reducing or minimizing the oxidation of tin ions in an acid electroplating solution by adding one of these antioxidant compounds thereto. This method is effective in certain basis solutions even when iron contamination or high oxygen levels are present.
摘要翻译：本发明涉及一种用于锡和锡合金电镀的溶液，其包括基础溶液，其包含氟硼酸或有机磺酸或它们的一种盐，二价锡离子和包含所选择的过渡金属的抗氧化剂化合物从元素周期表第ⅣB族，Ⅴ族或ⅥB族元素中以有助于维持二价态的锡离子的量。本发明的另一方面涉及一种通过向其中加入这些抗氧化剂化合物之一来防止，减少或最小化酸性电镀溶液中锡离子氧化的方法。即使存在铁污染或高氧含量，该方法在某些基础溶液中也是有效的。

4. 发明授权

US4731389A Foam insulation and process for producing the same 失效
标题翻译：泡沫保温及其制造方法
公开(公告)号：US4731389A
公开(公告)日：1988-03-15
申请号：US798145
申请日：1985-11-14
申请人： R. Keene Christopher , Donald Thomson
发明人： R. Keene Christopher , Donald Thomson
IPC分类号： B29B7/74 , C04B28/00 , C04B28/10 , C04B28/26 , C04B28/30 , E04B1/76 , E04F21/08 , C08J9/30 , B29C39/10 , C08J9/32 , E04B2/34
CPC分类号： B29B7/7438 , C04B28/02 , C04B28/26 , E04B1/7604 , E04F21/085 , C04B2111/28 , Y02W30/92 , Y10S264/06
摘要： The invention relates to foams for insulating cavities and structures, such as spaces between walls in houses. The inventive foam compositions are prepared in separate portions, generally comprising (A) cement and (B) foam. Air is added initially to foam one of the components or a mixture of components.In a first embodiment, the first component comprises an aqueous solution of polyvinyl alcohol and a dispersant. This component is mechanically foamed by injection of air, for example. After the mechanical foaming a second, cement component is added to the first component. This second component comprises an aqueous solution, mixture or suspension of magnesium oxide and barium metaborate, and a dispersant.In a second, preferred embodiment, the first component comprises an aqueous solution of polyvinyl alcohol and calcium chloride, which component is mechanically foamed by injection of air. After the foaming a second component is added, comprising an aqueous solution of Portland Cement, a dispersant and sodium metaborate.
摘要翻译：本发明涉及用于绝缘空腔和结构的泡沫，例如房屋中墙壁之间的空间。本发明的泡沫组合物分别制备，通常包含（A）水泥和（B）泡沫。最初添加空气来泡沫组分之一或组分的混合物。在第一实施方案中，第一组分包含聚乙烯醇的水溶液和分散剂。例如，该组分通过注入空气机械发泡。在第二次机械发泡之后，将水泥组分加入到第一组分中。该第二组分包括氧化镁和偏硼酸钡的水溶液，混合物或悬浮液以及分散剂。在第二个优选实施方案中，第一组分包含聚乙烯醇和氯化钙的水溶液，该组分通过注入空气机械发泡。在发泡后，加入第二组分，其包含波特兰水泥水溶液，分散剂和偏硼酸钠。

5. 发明授权

US5312539A Electrolytic tin plating method 失效
标题翻译：电解锡电镀法
公开(公告)号：US5312539A
公开(公告)日：1994-05-17
申请号：US76750
申请日：1993-06-15
申请人： Donald Thomson
发明人： Donald Thomson
IPC分类号： C25D3/30 , C25D21/14 , C25D21/22 , C25D21/18
CPC分类号： C25D3/30 , Y10S204/13
摘要： A method for plating tin onto the surface of steel strip in an acidic electrolyte bath utilizing insoluble anodes is disclosed. Free acid in the bath is extracted from the bath and concentrated. Tin is dissolved in the concentrated extract and the extract is returned to the bath to replenish the tin in the bath.
摘要翻译：公开了一种在使用不溶性阳极的酸性电解液槽中将锡镀在钢带表面上的方法。浴中的游离酸从浴中提取并浓缩。将锡溶解在浓缩的提取物中，并将提取物返回到浴中以补充浴中的锡。

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