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1. 发明授权

US07988919B2 Laboratory scale continuous flow hydrogenation process 有权
标题翻译：实验室规模连续流加氢工艺
公开(公告)号：US07988919B2
公开(公告)日：2011-08-02
申请号：US12907239
申请日：2010-10-19
申请人： Ferenc Darvas , Lajos Godorhazy , Tamas Karancsi , Daniel Szalay , Ferenc Boncz , Laszlo Urge
发明人： Ferenc Darvas , Lajos Godorhazy , Tamas Karancsi , Daniel Szalay , Ferenc Boncz , Laszlo Urge
IPC分类号： G05D16/00 , B01J19/00
CPC分类号： B01J10/007 , B01J10/002 , B01J23/44 , B01J2208/00539 , B01J2208/00548 , B01J2219/00011 , B01J2219/0002 , B01J2219/00038 , B01L5/00
摘要： A process for hydrogenating a sample in a pressure range below supercritical pressure values includes supplying at least a solvent of the sample to be hydrogenated by a feed pump with a constant volume rate into a flow path to create a base solution; adding the sample being dissolved into the flow path; feeding hydrogen into the flow path through a valve configured to transmit hydrogen only into a single direction; leading the dissolved sample in the presence of a catalyst through a hydrogenation reactor, where the reactor is inserted into a section of the flow path located after the hydrogen feeding position; maintaining the pressure of the reaction in a given pressure range by element of a pressure-adjusting unit, and collecting a hydrogenate formed within the hydrogenation reactor in a product receptacle connected to the end of the flow path.
摘要翻译：在低于超临界压力值的压力范围内对样品进行氢化的方法包括：将具有恒定体积比率的进料泵至少将被氢化的样品的溶剂供应到流路中以产生碱溶液; 将溶解的样品加入到流路中; 通过构造成将氢气仅仅传输到单个方向的阀将氢气供给到流路; 在催化剂存在下通过氢化反应器引导溶解的样品，其中反应器插入位于氢气供给位置之后的流路的一部分中; 通过压力调节单元的元件保持在给定压力范围内的反应压力，以及在连接到流路端部的产品容器中收集在氢化反应器内形成的氢化物。

2. 发明申请

US20070212268A1 Laboratory-scale hydrogenation cartridge reactor for hydrogenating an inflowing multi-component fluid composition 审中-公开
标题翻译：用于氢化流入的多组分流体组合物的实验室规模的氢化反应器
公开(公告)号：US20070212268A1
公开(公告)日：2007-09-13
申请号：US11709258
申请日：2007-02-22
申请人： Ferenc Darvas , Lajos Godorhazy , Tamas Karancsi , Daniel Szalay , Ferenc Boncz , Laszlo Urge
发明人： Ferenc Darvas , Lajos Godorhazy , Tamas Karancsi , Daniel Szalay , Ferenc Boncz , Laszlo Urge
IPC分类号： B01J8/18
CPC分类号： B01J8/0221 , B01J8/006 , B01J8/008 , B01J2208/00814 , B01J2208/00884 , B01J2219/00011
摘要： A laboratory-scale hydrogenation cartridge reactor for hydrogenating an inflowing multi-component fluid composition includes a flow inlet defining an inflow cross-section and used for introducing the fluid composition, a flow outlet defining an outflow cross-section for discharging the hydrogenated fluid, a closed reaction volume extending between and communicating with the inlet and outlet and having a useful space of at most 10 cm3. The reaction volume is filled with an immobilized packing medium that increases flow resistance and facilitates mixing of the fluid composition. The flow inlet and the flow outlet are formed with respective detachable connection structures. A steep transitional zone is defined between the inflow side of the reaction volume and the flow inlet, wherein the cross-section of the widest portion of the steep transitional zone where the zone communicates with the reaction volume is significantly larger than the inflow cross-section.
摘要翻译：用于氢化流入的多组分流体组合物的实验室规模的氢化反应器包括限定流入横截面并用于引入流体组合物的流入口，限定用于排出氢化流体的流出横截面的流出口，闭合反应体积在入口和出口之间延伸并与入口和出口连通，并且具有至多10cm 3的有用空间。反应体积填充固定的填充介质，其增加流动阻力并促进流体组合物的混合。流入口和流出口形成有各自可拆卸的连接结构。在反应体积的流入侧和流入口之间限定陡峭的过渡区域，其中该区域与反应体积连通的陡峭过渡区域的最宽部分的横截面显着大于流入横截面。

3. 发明申请

US20090101519A1 FLOW-TYPE LABORATORY OZONOLYSIS APPARATUS AND METHOD OF PERFORMING OZONOLYSIS REACTION 审中-公开
标题翻译：流动型实验室臭氧分析装置及其执行臭氧反应的方法
公开(公告)号：US20090101519A1
公开(公告)日：2009-04-23
申请号：US12158814
申请日：2006-12-22
申请人： Daniel Szalay , Norbert Varga , Ferenc Boncz , Ferenc Darvas , Tamas Karancsi , Lajos Godorhazy , Laszlo Urge
发明人： Daniel Szalay , Norbert Varga , Ferenc Boncz , Ferenc Darvas , Tamas Karancsi , Lajos Godorhazy , Laszlo Urge
IPC分类号： C25B1/13
CPC分类号： B01J19/0093 , B01J2219/00783 , B01J2219/00788 , B01J2219/00833 , B01J2219/00835 , B01J2219/0086 , B01J2219/00867 , B01J2219/00873 , B01J2219/00889 , B01J2219/00891 , B01J2219/0095 , B01J2219/00986 , C07C29/48 , C07C231/10 , C25B1/13 , C25B9/08 , C25B11/04 , C07C233/25 , C07C33/22 , C07C33/24
摘要： A flow-type laboratory scale ozonolysis apparatus (100) according to the invention comprises a reservoir (104), a n feed pump (102), a mixing element (120) with two inlets and an outlet, a reactor unit (110) and a pressure-adjusting means (160), all connected into a flow path. The ozonolysis apparatus (100) further comprises an ozone source (110), as well as a dispensing valve (112) transmitting a gas stream only in a single direction and installed between the ozone source (110) and one of the inlets of the mixing element (120). The feed pump (102) of the ozonolysis apparatus (100) according to the invention is a liquid pump generating a constant volume rate, the reservoir (104) contains at least the substance, as a solute, to be subjected to the ozonolysis reaction and the reactor unit consists of first and second reactor zones differing in function from one another. In the flow path, the outlet of the first reactor zone is connected to the inlet of the second reactor zone. Furthermore, an inlet for feeding in substances is inserted into the flow path between the reactor zones, and the pressure-adjusting means (160) is installed into the flow path after the reactor unit and is provided with an electrically governed control.
摘要翻译：根据本发明的流式实验室规模臭氧分解装置（100）包括储存器（104），进料泵（102），具有两个入口和出口的混合元件（120），反应器单元（110）和压力调节装置（160），全部连接到流路中。臭氧分解装置（100）还包括臭氧源（110）以及仅在单个方向上传输气流并且安装在臭氧源（110）和混合入口之一之间的分配阀（112）元件（120）。根据本发明的臭氧分解装置（100）的进料泵（102）是产生恒定体积比的液体泵，储存器（104）至少含有作为溶质的待进行臭氧分解反应的物质，反应器单元由功能彼此不同的第一和第二反应器区组成。在流动路径中，第一反应器区的出口连接到第二反应器区的入口。此外，用于进料物质的入口插入在反应器区域之间的流动路径中，并且压力调节装置（160）安装在反应器单元之后的流动路径中并且被设置有电控制的控制。

4. 发明申请

US20070122315A1 Flow-type laboratory hydrogenation apparatus and laboratory hydrogenation process using the apparatus 有权
标题翻译：流式实验室加氢装置和实验室加氢过程采用该装置
公开(公告)号：US20070122315A1
公开(公告)日：2007-05-31
申请号：US11593601
申请日：2006-11-07
申请人： Ferenc Darvas , Lajos Godorhazy , Tamas Karancsi , Daniel Szalay , Ferenc Boncz , Laszlo Urge
发明人： Ferenc Darvas , Lajos Godorhazy , Tamas Karancsi , Daniel Szalay , Ferenc Boncz , Laszlo Urge
IPC分类号： B01J8/00 , B01J19/00
CPC分类号： B01J10/007 , B01J10/002 , B01J23/44 , B01J2208/00539 , B01J2208/00548 , B01J2219/00011 , B01J2219/0002 , B01J2219/00038 , B01L5/00
摘要： A flow-type laboratory hydrogenation apparatus (100) comprises a reservoir (104), a feed pump (102), a mixing element (108) with two inlets and an outlet, a hydrogenation reactor (110) and a pressure-adjusting unit (112), all connected into a flow path. The apparatus (100) also comprises a hydrogen source (126) and a one-way valve (120) arranged between the hydrogen source (126) and the second inlet of the mixing element (108). The feed pump (102) is realized by a pump providing a constant volume rate. The reservoir (104) contains at least the solvent, as base solution, of the sample to be hydrogenated. The hydrogenation reactor (110) is connected into the flow path by means of detachable connections and is formed as a replaceable cartridge which contains a packing which increases the flow resistance and facilitates mixing of the liquid and gaseous components. The pressure-adjusting unit (112) is connected into the flow path after the hydrogenation reactor (110) and is provided with a regulation controlled electrically.
摘要翻译：流式实验室加氢装置（100）包括储存器（104），进料泵（102），具有两个入口和出口的混合元件（108），氢化反应器（110）和压力调节单元 112），全部连接成流路。装置（100）还包括氢源（126）和布置在氢源（126）和混合元件（108）的第二入口之间的单向阀（120）。进料泵（102）由提供恒定体积速率的泵实现。储存器（104）至少含有待氢化的样品的溶剂作为碱溶液。氢化反应器（110）通过可拆卸的连接件连接到流动路径中，并且形成为可更换的筒，其包含增加流动阻力并促进液体和气体组分的混合的填料。压力调节单元（112）在氢化反应器（110）之后连接到流路中，并且具有电控调节。

5. 发明申请

US20080314740A1 Ozone Generating Electrolysis Cell 审中-公开
标题翻译：臭氧发生电解池
公开(公告)号：US20080314740A1
公开(公告)日：2008-12-25
申请号：US12158909
申请日：2006-12-22
申请人： Daniel Szalay , Norbert Varga , Ferenc Boncz , Ferenc Darvas , Tamas Karancsi , Lajos Godorhazy
发明人： Daniel Szalay , Norbert Varga , Ferenc Boncz , Ferenc Darvas , Tamas Karancsi , Lajos Godorhazy
IPC分类号： C25B9/00 , C25B1/13
CPC分类号： C25B1/13 , C25B9/08 , C25B11/04
摘要： The ozone generating electrolysis cell (10) according to the invention has a negative electrode (13) and an ozone generating positive electrode (16) comprising a mixture of lead dioxide and polytetrafluoroethylene (PTFE). A proton conducting solid electrolytic membrane (15) is arranged between the negative and positive electrodes (13, 16). The ozone generating electrolysis cell (10) also comprises an electrically conducting, liquid and gas permeable first electrode support (17) in contact with a side of the positive electrode (16) located opposite to the membrane (15), wherein said side of the electrode support (17) has a surface covered with a platinum-containing layer. The positive electrode (16) is made of a mixture prepared by the high-pressure compression of lead dioxide grains of colloid size and PTFE filaments having a dimension of at most 1 mm. Furthermore, the negative electrode (13) is adjoined to a side of the membrane (15) located opposite to the positive electrode (16) by a given compressing force and is formed on a surface of a porous second electrode support (12).
摘要翻译：根据本发明的臭氧发生电解槽（10）具有负极（13）和包含二氧化铅和聚四氟乙烯（PTFE）的混合物的产生臭氧的正极（16）。质子传导固体电解质膜（15）设置在负极和正极（13,16）之间。臭氧发生电解槽（10）还包括与位于与膜（15）相对的正电极（16）的一侧接触的导电，液体和气体可透过的第一电极支撑件（17），其中电极支撑件（17）具有被含铂层覆盖的表面。正极（16）由通过高压压缩胶体尺寸的二氧化铅颗粒和尺寸至多为1mm的PTFE细丝制成的混合物制成。此外，负极（13）通过给定的压缩力与位于与正极（16）相对的膜（15）的一侧相邻，并形成在多孔第二电极支撑体（12）的表面上。

6. 发明申请

US20090098029A1 METHOD OF FORMING A SEALED CHANNEL OF A MICROFLUIDIC REACTOR AND A MICROFLUIDIC REACTOR COMPRISING SUCH CHANNEL 有权
标题翻译：形成微流化反应器的密封通道的方法和包含这种通道的微流化反应器
公开(公告)号：US20090098029A1
公开(公告)日：2009-04-16
申请号：US12158784
申请日：2006-12-22
申请人： Daniel Szalay , Norbert Varga , Ferenc Boncz , Ferenc Darvas , Tamas Karancsi , Lajos Godorhazy
发明人： Daniel Szalay , Norbert Varga , Ferenc Boncz , Ferenc Darvas , Tamas Karancsi , Lajos Godorhazy
IPC分类号： B01J19/00 , B29C59/04
CPC分类号： B81C1/0046
摘要： In a method according to the invention for forming a sealed channel (125) in the surface of a sheet made of a material with certain extent of plasticity, the machining surface of a tool with a rolling machining surface is brought into contact with a first point of the channel (125) to be formed in the surface of the sheet constituting a reactor block. Next, said machining surface is pressed onto the surface of the sheet with a compressive force (F) required to achieve the depth of the channel (125) to be formed, whereby the plastic material is squeezed out and becomes raised from the sheet surface on the peripheries of the depression being formed. After this, while maintaining the compressive force (F), by displacing said machining surface along the centerline of the channel (125) over the sheet surface it is rolled from the first point of the channel (125) to be formed to a second point thereof, whereby the channel (125) is machined in the material of the sheet and sealing edges (127) are created on the peripheries of the channel (125) from the material squeezed out and become raised. After creating said sealing edges (127), a closing member bearing against the sealing edges (127) is arranged at the surface of the sheet provided with the channel (125) and the sealing edges (127), and then said closing member is pressed onto the sheet by a compressive force required to deform said sealing edges (127) and is fixed in the position obtained, whereby a sealed channel (125) running between the first and second points is formed within the reactor block.
摘要翻译：在根据本发明的用于在由具有一定塑性的材料制成的片材的表面中形成密封通道（125）的方法中，具有滚动加工表面的工具的加工表面与第一点的通道（125）形成在构成反应器块的片材的表面中。接下来，所述加工表面以实现要形成的通道（125）的深度所需的压缩力（F）被压在片材的表面上，由此塑料材料被挤出并从片材表面升高形成凹陷的周边。此后，在保持压缩力（F）的同时，通过沿着通道（125）的中心线将所述加工表面移动在片材表面上，其从通道（125）的第一点被轧制以形成第二点由此通道（125）在片材的材料中加工，并且密封边缘（127）由挤出的材料在通道（125）的周边上产生并升高。在形成所述密封边缘（127）之后，在设置有通道（125）和密封边缘（127）的片材的表面处布置有抵靠密封边缘（127）的封闭构件，然后按压所述封闭构件通过使所述密封边缘（127）变形所需的压缩力而被固定在片材上，并被固定在所获得的位置，由此在反应器块内形成在第一和第二点之间运行的密封通道（125）。

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