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1. 发明授权

US07391212B2 Resonator apparatus for electron spin resonance (ESR) measurements and method for measuring electron spin resonance (ESR) signals 有权
标题翻译：用于电子自旋共振（ESR）测量的谐振器装置和用于测量电子自旋共振（ESR）信号的方法
公开(公告)号：US07391212B2
公开(公告)日：2008-06-24
申请号：US10197236
申请日：2002-07-15
申请人： Diether Maier , Dieter Schmalbein , Andreas Kamlowski , Marian Kloza , Peter Hoefer
发明人： Diether Maier , Dieter Schmalbein , Andreas Kamlowski , Marian Kloza , Peter Hoefer
IPC分类号： G01V3/00
CPC分类号： G01R33/307 , G01R33/34 , G01R33/60
摘要： A resonator apparatus and a method for electron spin resonance (ESR) measurements are disclosed. The resonator apparatus comprises a dielectric resonator and a sample vessel extending through the resonator. The sample vessel is configured as one single flexible tube. Means are provided for conveying a liquid sample substance through the flexible tube. According to the method a liquid sample substance is guided through the sample vessel, wherein the sample substance is gated by cyclically conveying and stopping, resp., a flow of the sample substance. A measurement is conducted within the resonator when the flow of sample substance is stopped.
摘要翻译：公开了一种用于电子自旋共振（ESR）测量的谐振器装置和方法。谐振器装置包括介质谐振器和延伸穿过谐振器的样品容器。样品容器配置为单个柔性管。提供用于通过柔性管输送液体样品物质的装置。根据该方法，液体样品物质被引导通过样品容器，其中通过循环输送和停止或样品物质的流动来选择样品物质。当样品物质的流动停止时，在谐振器内进行测量。

2. 发明授权

US07397247B2 Apparatus and probe head for determining a quantitative property of a sample substance by means of magnetic resonance 有权
标题翻译：用于通过磁共振确定样品物质的定量性质的装置和探针头
公开(公告)号：US07397247B2
公开(公告)日：2008-07-08
申请号：US11346613
申请日：2006-02-02
申请人： Marian Kloza , Dieter Schmalbein , Diether Maier
发明人： Marian Kloza , Dieter Schmalbein , Diether Maier
IPC分类号： G01V3/00
CPC分类号： G01N24/08 , G01R33/30
摘要： An apparatus for determining a quantitative property of a sample substance by means of magnetic resonance is disclosed. The apparatus comprises a conveyor for conveying sample containers containing the sample substance through a measuring station. The measuring station comprises a magnet system for generating a constant magnetic field of high homogeneity. The measuring station, further, comprises a probe head adapted for letting sample containers be conveyed therethrough and for generating a high frequency magnetic field. A magnetic resonance measuring unit determines the quantitative property of the sample substance contained in the probe head. The probe head excites and detects, resp., the magnetic resonance essentially only within that section of the sample container which contains the sample substance. The probe head comprises a split-ring resonator which, as seen in a conveying direction of the conveyor, has a passage cross-section for letting run the sample containers therethrough. The high frequency magnetic field is generated essentially only in an area of the passage cross-section through which the sample containers run during conveying.
摘要翻译：公开了一种用于通过磁共振确定样品物质的定量性质的装置。该装置包括用于通过测量站传送包含样品物质的样品容器的输送机。测量站包括用于产生高均匀性的恒定磁场的磁体系统。此外，测量站还包括探头，其适于使样品容器通过其传送并产生高频磁场。磁共振测量单元确定包含在探头中的样品物质的定量性质。探针头基本上仅在包含样品物质的样品容器的该部分内激发和检测磁共振。探头包括开环谐振器，从输送机的输送方向看，该环形谐振器具有用于使样品容器通过的通道横截面。高频磁场基本上仅在样品容器在传送过程中运行的通道横截面的区域中产生。

3. 发明申请

US20060192557A1 Apparatus and probe head for determining a quantitative property of a sample substance by means of magnetic resonance 有权
标题翻译：用于通过磁共振确定样品物质的定量性质的装置和探针头
公开(公告)号：US20060192557A1
公开(公告)日：2006-08-31
申请号：US11346613
申请日：2006-02-02
申请人： Marian Kloza , Dieter Schmalbein , Diether Maier
发明人： Marian Kloza , Dieter Schmalbein , Diether Maier
IPC分类号： G01V3/00
CPC分类号： G01N24/08 , G01R33/30
摘要： An apparatus for determining a quantitative property of a sample substance by means of magnetic resonance is disclosed. The apparatus comprises a conveyor for conveying sample containers containing the sample substance through a measuring station. The measuring station comprises a magnet system for generating a constant magnetic field of high homogeneity. The measuring station, further, comprises a probe head adapted for letting sample containers be conveyed therethrough and for generating a high frequency magnetic field. A magnetic resonance measuring unit determines the quantitative property of the sample substance contained in the probe head. The probe head excites and detects, resp., the magnetic resonance essentially only within that section of the sample container which contains the sample substance. The probe head comprises a split-ring resonator which, as seen in a conveying direction of the conveyor, has a passage cross-section for letting run the sample containers therethrough. The high frequency magnetic field is generated essentially only in an area of the passage cross-section through which the sample containers run during conveying.
摘要翻译：公开了一种用于通过磁共振确定样品物质的定量性质的装置。该装置包括用于通过测量站传送包含样品物质的样品容器的输送机。测量站包括用于产生高均匀性的恒定磁场的磁体系统。此外，测量站还包括探头，其适于使样品容器通过其传送并产生高频磁场。磁共振测量单元确定包含在探头中的样品物质的定量性质。探针头基本上仅在包含样品物质的样品容器的该部分内激发和检测磁共振。探头包括开环谐振器，从输送机的输送方向看，该环形谐振器具有用于使样品容器通过的通道横截面。高频磁场基本上仅在样品容器在传送过程中运行的通道横截面的区域中产生。

4. 发明授权

US06791324B2 Probehead and a sample substance for an electron spin resonance dosimeter 有权
标题翻译：探针头和电子自旋共振剂量计的样品物质
公开(公告)号：US06791324B2
公开(公告)日：2004-09-14
申请号：US10197629
申请日：2002-07-17
申请人： Diether Maier , Dieter Schmalbein , Jin Jie Jiang , Ralph T. Weber , Andreas Kamlowski , Thomas Schmidt
发明人： Diether Maier , Dieter Schmalbein , Jin Jie Jiang , Ralph T. Weber , Andreas Kamlowski , Thomas Schmidt
IPC分类号： G01V300
CPC分类号： G01R33/28 , G01R33/30 , G01R33/443 , G01R33/60
摘要： A probehead for an electron spin resonance (ESR) dosimeter comprises a resonator and an insert extending into the resonator. The insert has a guide channel for bringing a sample into the resonator. The sample comprises a dosimeter substance. The guide channel is configured for receiving and guiding a test strip. The insert is provided with a first machine-readable code imprint. The insert is provided with at least one reference sample. A pressurized air unit is provided for blowing the sample out of the resonator after completion of a measurement. The insert has an opening on an upper side of the resonator. The opening is openly accessible for manually inserting dosimeter pills thereinto. The insert, further, is provided on the upper side with a pressurized air connector. The pressurized air connector is connected to an orifice via a pressurized air channel within the insert. The orifice is located within a lower, otherwise closed bottom of the guide channel. The sample substance comprises a chromium-doped magnesium oxide (Cr:MgO). The magnesium oxide is doped with the isotope 52Cr.
摘要翻译：用于电子自旋共振（ESR）剂量计的探头包括谐振器和延伸到谐振器中的插入件。插入件具有用于将样品带入谐振器的引导通道。样品包含剂量计物质。引导通道被配置为用于接收和引导测试条。该插入件具有第一机器可读代码印记。插入件具有至少一个参考样品。提供加压空气单元，用于在完成测量之后将样品吹出谐振器。插入件在谐振器的上侧具有开口。开口是公开的手动插入剂量计药丸。此外，插入件在上侧设置有加压空气连接器。加压空气连接器通过插入件内的加压空气通道连接到孔口。孔口位于引导通道的下部或另外封闭的底部。样品物质包含掺杂铬的氧化镁（Cr：MgO）。氧化镁掺杂有同位素<52> Cr。

5. 发明授权

US06462546B1 Method and apparatus for investigating the imperishability of liquid foodstuffs by means of electron spin resonance 有权
标题翻译：通过电子自旋共振研究液体食品的不均匀性的方法和装置
公开(公告)号：US06462546B1
公开(公告)日：2002-10-08
申请号：US09700929
申请日：2000-11-21
申请人： Dieter Schmalbein , JinJie Jiang , Arthur H. Heiss , Ralph T. Weber , Andreas Kamlowski
发明人： Dieter Schmalbein , JinJie Jiang , Arthur H. Heiss , Ralph T. Weber , Andreas Kamlowski
IPC分类号： G01V300
CPC分类号： G01R33/307 , G01R33/60
摘要： A method and an apparatus for investigating the imperishability of n liquid foodstuffs using electron spin resonance (ESR) exposes samples of the foodstuffs to an elevated temperature for an extended time-period. At predetermined intervals during the period, the intensity of an ESR signal of each sample is measured and plotted vs. time in a diagram for that sample. The time of a superproportional increase in intensity is detected for each foodstuff. The number n of different foodstuffs is determined by dividing the predetermined interval by the measurement time. The n samples are investigated simultaneously by sequentially cycling the n samples through a common sample vessel. Each time, the intensity of the ESR signal of the sample is measured and then plotted in a diagram unique to that foodstuff. The sequence of foodstuffs are cycled through the sample vessel until a predetermined number m of measuring points per foodstuff has been attained.
摘要翻译：使用电子自旋共振（ESR）研究n种液体食品不均匀性的方法和装置将食品样品暴露于升高的温度下延长时间。在该期间的预定间隔，测量每个样品的ESR信号的强度，并对该样品的图中的时间作图。每种食品都会检测到强度超比例增加的时间。通过将预定间隔除以测量时间来确定不同食物的数量n。通过将n个样品顺序循环通过普通的样品容器来同时研究n个样品。每次测量样品的ESR信号的强度，然后绘制在该食品独特的图中。食物的顺序循环通过样品容器，直到达到每个食物预定数量的测量点。

6. 发明授权

US07838298B2 Method and apparatus for determining the fat or oil content of a sample 有权
标题翻译：用于确定样品的脂肪或油含量的方法和装置
公开(公告)号：US07838298B2
公开(公告)日：2010-11-23
申请号：US11252223
申请日：2005-10-17
申请人： Andreas Kamlowski , Dieter Schmalbein , Arne Kasten
发明人： Andreas Kamlowski , Dieter Schmalbein , Arne Kasten
IPC分类号： G01N31/00 , G01N33/06 , G01N33/92 , G01V3/00
CPC分类号： G01N24/08 , G01R33/30 , G01R33/343
摘要： A method and an apparatus serve the purpose of determining the fat or oil content of a sample. The sample is dried under the action of a microwave field and is examined under the action of a radio-frequency signal and of a constant magnetic field by means of nuclear magnetic resonance. The sample is exposed to the microwave field, the radio-frequency signal and the magnetic field at the same measuring place in a common measuring chamber. The apparatus has a microwave source for drying the sample, a magnetic system for generating a nuclear magnetic resonance magnetic field in the sample, and a nuclear magnetic resonance measuring arrangement for irradiating radio-frequency signals into the sample and for receiving excited nuclear magnetic resonance signals from the sample. The microwave source, the magnetic system and the nuclear magnetic resonance measuring arrangement are connected to a common measuring chamber in which the sample is located.
摘要翻译：方法和装置用于确定样品的脂肪或油含量的目的。样品在微波场作用下干燥，并通过核磁共振在射频信号和恒定磁场的作用下进行检测。样品暴露于微波场，射频信号和在同一测量室中相同测量位置处的磁场。该装置具有用于干燥样品的微波源，用于在样品中产生核磁共振磁场的磁系统和用于将射频信号照射到样品中并用于接收激发的核磁共振信号的核磁共振测量装置从样品。微波源，磁系统和核磁共振测量装置连接到样品所在的公共测量室。

7. 发明授权

US07397241B2 Method for determining the content of at least one component of a sample by means of a nuclear magnetic resonance pulse spectrometer 有权
标题翻译：通过核磁共振脉冲光谱仪测定样品中至少一种组分的含量的方法
公开(公告)号：US07397241B2
公开(公告)日：2008-07-08
申请号：US11119413
申请日：2005-04-29
申请人： Gisela Gauthausen , Andreas Kamlowski , Dieter Schmalbein
发明人： Gisela Gauthausen , Andreas Kamlowski , Dieter Schmalbein
IPC分类号： G01V3/00
CPC分类号： G01N24/08 , G01R33/46
摘要： A method is described for determination of the content of at least one component of a sample by means of a nuclear magnetic resonance pulse spectrometer, with the magnetization of the sample being influenced by a sequence of radio-frequency pulses such that the signal amplitudes to be observed can be determined. The magnetization of the sample is initially saturated, and the signal amplitudes which are determined at each time by the longitudinal and transverse relaxation times T1 and T2 and/or T2* and/or T1p, from which a value for the content of the at least one component is determined, are measured at the same time in a cohesive experimental procedure.
摘要翻译：描述了通过核磁共振脉冲光谱仪确定样品的至少一个组分的含量的方法，其中样品的磁化受到一系列射频脉冲的影响，使得信号幅度为观察可以确定。样品的磁化最初饱和，并且每次通过纵向和横向弛豫时间T 1和T 2和/或T 2确定的信号幅度，在粘性实验过程中同时测量从其中确定至少一种组分的含量的值的第二个和第二个碱基和/或T 1p 。

8. 发明申请

US20070010021A1 Method and apparatus for determining the fat or oil content of a sample 有权
标题翻译：用于确定样品的脂肪或油含量的方法和装置
公开(公告)号：US20070010021A1
公开(公告)日：2007-01-11
申请号：US11252223
申请日：2005-10-17
申请人： Andreas Kamlowski , Dieter Schmalbein , Arne Kasten
发明人： Andreas Kamlowski , Dieter Schmalbein , Arne Kasten
IPC分类号： G01N33/92
CPC分类号： G01N24/08 , G01R33/30 , G01R33/343
摘要： A method and an apparatus serve the purpose of determining the fat or oil content of a sample. The sample is dried under the action of a microwave field and is examined under the action of a radio-frequency signal and of a constant magnetic field by means of nuclear magnetic resonance. The sample is exposed to the microwave field, the radio-frequency signal and the magnetic field at the same measuring place in a common measuring chamber. The apparatus has a microwave source for drying the sample, a magnetic system for generating a nuclear magnetic resonance magnetic field in the sample, and a nuclear magnetic resonance measuring arrangement for irradiating radio-frequency signals into the sample and for receiving excited nuclear magnetic resonance signals from the sample. The microwave source, the magnetic system and the nuclear magnetic resonance measuring arrangement are connected to a common measuring chamber in which the sample is located.
摘要翻译：方法和装置用于确定样品的脂肪或油含量的目的。样品在微波场作用下干燥，并通过核磁共振在射频信号和恒定磁场的作用下进行检测。样品暴露于微波场，射频信号和在同一测量室中相同测量位置处的磁场。该装置具有用于干燥样品的微波源，用于在样品中产生核磁共振磁场的磁系统和用于将射频信号照射到样品中并用于接收激发的核磁共振信号的核磁共振测量装置从样品。微波源，磁系统和核磁共振测量装置连接到样品所在的公共测量室。

9. 发明申请

US20050270026A1 Method for determining the content of at least one component of a sample by means of a nuclear magnetic resonance pulse spectrometer 有权
标题翻译：通过核磁共振脉冲光谱仪测定样品中至少一种组分的含量的方法
公开(公告)号：US20050270026A1
公开(公告)日：2005-12-08
申请号：US11119413
申请日：2005-04-29
申请人： Gisela Guthausen , Andreas Kamlowski , Dieter Schmalbein
发明人： Gisela Guthausen , Andreas Kamlowski , Dieter Schmalbein
IPC分类号： G01N24/08 , G01R33/46 , G01V3/00
CPC分类号： G01N24/08 , G01R33/46
摘要： A method is described for determination of the content of at least one component of a sample by means of a nuclear magnetic resonance pulse spectrometer, with the magnetization of the sample being influenced by a sequence of radio-frequency pulses such that the signal amplitudes to be observed can be determined. The magnetization of the sample is initially saturated, and the signal amplitudes which are determined at each time by the longitudinal and transverse relaxation times T1 and T2 and/or T2* and/or T1p, from which a value for the content of the at least one component is determined, are measured at the same time in a cohesive experimental procedure.
摘要翻译：描述了通过核磁共振脉冲光谱仪确定样品的至少一个组分的含量的方法，其中样品的磁化受到一系列射频脉冲的影响，使得信号幅度为观察可以确定。样品的磁化最初饱和，并且每次通过纵向和横向弛豫时间T 1和T 2和/或T 2确定的信号幅度，在粘性实验过程中同时测量从其中确定至少一种组分的含量的值的第二个和第二个碱基和/或T 1p 。

10. 发明授权

US5619139A Magnetic resonance method and apparatus for detecting an atomic structure of a sample along a surface thereof 失效
标题翻译：用于检测样品沿其表面的原子结构的磁共振方法和装置
公开(公告)号：US5619139A
公开(公告)日：1997-04-08
申请号：US393121
申请日：1995-02-21
申请人： Karoly Holczer , Dieter Schmalbein , Peter Hoefer
发明人： Karoly Holczer , Dieter Schmalbein , Peter Hoefer
IPC分类号： G01B7/34 , G01Q30/02 , G01Q60/08 , G01Q60/52 , G01R33/56 , G01R33/60 , G01R33/20
CPC分类号： G01Q60/08 , B82Y35/00 , G01Q60/52 , G01R33/60 , G01R33/5604 , Y10S977/838 , Y10S977/84 , Y10S977/863 , Y10S977/865 , Y10S977/88 , Y10S977/96
摘要： A method and an apparatus are disclosed for detecting an atomic structure of a sample along a surface thereof. The method comprises arranging the sample in a constant magnetic field (B.sub.0) of predetermined field strength and high homogeneity and irradiating a high-frequency magnetic field (B.sub.1) of a predetermined frequency on the sample, wherein the fields (B.sub.0) and (B.sub.1) are oriented perpendicularly to each other. The method further comprises providing a force-sensitive sensor having a paramagnetic tip comprising a paramagnetic material. The sensor is placed in close vicinity to the sample such that the paramagnetic tip is in atomic interaction with the sample surface which means that the distance between the tip and the surface is in the order of between 1 and 10 .ANG.. The predetermined field strength and the predetermined frequency are set such that electron paramagnetic resonance (EPR) is excited within the tip paramagnetic material. The paramagnetic tip is then displaced parallel to the sample surface for mapping predetermined points on the sample surface. During displacing the tip the force exerted on the tip by a local inhomogeneous magnetic field (B.sub.loc) caused by atomic magnetic moments (m.sub.e,k) of the sample is measured.
摘要翻译：公开了一种用于检测样品沿其表面的原子结构的方法和装置。该方法包括将样品置于具有预定场强和高均匀性的恒定磁场（B0）中，并且对样品照射预定频率的高频磁场（B1），其中场（B0）和（B1）彼此垂直取向。该方法还包括提供具有包括顺磁材料的顺磁性尖端的力敏感传感器。将传感器放置在样品附近，使得顺磁性尖端与样品表面原子相互作用，这意味着尖端和表面之间的距离在1和10埃之间。将预定的场强和预定频率设定为使得电子顺磁共振（EPR）在尖端顺磁性材料内被激发。然后顺磁性尖端平行于样品表面移位，用于映射样品表面上的预定点。在移动尖端期间，测量由样品的原子磁矩（me，k）引起的局部不均匀磁场（Bloc）施加在尖端上的力。

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