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1. 发明授权

US3978103A Sulfur containing organosilicon compounds 失效
标题翻译：含硫的有机硅化合物
公开(公告)号：US3978103A
公开(公告)日：1976-08-31
申请号：US467583
申请日：1974-05-06
申请人： Eugen Meyer-Simon , Werner Schwarze , Friedrich Thurn , Rudolf Michel
发明人： Eugen Meyer-Simon , Werner Schwarze , Friedrich Thurn , Rudolf Michel
IPC分类号： C07F7/18 , C08K5/548 , C09C1/30 , C23F11/16
CPC分类号： B82Y30/00 , C07F7/1804 , C08K5/548 , C09C1/3081 , C23F11/16 , C01P2004/62 , C01P2004/64 , C01P2004/80 , C01P2006/12 , Y10T152/10495
摘要： Sulfur containing organosilicon compounds are prepared having the formula:Z -- Alk -- S.sub.n -- Alk -- Zin which Z is: ##EQU1## where R.sub.1 and R.sub.alkyl of 1 to 4 carbon atoms or phenyl andR.sub.2 is alkoxy of 1 to 8 carbon atoms, cycloalkoxy of 5 to 8 carbon atoms or alkylmercapto of 1 to 8 carbon atoms, alk is a divalent aliphatic hydrocarbon or unsaturated aliphatic hydrocarbon or a cyclic hydrocarbon containing 1 to 18 carbon atoms and n is a whole number from 2 to 6.

2. 发明授权

US09580674B2 Method for adding hops in beer manufacture 有权
标题翻译：在啤酒制造中添加啤酒花的方法
公开(公告)号：US09580674B2
公开(公告)日：2017-02-28
申请号：US14112149
申请日：2012-03-08
申请人： Ludwig Scheller , Rudolf Michel , Patrick Bahns
发明人： Ludwig Scheller , Rudolf Michel , Patrick Bahns
IPC分类号： C12C3/00 , B01F3/08 , B01F5/06 , B01F13/10 , C12C7/22 , C12C13/00
CPC分类号： C12C3/00 , B01F3/0807 , B01F5/0661 , B01F13/103 , B01F2003/0849 , C12C7/22 , C12C13/00
摘要： The invention relates to a method for adding hops in beer manufacture, having the following process steps; a) separation of a sub-quantity (07a) of water and/or wort (07) and/or beer as an aqueous fluid, b) addition of hop extract (10) in liquid or pasty form to the separated aqueous fluid (07a), c) production of a macroemulsion (13) of the hop extract by emulsifying the hop extract (10) in the aqueous fluid (07a), d) increasing the pressure in the macroemulsion (13) of the hop extract to a feed pressure of in particular higher than 100 bar, e) production of a microemulsion (17) of the hop extract by feeding the pressurized macroemulsion (13) through a gap or a valve (16) or by feeding the pressurized macroemulsion against a baffle plate, f) at least partial return of the microemulsion (17) of the hop extract to the beer manufacturing process.
摘要翻译：本发明涉及啤酒加工啤酒花的方法，具有以下工艺步骤; a）以水和/或麦芽汁（07）和/或啤酒作为水性液体分离子量（07a）和/或啤酒; b）将液体或糊状形式的啤酒花提取物（10）加入到分离的含水流体（07a）），c）通过在水性流体（07a）中乳化啤酒花提取物（10）来生产啤酒花提取物的粗乳液（13），d）将啤酒花提取物的粗乳液（13）中的压力增加到进料压力特别是高于100巴，e）通过将加压的粗乳液（13）通过间隙或阀（16）供给或通过将加压的宏乳剂输送到挡板上来生产啤酒花提取物的微乳液（17），f ）啤酒花提取物的微乳液（17）的至少部分返回到啤酒制造过程。

3. 发明授权

US4129585A Process for the production of sulfur containing organosilicon compounds 失效
标题翻译：含硫有机硅化合物生产工艺
公开(公告)号：US4129585A
公开(公告)日：1978-12-12
申请号：US884212
申请日：1978-03-07
申请人： Wolfgang Buder , Hans-Dieter Pletka , Rudolf Michel , Rudolf Schwarz , Gerhard Dusing
发明人： Wolfgang Buder , Hans-Dieter Pletka , Rudolf Michel , Rudolf Schwarz , Gerhard Dusing
IPC分类号： C07F7/18 , C08K5/548 , C08K5/549 , C07F7/08 , C07F7/10
CPC分类号： C08K5/548 , C07F7/1892 , C08K5/549
摘要： There is provided a process for the production of sulfur containing organosilicon compounds of the formula (I) Z -- Alk -- S.sub.x -- Alk -- Z, where Z is the grouping: ##STR1## in which R.sup.1 is an alkyl group having 1 to 5 carbon atoms, a cycloalkyl group with 5 to 8 carbon atoms, the benzyl group, phenyl or phenyl substituted with at least one methyl, ethyl or chloro group, R.sup.2 is alkoxy of 1 to 4 carbon atoms, methoxyethoxy, cycloalkoxy with 5 to 8 carbon atoms, phenoxy or benzyloxy, R.sup.3 and R.sup.4 are alkyl of 1 to 3 carbon atoms or hydrogen, Alk is divalent saturated hydrocarbon group having 1 to 5 carbon atoms or such a group interrupted by --O--, --S-- or --NH-- and x is a number from 2.0 to 6.0 comprising reacting an alkali metal alcoholate, preferably in alcoholic solution with a compound of the formula (II) Z -- Alk -- Hal, where Hal is chlorine, bromine or iodine with a hydrosulfide of the formula (III) MeSH, in which Me is ammonium, an alkali metal atom or an equivalent of an alkaline earth metal or zinc and with sulfur, preferably in the presence of at least one organic solvent, separating from the halide formed, and removing the organic solvent.
摘要翻译：提供了一种制备式（I）Z-Alk-Sx-Alk-Z的含硫有机硅化合物的方法，其中Z是分组：其中R 1是烷基具有1至5个碳原子的环烷基，具有5至8个碳原子的环烷基，苄基，苯基或被至少一个甲基，乙基或氯基取代的苯基，R 2是1至4个碳原子的烷氧基，甲氧基乙氧基， 5至8个碳原子，苯氧基或苄氧基，R3和R4是1至3个碳原子的烷基或氢，Alk是具有1至5个碳原子的二价饱和烃基或被-O - ， - S-或 - -NH-，x是2.0至6.0的数，包括使碱金属醇盐，优选在醇溶液中与式（II）化合物Z-Alk-Hal反应，其中Hal为氯，溴或碘，其中硫氢化物为 Me III，其中Me为铵，碱金属原子或碱性ea当量第二金属或锌和硫，优选在至少一种有机溶剂的存在下，与形成的卤化物分离，并除去有机溶剂。

4. 发明授权

US4072701A Process for the production of sulfur containing organosilicon compounds 失效
标题翻译：含硫有机硅化合物生产工艺
公开(公告)号：US4072701A
公开(公告)日：1978-02-07
申请号：US730726
申请日：1976-09-24
申请人： Hans-Dieter Pletka , Rudolf Michel
发明人： Hans-Dieter Pletka , Rudolf Michel
IPC分类号： C07F7/08 , C07F7/18 , C08K5/548 , C08K5/549
CPC分类号： C08K5/548 , C07F7/1892 , C08K5/549
摘要： There is provided a process for the production of sulfur containing organosilicon compounds of the formula (I) Z--Alk--S.sub.x --Alk--Z, where Z is the grouping: ##STR1## in which R.sup.1 is an alkyl group having 1 to 8 carbon atoms, a cycloalkyl group with 5 to 8 carbon atoms, the benzyl group, phenyl or phenyl substituted with at least one methyl, ethyl or chloro group and R.sup.2 is alkoxy of 1 to 8 carbon atoms, methoxyethoxy, cycloalkoxy with 5 to 8 carbon atoms, phenoxy or benzyloxy, Alk is divalent saturated hydrocarbon group having 1 to 10 carbon atoms or such a group interrupted once or twice by --O--, --S-- or --NH-- and x is a number from 2.0 to 6.0 comprising reacting a compound of the formula (II) Y--Alk--Hal, where Y is: ##STR2## WHERE Hal is fluorine, chlorine, bromine or iodine with at least one compound of the formula R.sup.3 OH in which R.sup.3 is alkyl of 1 to 8 carbon atoms, methoxyethyl, cycloalkyl with 5 to 8 carbon atoms, phenyl or benzyl or in the case of forming (d) reacting a tris alkoxysilane with triethanolamine to form the corresponding silatrane and with a hydrosulfide of the formula (III) MeSH, in which Me is ammonium, an alkali metal atom or an equivalent of an alkaline earth metal and with sulfur, preferably in the presence of at least one organic solvent, separating from the halide formed, and removing the organic solvent.
摘要翻译：提供了制备式（I）的Z-Alk-Sx-Alk-Z的含硫有机硅化合物的方法，其中Z是分组：其中R 1是具有1个 8个碳原子的环烷基，具有5至8个碳原子的环烷基，苄基，苯基或被至少一个甲基，乙基或氯基取代的苯基，R 2是1至8个碳原子的烷氧基，甲氧基乙氧基，环烷氧基， 8个碳原子，苯氧基或苄氧基，Alk是具有1-10个碳原子的二价饱和烃基，或者被-O - ， - S-或-NH-中断一次或两次的基团，x是2.0至6.0的数，包括使式（II）Y-Alk-Hal的化合物与其中Y是：其中Hal是氟，氯，溴或碘与至少一种式R 3 OH的化合物反应，其中R 3是1至8的烷基碳原子，甲氧基乙基，具有5至8个碳原子的环烷基，苯基或苄基，或在形成（d）使三烷氧基硅烷 e与三乙醇胺形成相应的硅藻土和与式（III）MeSH的氢硫化物，其中Me是铵，碱金属原子或碱当量的碱土金属和硫，优选在至少一种有机溶剂，与形成的卤化物分离，除去有机溶剂。

5. 发明授权

US06531539B2 Organosilicon compounds 失效
标题翻译：有机硅化合物
公开(公告)号：US06531539B2
公开(公告)日：2003-03-11
申请号：US09825866
申请日：2001-04-05
申请人： Roland Krafczyk , Rudolf Michel , Jörg Münzenberg , Hans-Detlef Luginsland
发明人： Roland Krafczyk , Rudolf Michel , Jörg Münzenberg , Hans-Detlef Luginsland
IPC分类号： C08L8304
CPC分类号： C08K5/5442 , C07D251/16 , C07D251/22 , C07D251/46 , C07D251/52 , C07F7/1804 , C08K5/0025 , C08K5/3492
摘要： The invention is directed to organosilicon compounds of the general formula prepared by reacting triazine compounds with functional groups (e.g., chlorine) and corresponding compounds (e.g., mercapto). The organosilicon compounds can be used in rubber mixtures.
摘要翻译：本发明涉及通过使三嗪化合物与官能团（例如氯）和相应的化合物（例如巯基）反应而一般制备的有机硅化合物。有机硅化合物可用于橡胶混合物中。

6. 发明授权

US5314533A Aqueous emulsions containing organosilicon compounds for the impregnation of inorganic materials 失效
标题翻译：含有有机硅化合物的含水乳液用于浸渍无机材料
公开(公告)号：US5314533A
公开(公告)日：1994-05-24
申请号：US902882
申请日：1992-06-23
申请人： Thomas Goebel , Rudolf Michel , Harald Alff , Josef Karl
发明人： Thomas Goebel , Rudolf Michel , Harald Alff , Josef Karl
IPC分类号： B01F17/54 , B01J13/00 , C04B41/49 , C04B41/64 , C07F7/18 , C08G65/336 , C08L71/02 , C08L83/02 , C08L83/04 , C09K3/18 , C09D201/10
CPC分类号： C04B41/4905 , C04B41/4922 , C07F7/1824 , C07F7/1832 , C07F7/1836 , C07F7/184 , C09K3/18 , C04B2111/00112
摘要： Aqueous emulsions are disclosed containing organosilicon compounds for the impregnation of inorganic materials, in particular building materials, containing alkoxysilanes and silane surfactants. The emulsions comprise 1-80% by weight of one alkoxy silane, ##STR1## X.dbd.H,cl,Br, I, NH.sub.2, SCN, CN, N.sub.3, NHR, NR, NR.sub.3, --S.sub.x --, aryl or alkenyla.dbd.0 or 1b.dbd.1 or 2and, 1-30% of an organosilicon compound ##STR2##
摘要翻译：公开了含有用于浸渍含有烷氧基硅烷和硅烷表面活性剂的无机材料，特别是建筑材料的有机硅化合物的乳液。乳液包含1-80重量％的一个烷氧基硅烷，X = H，Cl，Br，I，NH 2，SCN，CN，N 3，NHR，NR，NR 3，-S x - ，芳基或链烯基a = 0或1b = 1或2，和1-30％的有机硅化合物＆lt; IMAGE＆gt;

7. 发明授权

US4623740A N,N'- and N,N',N'-substituted silylureas and process for their production 失效
标题翻译： N，N'-和N，N'，N'-取代的甲硅烷基脲及其制备方法
公开(公告)号：US4623740A
公开(公告)日：1986-11-18
申请号：US750272
申请日：1985-07-01
申请人： Ulrich Deschler , Wolfgang Buder , Peter Kleinschmit , Rudolf Michel
发明人： Ulrich Deschler , Wolfgang Buder , Peter Kleinschmit , Rudolf Michel
IPC分类号： C07F7/18 , C07F7/10
CPC分类号： C07F7/182
摘要： The invention is directed to N,N' and N,N',N'-substituted silylureas and a process for their production in which in a single step process there are reacted a halogenoalkylsilane or a halogenbenzylsilane with a primary or secondary amine and an alkali cyanate in equimolar amounts.
摘要翻译：本发明涉及N，N'和N，N'，N'-取代的甲硅烷基脲及其制备方法，其中在单步骤中使卤代烷基硅烷或卤代苄基硅烷与伯胺或仲胺和碱反应氰酸酯等摩尔量。

8. 发明授权

US3997581A Process for the production of sulfur containing organosilicon compounds 失效
标题翻译：含硫有机硅化合物生产工艺
公开(公告)号：US3997581A
公开(公告)日：1976-12-14
申请号：US546084
申请日：1975-01-31
申请人： Hans-Dieter Pletka , Rudolf Michel
发明人： Hans-Dieter Pletka , Rudolf Michel
IPC分类号： C07F7/08 , C07F7/18 , C08K5/548 , C08K5/549 , C07F7/10
CPC分类号： C08K5/548 , C07F7/1892 , C08K5/549
摘要： Compounds are prepared having the formulaZ--Alk--S.sub.x --Alk Z Iwherein Z is ##STR1## where R.sup.1 is an alkyl group of 1 to 4 carbon atoms, a cycloalkyl group having 5 to 8 carbon atoms or phenyl,R.sup.2 is an alkoxy group of 1 to 8 carbon atoms, a cycloalkoxy group of 5 to 8 carbon atoms or phenoxy,Alk is a divalent hydrocarbon chain of 1 to 10 carbon atoms which can be interrupted with one or two --O--, --S-- or --NH group, andX is a number of 2 to 6 by reacting a compound having the formulaIi. z--alk--SH with sulfur. Some of the compounds are novel and some are old, e.g., in Meyer-Simon U.S. Pat. No. 3,842,111. The compounds are useful as bonding agents in sulfur vulcanizable rubbers.
摘要翻译：制备具有式Z-Alk-Sx-Alk ZI的化合物，其中Z是其中R 1是1至4个碳原子的烷基，具有5至8个碳原子的环烷基或苯基，R 2是烷氧基 1〜8个碳原子的环烷氧基或苯氧基，Alk是1〜10个碳原子的二价烃链，其可以被一个或两个-O - ， - S-或-NH基团中断并且X是通过使具有式II的化合物反应而为2至6的数。 Z-Alk-SH与硫。一些化合物是新颖的，一些化合物是老的，例如在Meyer-Simon的美国专利中。 3,842,111。这些化合物可用作硫磺可硫化橡胶中的粘合剂。

9. 发明授权

US06506922B2 Process for the production of yellow bis(3-[triethoxysilyl]-propyl) polysulfane 有权
标题翻译：制备黄色双（3- [三乙氧基甲硅烷基] - 丙基）多硫烷的方法
公开(公告)号：US06506922B2
公开(公告)日：2003-01-14
申请号：US09948712
申请日：2001-09-10
申请人： Roland Krafczyk , Ulrich Deschler , Rudolf Michel , Christoph Batz-Sohn
发明人： Roland Krafczyk , Ulrich Deschler , Rudolf Michel , Christoph Batz-Sohn
IPC分类号： C07F708
CPC分类号： C07F7/188 , C07F7/1892
摘要： Process for the production of yellow bis(3-[triethoxysilyl]propyl)polysulfane with an average sulfur chain length of less than 4 and an iodine colour value of ≦10 mg iodine/100 ml, wherein neutral chloropropyltriethoxysilane is mixed with chloropropyltrichlorosilane and then reacted with sodium sulfide (Na2S) and sulfur, disodium tetrasulfide (Na2S4) and Na2S or disodium trisulfide (Na2S3) and Na2S in ethanol.
摘要翻译：制备平均硫链长度小于4且碘色值<= 10mg碘/ 100ml的黄色双（3- [三乙氧基甲硅烷基]丙基）多硫烷的方法，其中中性氯丙基三乙氧基硅烷与氯丙基三氯硅烷混合，然后与硫化钠（Na2S）和硫磺，二硫化二钠（Na2S4）和Na2S或二硫化钠（Na2S3）和Na2S在乙醇中反应。

10. 发明授权

US06465672B2 Process for the production of organosilylalkyl polysulfanes 有权
标题翻译：生产有机硅烷基烷基聚硫烷的方法
公开(公告)号：US06465672B2
公开(公告)日：2002-10-15
申请号：US09795709
申请日：2001-03-01
申请人： Rudolf Michel , Jorg Munzenberg , Werner Will , Gerd Rainhard Zezulka
发明人： Rudolf Michel , Jorg Munzenberg , Werner Will , Gerd Rainhard Zezulka
IPC分类号： C07F708
CPC分类号： C07F7/1892
摘要： The invention relates to a process for the production of organosilylalkyl polysulfanes by reacting an organosilylalide alkyl halide and an anhydrous or virtually anhydrous ionic sulfide and elementary sulfur, wherein the elementary sulfur and organosilylalkyl halide are suspended in a polar organic solvent and the ionic sulfide is added to this suspension.
摘要翻译：本发明涉及一种通过使有机甲硅烷基烷基卤化物与无水或几乎无水的离子性硫化物和元素硫反应生产有机甲硅烷基烷基聚磺酰胺的方法，其中将单体硫和有机甲硅烷基烷基卤化物悬浮于极性有机溶剂中，并加入离子硫化物到这个暂停。

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