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1. 发明申请

US20120177808A1 SYSTEM AND METHOD FOR LOW-POWER NANOTUBE GROWTH USING DIRECT RESISTIVE HEATING 有权
标题翻译：使用直接电阻加热的低功率纳米生长的系统和方法
公开(公告)号：US20120177808A1
公开(公告)日：2012-07-12
申请号：US12102302
申请日：2008-04-14
申请人： DELMAR L. BARKER , Mead M. Jordan , William R. Owens
发明人： DELMAR L. BARKER , Mead M. Jordan , William R. Owens
IPC分类号： C23C16/26 , C23C16/48 , C23C16/52 , B05C11/00 , C23C16/44 , B82Y40/00
CPC分类号： C01B21/0602 , B82Y30/00 , B82Y40/00 , C01B21/064 , C01B32/16 , C01B32/956 , C01B33/02 , C01B35/023 , C01B2202/08 , C01P2004/13 , C30B11/12 , C30B25/00 , C30B29/602 , Y10S977/72 , Y10S977/721 , Y10S977/722 , Y10S977/734 , Y10S977/742 , Y10S977/743 , Y10S977/75 , Y10S977/751 , Y10S977/752 , Y10S977/813 , Y10S977/814 , Y10S977/822 , Y10T117/10 , Y10T117/1016 , Y10T117/102
摘要： Direct resistive heating is used to grow nanotubes out of carbon and other materials. A growth-initiated array of nanotubes is provided using a CVD or ion implantation process. These processes use indirect heating to heat the catalysts to initiate growth. Once growth is initiated, an electrical source is connected between the substrate and a plate above the nanotubes to source electrical current through and resistively heat the nanotubes and their catalysts. A material source supplies the heated catalysts with carbon or another material to continue growth of the array of nanotubes. Once direct heating has commenced, the source of indirect heating can be removed or at least reduced. Because direct resistive heating is more efficient than indirect heating the total power consumption is reduced significantly.
摘要翻译：直接电阻加热用于从碳和其他材料中生长纳米管。使用CVD或离子注入工艺提供了生长起始的纳米管阵列。这些方法使用间接加热来加热催化剂以引发生长。一旦生长开始，电源连接在基板和纳米管上方的板之间，以通过电流和电阻加热纳米管及其催化剂。材料源为加热的催化剂提供碳或其他材料，以继续纳米管阵列的生长。一旦直接加热开始，可以去除或至少减少间接加热的来源。由于直接电阻加热比间接加热更有效，因此总功耗显着降低。

2. 发明申请

US20120128574A1 CARBON NANOSTRUCTURE SYNTHESIS FROM CARBON-EXCESS EXPLOSIVES IN SUPERCRITICAL FLUID 有权
标题翻译：超临界流体中碳爆炸的碳纳米结构合成
公开(公告)号：US20120128574A1
公开(公告)日：2012-05-24
申请号：US12949670
申请日：2010-11-18
申请人： DELMAR L. BARKER , Mead M. Jordan , William R. Owens , John Warren Beck
发明人： DELMAR L. BARKER , Mead M. Jordan , William R. Owens , John Warren Beck
IPC分类号： D01F9/12 , C01B31/04 , B82Y30/00 , B82Y40/00
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/05 , C01B32/15 , C01B32/152 , C01B32/166 , C01B32/182 , C01B32/40 , Y02P20/544
摘要： Carbon nanostructures are synthesized from carbon-excess explosives having a negative oxygen balance. A supercritical fluid provides an environment that safely dissolves and decomposes the explosive molecules into its reactant products including activated C or CO and provides the temperature and pressure for the required collision rate of activated C atoms and CO molecules to form carbon nanostructures such as graphene, fullerenes and nanotubes. The nanostructures may be synthesized without a metal reactant at relatively low temperatures in the supercritical fluid to provide a cost-effective path to bulk fabrication. These nanostructures may be synthesized “metal free”. As the supercritical fluid provides an inert buffer that does not react with the explosive, the fluid is preserved. Once the nanostructures are removed, the other reaction products may be removed and the fluid recycled.
摘要翻译：碳纳米结构由具有负氧平衡负的碳过量炸药合成。超临界流体提供了一种安全地将爆炸分子溶解并分解成其反应物产物（包括活化的C或CO）的环境，并为活化的C原子和CO分子所需的碰撞速率提供温度和压力以形成碳纳米结构，例如石墨烯，富勒烯和纳米管。纳米结构可以在超临界流体中在相对较低的温度下合成而没有金属反应物，以提供大量制造的成本有效的途径。这些纳米结构可以合成“无金属”。当超临界流体提供不与爆炸物反应的惰性缓冲液时，流体被保留。一旦去除了纳米结构，可以除去其它反应产物，再循环流体。

3. 发明授权

US08323609B2 Carbon nanostructure synthesis from carbon-excess explosives in supercritical fluid 有权
标题翻译：超临界流体中碳过量爆炸物的碳纳米结构合成
公开(公告)号：US08323609B2
公开(公告)日：2012-12-04
申请号：US12949670
申请日：2010-11-18
申请人： Delmar L. Barker , Mead M. Jordan , William R. Owens , John Warren Beck
发明人： Delmar L. Barker , Mead M. Jordan , William R. Owens , John Warren Beck
IPC分类号： D01F9/12 , C01B31/04 , B82Y30/00 , B82Y40/00
CPC分类号： B82Y30/00 , B82Y40/00 , C01B32/05 , C01B32/15 , C01B32/152 , C01B32/166 , C01B32/182 , C01B32/40 , Y02P20/544
摘要： Carbon nanostructures are synthesized from carbon-excess explosives having a negative oxygen balance. A supercritical fluid provides an environment that safely dissolves and decomposes the explosive molecules into its reactant products including activated C or CO and provides the temperature and pressure for the required collision rate of activated C atoms and CO molecules to form carbon nanostructures such as graphene, fullerenes and nanotubes. The nanostructures may be synthesized without a metal reactant at relatively low temperatures in the supercritical fluid to provide a cost-effective path to bulk fabrication. These nanostructures may be synthesized “metal free”. As the supercritical fluid provides an inert buffer that does not react with the explosive, the fluid is preserved. Once the nanostructures are removed, the other reaction products may be removed and the fluid recycled.
摘要翻译：碳纳米结构由具有负氧平衡负的碳过量炸药合成。超临界流体提供了一种安全地将爆炸分子溶解并分解成其反应物产物（包括活化的C或CO）的环境，并为活化的C原子和CO分子所需的碰撞速率提供温度和压力以形成碳纳米结构，例如石墨烯，富勒烯和纳米管。纳米结构可以在超临界流体中在相对较低的温度下合成而没有金属反应物，以提供大量制造的成本有效的途径。这些纳米结构可以无金属合成。当超临界流体提供不与爆炸物反应的惰性缓冲液时，流体被保留。一旦去除了纳米结构，可以除去其它反应产物，再循环流体。

4. 发明授权

US08216364B1 System and method for low-power nanotube growth using direct resistive heating 有权
标题翻译：使用直接电阻加热的低功率纳米管生长的系统和方法
公开(公告)号：US08216364B1
公开(公告)日：2012-07-10
申请号：US12102302
申请日：2008-04-14
申请人： Delmar L. Barker , Mead M. Jordan , William R. Owens
发明人： Delmar L. Barker , Mead M. Jordan , William R. Owens
IPC分类号： C30B25/22
CPC分类号： C01B21/0602 , B82Y30/00 , B82Y40/00 , C01B21/064 , C01B32/16 , C01B32/956 , C01B33/02 , C01B35/023 , C01B2202/08 , C01P2004/13 , C30B11/12 , C30B25/00 , C30B29/602 , Y10S977/72 , Y10S977/721 , Y10S977/722 , Y10S977/734 , Y10S977/742 , Y10S977/743 , Y10S977/75 , Y10S977/751 , Y10S977/752 , Y10S977/813 , Y10S977/814 , Y10S977/822 , Y10T117/10 , Y10T117/1016 , Y10T117/102
摘要： Direct resistive heating is used to grow nanotubes out of carbon and other materials. A growth-initiated array of nanotubes is provided using a CVD or ion implantation process. These processes use indirect heating to heat the catalysts to initiate growth. Once growth is initiated, an electrical source is connected between the substrate and a plate above the nanotubes to source electrical current through and resistively heat the nanotubes and their catalysts. A material source supplies the heated catalysts with carbon or another material to continue growth of the array of nanotubes. Once direct heating has commenced, the source of indirect heating can be removed or at least reduced. Because direct resistive heating is more efficient than indirect heating the total power consumption is reduced significantly.
摘要翻译：直接电阻加热用于从碳和其他材料中生长纳米管。使用CVD或离子注入工艺提供了生长起始的纳米管阵列。这些方法使用间接加热来加热催化剂以引发生长。一旦生长开始，电源连接在基板和纳米管上方的板之间，以通过电流和电阻加热纳米管及其催化剂。材料源为加热的催化剂提供碳或其他材料，以继续纳米管阵列的生长。一旦直接加热开始，可以去除或至少减少间接加热的来源。由于直接电阻加热比间接加热更有效，因此总功耗显着降低。

5. 发明授权

US07837905B2 Method of making reinforced filament with doubly-embedded nanotubes 有权
标题翻译：双层纳米管加强丝的制备方法
公开(公告)号：US07837905B2
公开(公告)日：2010-11-23
申请号：US12121985
申请日：2008-05-16
申请人： Delmar L. Barker , Mead M. Jordan , W. Howard Poisl
发明人： Delmar L. Barker , Mead M. Jordan , W. Howard Poisl
IPC分类号： D01D5/12 , D01F1/10 , D01F9/22
CPC分类号： B82Y30/00 , D01F1/10 , D01F9/20 , Y10T428/2918
摘要： Strengthened filaments and fibers are realized by mixing and dissolving monomer and catalyst in a solvent into open-ended nanotubes to form a polymer precursor prior to polymerization in which the open nanotubes are filled with monomer and catalyst. The remaining steps for forming a stabilized filament may follow the conventional sequence. The result is that the nanotubes are “doubly-embedded” in the polymer matrix (bonds to the polymer inside and extending through the nanotube and bonds to other polymer chains outside the nanotube) in the filament. These additional bonds provide additional mechanical strength. The number of bonds may be further enhanced by pretreating the nanotubes to create defects in the nanotubes to form sites along the inner and outer walls for additional polymer-to-nanotube bonds. The aligned filaments may be radiated to create additional polymer-to-nanotube bonds such as between the polymer chain inside the nanotube and the inner walls of the nanotube and to create nanotube-to-nanotube bonds. In the case of carbon fiber, the carbonized filament may be radiated to create additional carbon-carbon bonds prior to twisting the filaments into the fiber.
摘要翻译：通过将单体和催化剂在溶剂中混合并溶解到开放式纳米管中以在聚合之前形成聚合物前体，其中开放纳米管填充有单体和催化剂来实现加强的长丝和纤维。用于形成稳定的丝的其余步骤可以遵循常规顺序。结果是纳米管被“双嵌入”在聚合物基质中（与内部聚合物结合并延伸穿过纳米管并与纳米管外部的其它聚合物链结合）。这些附加键提供额外的机械强度。可以通过预处理纳米管以在纳米管中产生缺陷以形成沿着内壁和外壁的位点用于另外的聚合物 - 纳米管键来进一步增强键的数量。可以辐射对准的长丝以产生另外的聚合物 - 纳米管结合，例如在纳米管内部的聚合物链和纳米管的内壁之间，并产生纳米管与纳米管的键。在碳纤维的情况下，碳化细丝可以在将细丝扭曲成纤维之前被辐射以产生额外的碳 - 碳键。

6. 发明授权

US07883580B2 System and method for nanotube growth via Ion implantation using a catalytic transmembrane 有权
标题翻译：使用催化跨膜通过离子注入的纳米管生长的系统和方法
公开(公告)号：US07883580B2
公开(公告)日：2011-02-08
申请号：US12061317
申请日：2008-04-02
申请人： Delmar L. Barker , Mead M. Jordan , W. Howard Poisl
发明人： Delmar L. Barker , Mead M. Jordan , W. Howard Poisl
IPC分类号： C23C16/00 , C23C16/448
CPC分类号： C01B35/02 , C01B21/064 , C01B32/05 , C01B32/956 , C01B33/02 , Y10S977/844
摘要： Ion implantation is used to grow nanotubes out of carbon and other materials. Catalytic material is placed on or in a membrane that physically and possibly environmentally separates an implantation chamber or region from a growth chamber or region. High-energy ions are implanted into the catalytic material from one side to grow nanotubes on an exposed surface in the growth chamber. Ion implantation via the membrane provides for greater flexibility to separate and independently control the implantation and growth processes.
摘要翻译：离子注入用于从碳和其他材料中生长纳米管。将催化材料放置在膜上或膜上，物理上和可能地将植入室或区域与生长室或区域环境分离。高能离子从一侧注入到催化材料中，以在生长室的暴露表面上生长纳米管。通过膜的离子注入提供了更大的灵活性来分离和独立地控制植入和生长过程。

7. 发明申请

US20090286079A1 REINFORCED FILAMENT WITH DOUBLY-EMBEDDED NANOTUBES AND METHOD OF MANUFACTURE 有权
标题翻译：具有双嵌段纳米管的增强型薄膜及其制造方法
公开(公告)号：US20090286079A1
公开(公告)日：2009-11-19
申请号：US12121985
申请日：2008-05-16
申请人： Delmar L. Barker , Mead M. Jordan , W. Howard Poisl
发明人： Delmar L. Barker , Mead M. Jordan , W. Howard Poisl
IPC分类号： C08K3/04 , B32B1/00
CPC分类号： B82Y30/00 , D01F1/10 , D01F9/20 , Y10T428/2918
摘要： Strengthened filaments and fibers are realized by mixing and dissolving monomer and catalyst in a solvent into open-ended nanotubes to form a polymer precursor prior to polymerization in which the open nanotubes are filled with monomer and catalyst. The remaining steps for forming a stabilized filament may follow the conventional sequence. The result is that the nanotubes are “doubly-embedded” in the polymer matrix (bonds to the polymer inside and extending through the nanotube and bonds to other polymer chains outside the nanotube) in the filament. These additional bonds provide additional mechanical strength. The number of bonds may be further enhanced by pretreating the nanotubes to create defects in the nanotubes to form sites along the inner and outer walls for additional polymer-to-nanotube bonds. The aligned filaments may be radiated to create additional polymer-to-nanotube bonds such as between the polymer chain inside the nanotube and the inner walls of the nanotube and to create nanotube-to-nanotube bonds. In the case of carbon fiber, the carbonized filament may be radiated to create additional carbon-carbon bonds prior to twisting the filaments into the fiber.
摘要翻译：通过将单体和催化剂在溶剂中混合并溶解到开放式纳米管中以在聚合之前形成聚合物前体，其中开放纳米管填充有单体和催化剂来实现加强的长丝和纤维。用于形成稳定的丝的其余步骤可以遵循常规顺序。结果是纳米管被“双嵌入”在聚合物基质中（与内部聚合物结合并延伸穿过纳米管并与纳米管外部的其它聚合物链结合）。这些附加键提供额外的机械强度。可以通过预处理纳米管以在纳米管中产生缺陷以形成沿着内壁和外壁的位点用于另外的聚合物 - 纳米管键来进一步增强键的数量。可以辐射对准的长丝以产生另外的聚合物 - 纳米管结合，例如在纳米管内的聚合物链和纳米管的内壁之间，并产生纳米管与纳米管的键。在碳纤维的情况下，碳化细丝可以在将细丝扭曲成纤维之前被辐射以产生额外的碳 - 碳键。

8. 发明申请

US20090252886A1 SYSTEM AND METHOD FOR NANOTUBE GROWTH VIA ION IMPLANTATION USING A CATALYTIC TRANSMEMBRANE 有权
标题翻译：通过催化转移膜进行离子植入的纳米生长体系及方法
公开(公告)号：US20090252886A1
公开(公告)日：2009-10-08
申请号：US12061317
申请日：2008-04-02
申请人： DELMAR L. BARKER , Mead M. Jordan , W. Howard Poisl
发明人： DELMAR L. BARKER , Mead M. Jordan , W. Howard Poisl
IPC分类号： C23C14/48 , H01J37/08
CPC分类号： C01B35/02 , C01B21/064 , C01B32/05 , C01B32/956 , C01B33/02 , Y10S977/844
摘要： Ion implantation is used to grow nanotubes out of carbon and other materials. Catalytic material is placed on or in a membrane that physically and possibly environmentally separates an implantation chamber or region from a growth chamber or region. High-energy ions are implanted into the catalytic material from one side to grow nanotobes on an exposed surface in the growth chamber. Ion implantation via the membrane provides for greater flexibility to separate and independently control the implantation and growth processes.
摘要翻译：离子注入用于从碳和其他材料中生长纳米管。将催化材料放置在膜上或膜上，物理上和可能地将植入室或区域与生长室或区域环境分离。将高能离子从一侧注入到催化材料中，以在生长室的暴露表面上生长纳米体。通过膜的离子注入提供了更大的灵活性来分离和独立地控制植入和生长过程。

9. 发明授权

US08669460B2 System and methods for optimal light collection array 有权
标题翻译：最佳光采集系统和方法
公开(公告)号：US08669460B2
公开(公告)日：2014-03-11
申请号：US12116902
申请日：2008-05-07
申请人： Mead M. Jordan , David G. Jenkins , Devon G. Crowe
发明人： Mead M. Jordan , David G. Jenkins , Devon G. Crowe
IPC分类号： H02N6/00 , H01L31/042
CPC分类号： H01L27/1446 , H01L31/0547 , Y02E10/52
摘要： Apparatus and methods according to various aspects of the present invention may operate in conjunction with a light collection array. One or more light redirectors located at or near inactive areas of light collection arrays may redirect incident light to active areas. In one embodiment, the light redirector may be implemented with additional light redirectors and/or a concentrating photovoltaic collection system.
摘要翻译：根据本发明的各个方面的装置和方法可以与光收集阵列结合操作。位于光收集阵列的非活动区域或附近的一个或多个光重定向器可以将入射光重定向到有源区域。在一个实施例中，光重定向器可以用附加的光重定向器和/或聚光光伏收集系统来实现。

10. 发明申请

US20080276982A1 SYSTEM AND METHODS FOR OPTIMAL LIGHT COLLECTION ARRAY 有权
标题翻译：用于最佳光收集阵列的系统和方法
公开(公告)号：US20080276982A1
公开(公告)日：2008-11-13
申请号：US12116902
申请日：2008-05-07
申请人： Mead M. Jordan , David G. Jenkins , Devon G. Crowe
发明人： Mead M. Jordan , David G. Jenkins , Devon G. Crowe
IPC分类号： H01L31/042
CPC分类号： H01L27/1446 , H01L31/0547 , Y02E10/52
摘要： Apparatus and methods according to various aspects of the present invention may operate in conjunction with a light collection array. One or more light redirectors located at or near inactive areas of light collection arrays may redirect incident light to active areas. In one embodiment, the light redirector may be implemented with additional light redirectors and/or a concentrating photovoltaic collection system.
摘要翻译：根据本发明的各个方面的装置和方法可以与光收集阵列结合操作。位于光收集阵列的非活动区域或附近的一个或多个光重定向器可以将入射光重定向到有源区域。在一个实施例中，光重定向器可以用附加的光重定向器和/或聚光光伏收集系统来实现。

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