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1. 发明申请

US20050029194A1 Method for removal of guanidine compound from aqueous media 审中-公开
标题翻译：从水性介质中除去胍化合物的方法
公开(公告)号：US20050029194A1
公开(公告)日：2005-02-10
申请号：US10743239
申请日：2003-12-22
申请人： David Hall , Thomas Guggenheim , James Silva , Farid Khouri , Matthew Littlejohn , Balakrishnan Ganesan , Ashok Shyadligeri , Pradeep Nadkarni
发明人： David Hall , Thomas Guggenheim , James Silva , Farid Khouri , Matthew Littlejohn , Balakrishnan Ganesan , Ashok Shyadligeri , Pradeep Nadkarni
IPC分类号： B01D15/08 , B01D61/00 , B01D61/02 , B01D61/14 , C07C277/06
CPC分类号： C02F9/00 , B01D61/027 , C02F1/281 , C02F1/283 , C02F1/44 , C02F2101/38 , C07C277/06 , C07C279/04
摘要： Disclosed is a method for removing a neutral or an ionic guanidine compound from an aqueous media optionally comprising an alkali metal halide, wherein the method is selected from the group consisting of (a) adsorption onto a carbonaceous adsorbent, (b) adsorption onto a clay adsorbent, (c) filtration through a nanofiltration membrane, and (d) removal of water and calcination.
摘要翻译：公开了一种从任选地包含碱金属卤化物的水性介质中除去中性或离子胍化合物的方法，其中所述方法选自（a）吸附到碳质吸附剂上，（b）吸附到粘土上吸附剂，（c）通过纳滤膜过滤，和（d）去除水和煅烧。

2. 发明申请

US20070161821A1 METHOD FOR REMOVAL OF GUANIDINE COMPOUND FROM AQUEOUS MEDIA 失效
标题翻译：从水性介质中去除胍基化合物的方法
公开(公告)号：US20070161821A1
公开(公告)日：2007-07-12
申请号：US11684882
申请日：2007-03-12
申请人： David Hall , Thomas Guggenheim , James Silva , Farid Khouri , Matthew Littlejohn , Balakrishnan Ganesan , Ashok Shyadligeri , Pradeep Nadkarni
发明人： David Hall , Thomas Guggenheim , James Silva , Farid Khouri , Matthew Littlejohn , Balakrishnan Ganesan , Ashok Shyadligeri , Pradeep Nadkarni
IPC分类号： C07C277/06
CPC分类号： C02F9/00 , B01D61/027 , C02F1/281 , C02F1/283 , C02F1/44 , C02F2101/38 , C07C277/06 , C07C279/04
摘要： Disclosed is a method for removing a neutral or an ionic guanidine compound from aqueous media optionally comprising an alkali metal halide, wherein the method is selected from the group consisting of (a) adsorption onto a carbonaceous adsorbent, (b) adsorption onto a clay adsorbent, (c) filtration through a nanofiltration membrane, and (d) removal of water and calcination.
摘要翻译：公开了一种从任选地包含碱金属卤化物的水性介质中除去中性或离子胍化合物的方法，其中所述方法选自（a）吸附到含碳吸附剂上，（b）吸附到粘土吸附剂上，（c）通过纳滤膜过滤，和（d）去除水和煅烧。

3. 发明申请

US20050049439A1 Method for making salts hydroxy-substituted hydrocarbons 有权
标题翻译：盐的制备方法羟基取代的烃
公开(公告)号：US20050049439A1
公开(公告)日：2005-03-03
申请号：US10647890
申请日：2003-08-25
申请人： Thomas Guggenheim , Daniel Brunelle , David Woodruff , Lee Bergman , Norman Johnson , Matthew Littlejohn , Farid Khouri
发明人： Thomas Guggenheim , Daniel Brunelle , David Woodruff , Lee Bergman , Norman Johnson , Matthew Littlejohn , Farid Khouri
IPC分类号： C07C29/70 , C07F1/02
CPC分类号： C07C37/70 , C07C37/66 , C07C39/235
摘要： Disclosed is a method for preparing an alkali metal salt of a hydroxy-substituted hydrocarbon which comprises the steps of (i) contacting in solvent media at least one hydroxy-substituted hydrocarbon with a base comprising an alkali metal cation; and (ii) devolatilizing the solvent media comprising alkali metal salt by adding or spraying the solvent media into a substantially water-immiscible organic solvent, said solvent being at a temperature greater than the boiling point of solvent media at the prevailing pressure. In one embodiment the solvent media comprises water, and optionally at least one water-soluble protic organic solvent.
摘要翻译：公开了一种制备羟基取代烃的碱金属盐的方法，其包括以下步骤：（i）在溶剂介质中使至少一种羟基取代的烃与包含碱金属阳离子的碱接触; 和（ii）通过将溶剂介质加入或喷雾到基本上与水不混溶的有机溶剂中来使包含碱金属盐的溶剂介质脱挥发分，所述溶剂的温度大于溶剂介质在当前压力下的沸点。在一个实施方案中，溶剂介质包含水和任选的至少一种水溶性质子有机溶剂。

4. 发明申请

US20060135741A1 Method to prepare bis(haloimides) 有权
标题翻译：制备双（卤代酰亚胺）的方法
公开(公告)号：US20060135741A1
公开(公告)日：2006-06-22
申请号：US11022907
申请日：2004-12-22
申请人： John Gui , Farid Khouri , Norman Johnson , Thomas Guggenheim , David Woodruff , James Silva
发明人： John Gui , Farid Khouri , Norman Johnson , Thomas Guggenheim , David Woodruff , James Silva
IPC分类号： C08G69/08
CPC分类号： C07D209/48 , C08G73/12
摘要： Bis(halophthalimides) are prepared in mixture in an organic liquid such as ortho-dichlorobenzene or anisole, by a reaction at a temperatire of at least 150° C. between at least one diamine compound and at least one halophthalic anhydride in the presence of imidization catalyst. The reaction mixture is maintained at about 15% by weight solids content and rich in the halophthalic anhydride by constantly monitoring the reaction mixture using analytical methods such as high performance liquid chromatography. The product mixture may be directly employed in the direct preparation of polyetherimides, and similar slurries may be employed to prepare other polyether polymers.
摘要翻译：通过在亚胺化存在下，在至少一种二胺化合物和至少一种卤代邻苯二甲酸酐之间的至少150℃的温度下进行反应，在邻二氯苯或苯甲醚的有机液体中混合制备双（卤代邻苯二酰亚胺）催化剂。通过使用诸如高效液相色谱法的分析方法不断监测反应混合物，将反应混合物保持在约15重量％的固体含量并富含卤代邻苯二甲酸酐。产物混合物可以直接用于直接制备聚醚酰亚胺，并且可以使用类似的浆料来制备其它聚醚聚合物。

5. 发明申请

US20060066004A1 Method for controlling haze in an article comprising a polymer composition 有权
公开(公告)号：US20060066004A1
公开(公告)日：2006-03-30
申请号：US10955740
申请日：2004-09-30
申请人： William Richards , Farid Khouri , Thomas Guggenheim
发明人： William Richards , Farid Khouri , Thomas Guggenheim
IPC分类号： B29C47/00
CPC分类号： C08G73/10 , C08L79/00 , C08L79/08
摘要： A method for controlling haze in an article comprising a polymer composition, said method comprising providing a polymer composition comprising less than 25 parts per million alkali metal halide; and fabricating an article from said polymer composition.

6. 发明申请

US20060173158A1 Phase transfer catalyzed method for preparation of polyetherimides 有权
标题翻译：相转移催化聚醚酰亚胺的制备方法
公开(公告)号：US20060173158A1
公开(公告)日：2006-08-03
申请号：US11363681
申请日：2006-02-28
申请人： Daniel Brunelle , Havva Acar , Farid Khouri , Thomas Guggenheim , David Woodruff , Norman Johnson
发明人： Daniel Brunelle , Havva Acar , Farid Khouri , Thomas Guggenheim , David Woodruff , Norman Johnson
IPC分类号： C08G8/02 , C08G75/00 , C07D401/00
CPC分类号： C08G73/12 , C08G73/121 , C08G73/124
摘要： Polyether polymers, such as polyetherimides, are prepared by the reaction of a dihydroxy-substituted aromatic hydrocarbon alkali metal salt, such as bisphenol A disodium salt, with a bis(N-(chlorophthalimido))aromatic compound, such as 1,3- and/or 1,4-bis(N-(4-chlorophthalimido))benzene, in a solvent such as o-dichlorobenzene and in the presence of a phase transfer catalyst such as a hexaalkylguanidinium chloride. Several embodiments may be employed to improve the method. They comprise employing substantially dry reagents, employing a high solids level in solvent, beginning with an excess of bis(N-(chlorophthalimido))-aromatic compound and incrementally adding alkali metal salt, employing alkali metal salt of small particle size, and using reagents of high purity.
摘要翻译：聚醚聚合物如聚醚酰亚胺通过二羟基取代的芳族烃碱金属盐如双酚A二钠盐与双（N-（氯代邻苯二甲酰亚胺基））芳族化合物如1,3-和 /或1,4-双（N-（4-氯邻苯二甲酰亚氨基））苯，在溶剂如邻二氯苯中，并在相转移催化剂如六烷基氯化the存在下进行。可以采用几个实施例来改进该方法。它们包括使用基本上干的试剂，在溶剂中使用高固体含量，从过量的双（N-（氯代邻苯二甲酰亚胺基）） - 芳族化合物开始，并逐渐加入碱金属盐，使用小粒径的碱金属盐，并使用试剂的高纯度。

7. 发明申请

US20050049390A1 Phase transfer catalyzed method for preparation of polyetherimides 审中-公开
标题翻译：相转移催化聚醚酰亚胺的制备方法
公开(公告)号：US20050049390A1
公开(公告)日：2005-03-03
申请号：US10647889
申请日：2003-08-25
申请人： Daniel Brunelle , Hava Acar , Farid Khouri , Thomas Guggenheim , David Woodruff , Norman Johnson
发明人： Daniel Brunelle , Hava Acar , Farid Khouri , Thomas Guggenheim , David Woodruff , Norman Johnson
IPC分类号： C08G73/12 , C08G8/02 , C08G14/00
CPC分类号： C08G73/124 , C08G73/121
摘要： Polyether polymers, such as polyetherimides, are prepared by the reaction of a dihydroxy-substituted aromatic hydrocarbon alkali metal salt, such as bisphenol A disodium salt, with a bis(N-(chlorophthalimido))aromatic compound, such as 1,3- and/or 1,4-bis[N-(4-chlorophthalimido)]benzene, in a solvent such as o-dichlorobenzene and in the presence of a phase transfer catalyst such as a hexaalkylguanidinium chloride. Several embodiments may be employed to improve the method. They comprise employing substantially dry reagents, employing a high solids level in solvent, beginning with an excess of bis(N-(chlorophthalimido))-aromatic compound and incrementally adding alkali metal salt, employing alkali metal salt of small particle size, and using reagents of high purity.
摘要翻译：聚醚聚合物如聚醚酰亚胺通过二羟基取代的芳族烃碱金属盐如双酚A二钠盐与双（N-（氯代邻苯二甲酰亚胺基））芳族化合物如1,3-和 /或1,4-双[N-（4-氯邻苯二甲酰亚氨基）]苯，在溶剂如邻二氯苯中，并在相转移催化剂如六烷基氯化the的存在下进行。可以采用几个实施例来改进该方法。它们包括使用基本上干的试剂，在溶剂中使用高固体含量，从过量的双（N-（氯代邻苯二甲酰亚胺基）） - 芳族化合物开始，并逐渐加入碱金属盐，使用小粒径的碱金属盐，并使用试剂的高纯度。

8. 发明申请

US20060167210A1 Method for producing polyether polymers 有权
标题翻译：聚醚聚合物的制备方法
公开(公告)号：US20060167210A1
公开(公告)日：2006-07-27
申请号：US11044942
申请日：2005-01-27
申请人： Thomas Guggenheim , Norman Johnson , Ganesh Kailasam , Pradeep Nadkarni , David Woodruff
发明人： Thomas Guggenheim , Norman Johnson , Ganesh Kailasam , Pradeep Nadkarni , David Woodruff
IPC分类号： C08G73/00
CPC分类号： C08G65/4093
摘要： A method of making a polyether polymer comprises reacting a salt of a dihydroxy-substituted aromatic hydrocarbon with a substituted aromatic compound of formula (I) Z(A1-X1)2 (I) in the presence of a catalyst to form an intermediate polymer having endgroups, wherein the molar ratio of the salt of a dihydroxy-substituted aromatic hydrocarbon to the substituted aromatic compound is less than 1, Z is an activating radical, A1 is an aromatic radical and X1 is fluoro, chloro, bromo or nitro; determining the additional amount of the salt of a dihydroxy-substituted aromatic hydrocarbon needed to form a final polyether polymer with a predetermined molecular weight and adding the additional amount of the salt of a dihydroxy-substituted aromatic hydrocarbon to the intermediate polymer.
摘要翻译：一种制备聚醚聚合物的方法包括使二羟基取代的芳族烃的盐与式（I）的取代的芳族化合物反应<？在线公式描述=“在线式”end =“lead”→> Z（A 1 - 1 - 1）2 2（I）<？in-line-formula description =“In-line Formulas”end = 在催化剂存在下形成具有端基的中间体聚合物，其中二羟基取代的芳族烃与取代的芳族化合物的盐的摩尔比小于1，Z是活化基团，A 1是一个芳基，X 1是氟，氯，溴或硝基; 确定形成具有预定分子量的最终聚醚聚合物所需的二羟基取代的芳烃的盐的额外量，并向中间体聚合物中加入额外量的二羟基取代的芳族烃的盐。

9. 发明申请

US20060224024A1 Method for preparation of salts of hydroxy-substituted aromatic compounds 有权
标题翻译：羟基取代芳族化合物的盐的制备方法
公开(公告)号：US20060224024A1
公开(公告)日：2006-10-05
申请号：US11095200
申请日：2005-03-30
申请人： James Silva , Thomas Guggenheim , David Woodruff
发明人： James Silva , Thomas Guggenheim , David Woodruff
IPC分类号： C07F1/02 , C07C39/16 , C07C39/12
CPC分类号： C07C37/66 , C07C39/235
摘要： A method for preparing a metal salt of a hydroxy-substituted aromatic compound is described. The method comprises contacting in an aqueous medium at least one hydroxy-substituted aromatic compound with a base comprising a metal cation to provide a mixture comprising water and a metal salt of said hydroxy-substituted aromatic compound. The aqueous metal salt is then contacted with a substantially water-immiscible solvent at a temperature greater than the boiling point of water at the prevailing pressure to provide a slurry comprising the metal salt of the hydroxy-substituted aromatic compound and a vapor stream comprising the water-immiscible solvent and water. The components of the vapor stream are separated using a vapor handling system comprising a partial reflux condenser to provide a water-rich component and a water immiscible solvent-rich component.
摘要翻译：描述了制备羟基取代的芳族化合物的金属盐的方法。该方法包括在含水介质中使至少一种羟基取代的芳族化合物与包含金属阳离子的碱接触以提供包含水和所述羟基取代的芳族化合物的金属盐的混合物。然后在主要压力下，在大于沸点的温度下，将水性金属盐与基本上与水不混溶的溶剂接触，以提供包含羟基取代的芳族化合物的金属盐和包含水的蒸汽流的浆料可混溶的溶剂和水。使用包含部分回流冷凝器的蒸汽处理系统分离蒸气流的组分以提供富含水的组分和与水不混溶的富含溶剂的组分。

10. 发明授权

US08729214B2 Mixtures resulting from methods for purification of polyether polymers 有权
标题翻译：由聚醚聚合物纯化方法得到的混合物
公开(公告)号：US08729214B2
公开(公告)日：2014-05-20
申请号：US13759083
申请日：2013-02-05
申请人： Beatriz Penalver Bernabe , Thomas Guggenheim , David Bruce Hall , Norman Johnson , Juan Justino Rodriguez Ordonez , David Woodruff
发明人： Beatriz Penalver Bernabe , Thomas Guggenheim , David Bruce Hall , Norman Johnson , Juan Justino Rodriguez Ordonez , David Woodruff
IPC分类号： C08G8/02
CPC分类号： C08K5/03 , C08G65/4093 , C08G73/1046 , C08G75/23 , C08K5/06 , C08L79/08
摘要： A method for the purification of aromatic polyether polymers prepared by a halide displacement polymerization process comprises adsorbing the catalyst with an alkali metal halide to form an adsorbent component and then removing the adsorbent component. Mixtures resulting from this method are also discussed.
摘要翻译：通过卤化物置换聚合方法制备的芳族聚醚聚合物的纯化方法包括用碱金属卤化物吸附催化剂以形成吸附剂组分，然后除去吸附剂组分。还讨论了由该方法产生的混合物。

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