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1. 发明授权

US07700668B2 Adhesive composition with decreased polarity upon polymerization 有权
标题翻译：聚合时极性降低的粘合剂组合物
公开(公告)号：US07700668B2
公开(公告)日：2010-04-20
申请号：US10564101
申请日：2004-07-14
申请人： Christoph Thalacker , Reinhold Hecht , Gioacchino Raia , Manfred Ludsteck , Karsten Dede
发明人： Christoph Thalacker , Reinhold Hecht , Gioacchino Raia , Manfred Ludsteck , Karsten Dede
IPC分类号： A61K6/083
CPC分类号： A61K6/0061 , A61K6/0073 , A61K6/0017 , C08L33/10
摘要： The invention relates to adhesive compositions that exhibit a significant decrease in polarity upon polymerization. More specifically, it relates to curable self etching dental adhesive compositions that can be applied to the tooth hard substance in one step and exhibit this decrease in polarity upon curing. In this respect a formulation is provided combining phosphoric acid esters bearing substituents with one ethylenically unsaturated moiety on the phosphorus atom and phosphoric acid esters bearing substituents with two or more ethylenically unsaturated moieties on the phosphorus atom.
摘要翻译：本发明涉及在聚合时显示极性显着降低的粘合剂组合物。更具体地，涉及可以一步施加到牙齿硬质物质的可固化自蚀牙牙胶粘剂组合物，并且在固化时表现出极性的降低。在这方面，提供了在磷原子上带有一个具有取代基的磷酸酯与一个烯属不饱和部分的磷酸酯和在磷原子上带有两个或更多个烯属不饱和部分的具有取代基的磷酸酯的配方。

2. 发明申请

US20060270751A1 Adhesive composition with decreased polarity upon polymerization 有权
标题翻译：聚合时极性降低的粘合剂组合物
公开(公告)号：US20060270751A1
公开(公告)日：2006-11-30
申请号：US10564101
申请日：2004-07-14
申请人： Christoph Thalacker , Reinhold Hecht , Gioacchino Raia , Manfred Ludsteck , Karsten Dede
发明人： Christoph Thalacker , Reinhold Hecht , Gioacchino Raia , Manfred Ludsteck , Karsten Dede
IPC分类号： A61K6/08
CPC分类号： A61K6/0061 , A61K6/0073 , A61K6/0017 , C08L33/10
摘要： The invention relates to adhesive compositions that exhibit a significant decrease in polarity upon polymerization. More specifically, it relates to curable self etching dental adhesive compositions that can be applied to the tooth hard substance in one step and exhibit this decrease in polarity upon curing. In this respect a formulation is provided combining phosphoric acid esters bearing substituents with one ethylenically unsaturated moiety on the phosphorus atom and phosphoric acid esters bearing substituents with two or more ethylenically unsaturated moieties on the phosphorus atom.
摘要翻译：本发明涉及在聚合时显示极性显着降低的粘合剂组合物。更具体地，涉及可以一步施加到牙齿硬质物质的可固化自蚀牙牙胶粘剂组合物，并且在固化时表现出极性的降低。在这方面，提供了在磷原子上带有一个具有取代基的磷酸酯与一个烯属不饱和部分的磷酸酯和在磷原子上带有两个或更多个烯属不饱和部分的具有取代基的磷酸酯的配方。

3. 发明申请

US20130109777A1 DENTAL COMPOSITION, KIT OF PARTS AND USE THEREOF 有权
标题翻译：牙齿组合物，零件套件及其用途
公开(公告)号：US20130109777A1
公开(公告)日：2013-05-02
申请号：US13807553
申请日：2011-06-24
申请人： Adrian S. Eckert , Michael M. Cub , Bettina Hailand , Marion B. Kestel , Karsten Dede , Uwe H. Hoheisel , Gioacchino Raia , Christoph Thalacker , Reinhold Hecht , Thomas Luchterhandt , Peter Bissinger , Wolf Steiger
发明人： Adrian S. Eckert , Michael M. Cub , Bettina Hailand , Marion B. Kestel , Karsten Dede , Uwe H. Hoheisel , Gioacchino Raia , Christoph Thalacker , Reinhold Hecht , Thomas Luchterhandt , Peter Bissinger , Wolf Steiger
IPC分类号： A61K6/083
CPC分类号： A61K6/083 , A61K6/0023 , A61K6/09 , C07C271/16 , C07C2603/64 , C07C2603/66 , C08L33/00 , C08L75/16
摘要： The invention relates to a dental composition comprising a) a compound (A) with the following features: only one backbone unit (U) with 6 to 20 carbon atoms, at least 6 carbon atoms thereof forming an aromatic or an aliphatic cyclic moiety, the remaining carbon atoms either being part of substituents pending from the cyclic moiety or being part of bridging groups to spacer units, wherein one or more of the remaining carbon atoms can be replaced by an oxygen atom, the backbone unit not comprising a bisphenol structure and halogen atoms, one or two unit(s) (S) being connected to the backbone unit (U) via an ether linkage, at least one unit (S) comprising a —CH2-CH2-CH2-CH2-O—CH2-CH(Q)-OG moiety or a —CH2-CH(OG)-CH2-OM moiety or a mixture of these two types of moieties within one unit (S), with G comprising at least one polymerizable moiety and an urethane moiety, the urethane moiety acting as connecting element to unit(s) (S), and M comprising at least one group selected from acroyl, methacroyl, aryl, mixtures and combinations thereof, Q comprising at least one group selected from hydrogen, methyl, phenyl, phenoxymethyl, mixtures and combinations thereof, and with the proviso that onto the backbone unit (U) at least two substituents are attached, each bearing at least one group G, wherein in the case where only one unit (S) is present, the group G not being part of said unit (S) is located in the further substituent pending from unit (U), b) a filler (B) and c) an initiator (C).
摘要翻译：本发明涉及牙科用组合物，其包含a）具有以下特征的化合物（A）：只有一个具有6至20个碳原子的骨架单元（U），其至少6个碳原子形成芳族或脂族环状部分，剩余的碳原子是作为从环状部分悬挂的取代基的一部分或作为间隔基单元的桥连基团的一部分，其中一个或多个剩余的碳原子可被氧原子代替，所述主链单元不包含双酚结构和卤素原子，一个或两个单元（S）经由醚键连接至主体单元（U），至少一个包含-CH 2 -CH 2 -CH 2 -CH 2 -O-CH 2 -CH（CH 3） Q）-OG部分或-CH2-CH（OG）-CH2-OM部分或这些两种类型的部分在一个单位（S）内的混合物，其中G包含至少一个可聚合部分和氨基甲酸酯部分，氨基甲酸酯用作单元（S）的连接元件的部分，和M包含至少一个选自丙酰基，甲基的基团包括至少一个选自氢，甲基，苯基，苯氧基甲基，其混合物和组合的基团，并且条件是在主链单元（U）上连接至少两个取代基，每个具有至少一个基团G，其中在仅存在一个单元（S）的情况下，不是所述单元（S）的一部分的基团G位于从单元（U）悬挂的另外的取代基中，b）填料（B）和c）引发剂（C）。

4. 发明授权

US09295617B2 Dental composition, method of producing and use thereof 有权
标题翻译：牙科组合物，其制造方法和使用方法
公开(公告)号：US09295617B2
公开(公告)日：2016-03-29
申请号：US13997697
申请日：2012-01-12
申请人： Adrian S. Eckert , Michael M. Cub , Bettina Hailand , Marion B. Kestel , Karsten Dede , Uwe H. Hoheisel , Gioacchino Raia , Christoph Thalacker , Reinhold Hecht , Thomas Luchterhandt
发明人： Adrian S. Eckert , Michael M. Cub , Bettina Hailand , Marion B. Kestel , Karsten Dede , Uwe H. Hoheisel , Gioacchino Raia , Christoph Thalacker , Reinhold Hecht , Thomas Luchterhandt
IPC分类号： A61K6/00 , A61K6/083
CPC分类号： A61K6/083 , A61K6/00 , A61K6/0002 , A61K6/0005 , A61K6/0017
摘要： The invention relates to a dental composition havinga) compound (A) with the following features:only one backbone unit (U) with 6 to 20 carbon atoms, at least 6 carbon atoms thereof forming an aromatic or an aliphatic cyclic moiety, the remaining carbon atoms either being part of substituents pending from the cyclic moiety or being part of bridging groups to spacer units, wherein one or more of the remaining carbon atoms can be replaced by an oxygen atom, the backbone unit not comprising a bisphenol structure, one or two spacer unit(s) (S) being connected to the backbone unit (U) via an ether linkage, at least one spacer unit (S) having a —CH2-CH2-CH2-CH2-O-CH2-CH(Q)-OG chain or a —CH2-CH(OG)-CH2-OM residue or a mixture of these two types of spacers within one spacer unit, with G having at least one group selected from acroyl, methacroyl, acetyl, benzoyl, and combinations thereof, M having at least one aryl group, and combinations thereof, Q having at least one group selected from hydrogen, methyl, phenyl, phenoxymethyl, and combinations thereof, b) filler (B) and c) initiator (C).
摘要翻译：本发明涉及具有以下特征的具有a）化合物（A）的牙科用组合物：只有一个具有6至20个碳原子的骨架单元（U），其至少6个碳原子形成芳族或脂族环状部分，剩下的碳原子既可以是环状部分的取代基的一部分，也可以是桥连基团与间隔基单元的一部分，其中一个或多个剩余的碳原子可被氧原子代替，不包含双酚结构的主链单元，一个或多个两个间隔单元（S）通过醚键连接到骨架单元（U），至少一个具有-CH 2 -CH 2 -CH 2 -CH 2 -O-CH 2 -CH（Q）的间隔单元（S） -OG链或-CH2-CH（OG）-CH2-OM残基或这些两种间隔物在一个间隔单元内的混合物，其中G具有至少一个选自丙酰基，甲基酰基，乙酰基，苯甲酰基和组合的基团具有至少一个芳基的M及其组合，具有选自至少一个基团的Q 氢，甲基，苯基，苯氧基甲基及其组合，b）填料（B）和c）引发剂（C）。

5. 发明授权

US08710113B2 Dental composition, kit of parts and use thereof 有权
标题翻译：牙科组成，零件套件及其用途
公开(公告)号：US08710113B2
公开(公告)日：2014-04-29
申请号：US13807553
申请日：2011-06-24
申请人： Adrian S. Eckert , Michael M. Cub , Bettina Hailand , Marion B. Kestel , Karsten Dede , Uwe H. Hoheisel , Gioacchino Raia , Christoph Thalacker , Reinhold Hecht , Thomas Luchterhandt , Peter Bissinger , Wolf Steiger
发明人： Adrian S. Eckert , Michael M. Cub , Bettina Hailand , Marion B. Kestel , Karsten Dede , Uwe H. Hoheisel , Gioacchino Raia , Christoph Thalacker , Reinhold Hecht , Thomas Luchterhandt , Peter Bissinger , Wolf Steiger
IPC分类号： A61K6/00 , B01F3/04 , C08F2/46 , C08G18/67 , C08G61/04
CPC分类号： A61K6/083 , A61K6/0023 , A61K6/09 , C07C271/16 , C07C2603/64 , C07C2603/66 , C08L33/00 , C08L75/16
摘要： The invention relates to a dental composition comprising a) a compound (A) with the following features: only one backbone unit (U) with 6 to 20 carbon atoms, at least 6 carbon atoms thereof forming an aromatic or an aliphatic cyclic moiety, the remaining carbon atoms either being part of substituents pending from the cyclic moiety or being part of bridging groups to spacer units, wherein one or more of the remaining carbon atoms can be replaced by an oxygen atom, the backbone unit not comprising a bisphenol structure and halogen atoms, one or two unit(s) (S) being connected to the backbone unit (U) via an ether linkage, at least one unit (S) comprising a —CH2-CH2-CH2-CH2-O—CH2-CH(Q)-OG moiety or a —CH2-CH(OG)-CH2-OM moiety or a mixture of these two types of moieties within one unit (S), with G comprising at least one polymerizable moiety and an urethane moiety, the urethane moiety acting as connecting element to unit(s) (S), and M comprising at least one group selected from acroyl, methacroyl, aryl, mixtures and combinations thereof, Q comprising at least one group selected from hydrogen, methyl, phenyl, phenoxymethyl, mixtures and combinations thereof, and with the proviso that onto the backbone unit (U) at least two substituents are attached, each bearing at least one group G, wherein in the case where only one unit (S) is present, the group G not being part of said unit (S) is located in the further substituent pending from unit (U), b) a filler (B) and c) an initiator (C).
摘要翻译：本发明涉及牙科用组合物，其包含a）具有以下特征的化合物（A）：只有一个具有6至20个碳原子的骨架单元（U），其至少6个碳原子形成芳族或脂族环状部分，剩余的碳原子是作为从环状部分悬挂的取代基的一部分或作为间隔基单元的桥连基团的一部分，其中一个或多个剩余的碳原子可被氧原子代替，所述主链单元不包含双酚结构和卤素原子，一个或两个单元（S）经由醚键连接至主体单元（U），至少一个包含-CH 2 -CH 2 -CH 2 -CH 2 -O-CH 2 -CH（CH 3） Q）-OG部分或-CH2-CH（OG）-CH2-OM部分或这些两种类型的部分在一个单位（S）内的混合物，其中G包含至少一个可聚合部分和氨基甲酸酯部分，氨基甲酸酯用作单元（S）的连接元件的部分，和M包含至少一个选自acroy的基团 Q，其包含至少一个选自氢，甲基，苯基，苯氧基甲基，其混合物和组合的基团，并且条件是在主链单元（U）上连接至少两个取代基各自具有至少一个基团G，其中在仅存在一个单元（S）的情况下，不是所述单元（S）的一部分的组G位于从单元（U）悬挂的另外的取代基中，b）填料（B）和c）引发剂（C）。

6. 发明申请

US20130303655A1 DENTAL COMPOSITION, METHOD OF PRODUCING AND USE THEREOF 有权
标题翻译：牙齿组合物，其生产方法和用途
公开(公告)号：US20130303655A1
公开(公告)日：2013-11-14
申请号：US13997697
申请日：2012-01-12
申请人： Adrian S. Eckert , Michael M. Cub , Bettina Hailand , Marion B. Kestel , Karsten Dede , Uwe H. Hoheisel , Gioacchino Raia , Christoph Thalacker , Reinhold Hecht , Thomas Luchterhandt
发明人： Adrian S. Eckert , Michael M. Cub , Bettina Hailand , Marion B. Kestel , Karsten Dede , Uwe H. Hoheisel , Gioacchino Raia , Christoph Thalacker , Reinhold Hecht , Thomas Luchterhandt
IPC分类号： A61K6/083 , A61K6/00
CPC分类号： A61K6/083 , A61K6/00 , A61K6/0002 , A61K6/0005 , A61K6/0017
摘要： The invention relates to a dental composition having a) compound (A) with the following features: only one backbone unit (U) with 6 to 20 carbon atoms, at least 6 carbon atoms thereof forming an aromatic or an aliphatic cyclic moiety, the remaining carbon atoms either being part of substituents pending from the cyclic moiety or being part of bridging groups to spacer units, wherein one or more of the remaining carbon atoms can be replaced by an oxygen atom, the backbone unit not comprising a bisphenol structure, one or two spacer unit(s) (S) being connected to the backbone unit (U) via an ether linkage, at least one spacer unit (S) having a —CH2-CH2-CH2-CH2-O—CH2-CH(Q)-OG chain or a —CH2-CH(OG)-CH2-OM residue or a mixture of these two types of spacers within one spacer unit, with G having at least one group selected from acroyl, methacroyl, acetyl, benzoyl, and combinations thereof, M having at least one aryl group, and combinations thereof, Q having at least one group selected from hydrogen, methyl, phenyl, phenoxymethyl, and combinations thereof, b) filler (B) and c) initiator (C).
摘要翻译：本发明涉及具有以下特征的具有a）化合物（A）的牙科用组合物：只有一个具有6至20个碳原子的骨架单元（U），其至少6个碳原子形成芳族或脂族环状部分，剩下的碳原子既可以是环状部分的取代基的一部分，也可以是桥连基团与间隔基单元的一部分，其中一个或多个剩余的碳原子可被氧原子代替，不包含双酚结构的主链单元，一个或多个两个间隔单元（S）通过醚键连接到骨架单元（U），至少一个具有-CH 2 -CH 2 -CH 2 -CH 2 -O-CH 2 -CH（Q）的间隔单元（S） -OG链或-CH2-CH（OG）-CH2-OM残基或这些两种间隔物在一个间隔单元内的混合物，其中G具有至少一个选自丙酰基，甲基酰基，乙酰基，苯甲酰基和组合的基团其具有至少一个芳基的M及其组合，Q具有至少一个选自以下的基团：氢，甲基，苯基，苯氧基甲基及其组合，b）填料（B）和c）引发剂（C）。

7. 发明授权

US08236871B2 Polymerizable compositions containing salts of barbituric acid derivatives 有权
标题翻译：含有巴比土酸衍生物盐的可聚合组合物
公开(公告)号：US08236871B2
公开(公告)日：2012-08-07
申请号：US12302591
申请日：2007-05-31
申请人： Reinhold Hecht , Manfred Ludsteck , Gioacchino Raia , Joel D. Oxman
发明人： Reinhold Hecht , Manfred Ludsteck , Gioacchino Raia , Joel D. Oxman
IPC分类号： A61K6/00 , C08J3/28 , C08F2/50
CPC分类号： C08F2/40 , A61K6/0017 , A61K6/0023 , A61K6/083 , C08F4/40 , C08L33/04 , C08L43/02
摘要： This invention relates to polymerizable compositions comprising a salt of a barbituric acid derivative. The compositions are typically shelf-life stable and may be polymerized through mixing of an acidic component with the salt of a barbituric acid derivative.
摘要翻译：本发明涉及包含巴比妥酸衍生物的盐的可聚合组合物。组合物通常保质期稳定，可通过酸性组分与巴比妥酸衍生物的盐混合而聚合。

8. 发明申请

US20090192239A1 POLYMERIZABLE COMPOSITIONS CONTAINING SALTS OF BARBITURIC ACID DERIVATIVES 有权
标题翻译：含有巴比妥酸衍生物的聚合物的可聚合组合物
公开(公告)号：US20090192239A1
公开(公告)日：2009-07-30
申请号：US12302591
申请日：2007-05-31
申请人： Reinhold Hecht , Manfred Ludsteck , Gioacchino Raia , Joel D. Oxman
发明人： Reinhold Hecht , Manfred Ludsteck , Gioacchino Raia , Joel D. Oxman
IPC分类号： C08J3/28 , C08G73/06
CPC分类号： C08F2/40 , A61K6/0017 , A61K6/0023 , A61K6/083 , C08F4/40 , C08L33/04 , C08L43/02
摘要： This invention relates to polymerizable compositions comprising a salt of a barbituric acid derivative. The compositions are typically shelf-life stable and may be polymerized through mixing of an acidic component with the salt of a barbituric acid derivative.
摘要翻译：本发明涉及包含巴比妥酸衍生物的盐的可聚合组合物。组合物通常保质期稳定，可通过酸性组分与巴比妥酸衍生物的盐混合而聚合。

9. 发明申请

US20060004122A1 Self-adhesive dental materials 有权
标题翻译：自粘牙科材料
公开(公告)号：US20060004122A1
公开(公告)日：2006-01-05
申请号：US11220004
申请日：2005-09-06
申请人： Reinhold Hecht , Manfred Ludsteck , Thomas Luchterhandt , Markus Mikulla
发明人： Reinhold Hecht , Manfred Ludsteck , Thomas Luchterhandt , Markus Mikulla
IPC分类号： A61F2/00
CPC分类号： A61K6/0067 , C09J4/00 , C08F230/02 , A61K6/0835 , C08L33/08 , C08L33/10 , C08L25/16 , A61K6/0023 , A61K6/0017
摘要： The invention relates to a composition which is self-adhesive to the hard tooth tissue, comprising: (A) 5 to 75 percent by weight of one or more mono or higher functional ethylenically unsaturated compounds which additionally have an acid functional group, wherein one of said compounds has a P—OH group, for instance a phosphoric, phosphonic or phosphinic acid group; (B) 2 to 50 percent by weight of one or more mono or higher functional ethylenically unsaturated compounds without any acid functional group; (C) 22.8 to 85 percent by weight of filling material(s), comprising at least one filling material that may react with component (A) in the sense of causing a ion exchange, neutralization, salt formation and/or chelate formation reaction; (D) 0.1 to 8 percent by weight of one or more initiators and optionally activators; (E) 0.1 to 20 percent by weight of further additives, for example, modifiers, wherein the weight ration in % of component (A) relative to component (B) ranges from 21 to 90: 10 to 79.
摘要翻译：本发明涉及一种与硬牙齿组织自粘的组合物，其包含：（A）5至75重量％的一种或多种另外具有酸官能团的单官能或高官能烯键式不饱和化合物，其中，所述化合物具有P-OH基团，例如磷酸，膦酸或次膦酸基团; （B）2至50重量％的一种或多种不具有酸官能团的单官能或高官能烯属不饱和化合物; （C）22.8至85重量％的填充材料，其包含至少一种填充材料，其可在引起离子交换，中和，形成盐和/或螯合形成反应的意义上与组分（A）反应; （D）0.1至8重量％的一种或多种引发剂和任选的活化剂; （E）0.1〜20重量％的其他添加剂，例如改性剂，其中组分（A）相对于组分（B）的重量比例为21至90：10至79。

10. 发明授权

US06953535B2 Initiator system for acid dental formulations 有权
标题翻译：酸性牙科配方的引发剂体系
公开(公告)号：US06953535B2
公开(公告)日：2005-10-11
申请号：US10477723
申请日：2002-05-13
申请人： Reinhold Hecht , Manfred Ludsteck
发明人： Reinhold Hecht , Manfred Ludsteck
IPC分类号： A61K6/083 , C08F4/40 , C09K3/00 , A61F2/00 , C08K3/10 , C08L41/00
CPC分类号： A61K6/083 , A61K6/0017 , A61K6/0023 , A61K6/005 , C08L33/00
摘要： The invention relates to a redox initiator system which allows dental formulations to be cured in acidic medium by way of a free-radical polymerization and which ensures a high level of adhesion of the polymerizing composition to the hard substances of the teeth, namely enamel and, in particular, dentine.The redox initiator system comprises the following constituents: (A) from 14.9 to 50% by weight of a barbituric acid or thiobarbituric acid and/or of a barbituric or thiobarbituric acid derivative, (B) from 30 to 75% by weight of a peroxodisulfate compound and/or peroxodiphosphate compound, (C) from 10 to 35% by weight of a sulfinic acid compound, and (D) from 0.1 to 5% by weight of a copper compound.
摘要翻译：本发明涉及氧化还原引发剂体系，其允许牙科制剂通过自由基聚合在酸性介质中固化，并且确保聚合组合物与牙齿的硬物质即釉质和/ 特别是牙质。氧化还原引发剂体系包括以下组分：（A）14.9至50重量％的巴比妥酸或硫代巴比妥酸和/或巴比妥酸或硫代巴比妥酸衍生物，（B）30至75重量％的过二硫酸化合物和/或过氧二磷酸酯化合物，（C）10〜35重量％的亚磺酸化合物，（D）0.1〜5重量％的铜化合物。

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