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1. 发明授权

US08404144B2 Compositions including polymerizable bisphosphonic acids and methods 有权
标题翻译：组合物，包括可聚合双膦酸和方法
公开(公告)号：US08404144B2
公开(公告)日：2013-03-26
申请号：US12275954
申请日：2008-11-21
申请人： Ahmed S. Abuelyaman , Gail S. Boardman , Brian A. Shukla , Steven M. Aasen , Sumita B. Mitra , Markus Mikulla , David K. Cinader, Jr.
发明人： Ahmed S. Abuelyaman , Gail S. Boardman , Brian A. Shukla , Steven M. Aasen , Sumita B. Mitra , Markus Mikulla , David K. Cinader, Jr.
IPC分类号： A61K6/00 , A61K6/02 , A61K6/083 , A61C5/00
CPC分类号： A61K6/0023 , A61K6/0017 , A61K6/083 , A61K6/09 , C08L33/00 , C08L75/16
摘要： The present invention is directed to compositions containing one or more polymerizable bisphosphonic acids and optionally one or more additional polymerizable components.
摘要翻译：本发明涉及含有一种或多种可聚合双膦酸和任选的一种或多种另外的可聚合组分的组合物。

2. 发明申请

US20060004122A1 Self-adhesive dental materials 有权
标题翻译：自粘牙科材料
公开(公告)号：US20060004122A1
公开(公告)日：2006-01-05
申请号：US11220004
申请日：2005-09-06
申请人： Reinhold Hecht , Manfred Ludsteck , Thomas Luchterhandt , Markus Mikulla
发明人： Reinhold Hecht , Manfred Ludsteck , Thomas Luchterhandt , Markus Mikulla
IPC分类号： A61F2/00
CPC分类号： A61K6/0067 , C09J4/00 , C08F230/02 , A61K6/0835 , C08L33/08 , C08L33/10 , C08L25/16 , A61K6/0023 , A61K6/0017
摘要： The invention relates to a composition which is self-adhesive to the hard tooth tissue, comprising: (A) 5 to 75 percent by weight of one or more mono or higher functional ethylenically unsaturated compounds which additionally have an acid functional group, wherein one of said compounds has a P—OH group, for instance a phosphoric, phosphonic or phosphinic acid group; (B) 2 to 50 percent by weight of one or more mono or higher functional ethylenically unsaturated compounds without any acid functional group; (C) 22.8 to 85 percent by weight of filling material(s), comprising at least one filling material that may react with component (A) in the sense of causing a ion exchange, neutralization, salt formation and/or chelate formation reaction; (D) 0.1 to 8 percent by weight of one or more initiators and optionally activators; (E) 0.1 to 20 percent by weight of further additives, for example, modifiers, wherein the weight ration in % of component (A) relative to component (B) ranges from 21 to 90: 10 to 79.
摘要翻译：本发明涉及一种与硬牙齿组织自粘的组合物，其包含：（A）5至75重量％的一种或多种另外具有酸官能团的单官能或高官能烯键式不饱和化合物，其中，所述化合物具有P-OH基团，例如磷酸，膦酸或次膦酸基团; （B）2至50重量％的一种或多种不具有酸官能团的单官能或高官能烯属不饱和化合物; （C）22.8至85重量％的填充材料，其包含至少一种填充材料，其可在引起离子交换，中和，形成盐和/或螯合形成反应的意义上与组分（A）反应; （D）0.1至8重量％的一种或多种引发剂和任选的活化剂; （E）0.1〜20重量％的其他添加剂，例如改性剂，其中组分（A）相对于组分（B）的重量比例为21至90：10至79。

3. 发明授权

US07264665B2 Inert dental glass 有权
标题翻译：惰性牙科玻璃
公开(公告)号：US07264665B2
公开(公告)日：2007-09-04
申请号：US10451222
申请日：2001-12-13
申请人： Stefan Hoescheler , Markus Mikulla , Gabriele Rackelmann , Volker Bambach
发明人： Stefan Hoescheler , Markus Mikulla , Gabriele Rackelmann , Volker Bambach
IPC分类号： A61K6/02
CPC分类号： A61K6/0835 , C03C3/062 , C03C3/068 , C03C3/095 , C08L33/00
摘要： The invention relates to the use of ions of weakly basic oxides as linking ions for polyacids in cements, preferably polyelectrolyte cements. Suitable ions comprise elements of the scandium series, for example, Sc3+, Y3+, La3+, Ce4+ and all subsequent tri- and tetra-valent lanthanides and the ions Mg2+, Zn2+, Ga2+, In2+. The application of said ions permits a regulation of the cement reaction without surface treatment of the glass powder.
摘要翻译：本发明涉及使用弱碱性氧化物的离子作为粘结剂中多酸的交联离子，优选聚电解质水泥。合适的离子包括钪系列的元素，例如Sc 3+，Y 3+，La 3+，Ce 4 +和所有后续的三价和四价镧系元素和离子Mg 2+，Zn 2+，+ 2+，Ga 2+，在^{2 + 中。所述离子的应用允许调节水泥反应而不对玻璃粉末进行表面处理。}

4. 发明申请

US20090012209A1 DENTAL COMPOSITIONS CONTAINING A SURFACE-MODIFIED FILLER 审中-公开
标题翻译：含有表面改性填料的牙膏组合物
公开(公告)号：US20090012209A1
公开(公告)日：2009-01-08
申请号：US11997788
申请日：2006-07-31
申请人： Gunther Eckhardt , Markus Mikulla , Robert F. Peez , Peter Bissinger , Gabriele Gottschalk-Gaudig
发明人： Gunther Eckhardt , Markus Mikulla , Robert F. Peez , Peter Bissinger , Gabriele Gottschalk-Gaudig
IPC分类号： A61K6/083 , A61K6/08
CPC分类号： A61K6/0023 , A61K6/0017 , A61K6/0835 , A61K6/09 , C08L33/00 , C08L75/16 , C08L25/04
摘要： The present invention features ionomer compositions containing a filler surface modified with a polyacid. The compositions can be used in a variety of dental and orthodontic applications, for example, as adhesives, cements, restoratives, coatings and sealants.
摘要翻译：本发明的特征在于含有用多酸改性的填料表面的离聚物组合物。组合物可用于各种牙科和正畸应用，例如粘合剂，水泥，修复剂，涂料和密封剂。

5. 发明授权

US07456232B2 Use of branched polyacids in dental compounds 有权
标题翻译：在牙科材料中使用支链多元酸
公开(公告)号：US07456232B2
公开(公告)日：2008-11-25
申请号：US10432946
申请日：2001-11-19
申请人： Markus Mikulla , Guenther Lechner , Klaus-Peter Stefan , Gabriele Rackelmann , Gunther Eckhardt
发明人： Markus Mikulla , Guenther Lechner , Klaus-Peter Stefan , Gabriele Rackelmann , Gunther Eckhardt
IPC分类号： A61K6/083 , C08F290/04
CPC分类号： A61K6/0835 , C08L33/00
摘要： The invention relates to dental compounds that contain at least one polyacid or at least one polyacid and at least one salt of at least one polyacid. The polyacids used have at least one branch point in the polymer structure and are water-soluble and not cross-linked and their repeat units consist to at least 80 mole % of acrylic acid segments.
摘要翻译：本发明涉及含有至少一种多酸或至少一种多酸和至少一种至少一种多酸的至少一种盐的牙齿化合物。所使用的多元酸在聚合物结构中具有至少一个分支点，并且是水溶性的并且不交联，并且它们的重复单元由至少80摩尔％的丙烯酸链段构成。

6. 发明申请

US20050261393A1 Utilization of polyacids having a tight molar mass distribution 审中-公开
标题翻译：具有紧密摩尔质量分布的多元酸的利用
公开(公告)号：US20050261393A1
公开(公告)日：2005-11-24
申请号：US10432820
申请日：2001-11-19
申请人： Markus Mikulla , Gabriele Rackelmann , Klaus-Peter Stefan
发明人： Markus Mikulla , Gabriele Rackelmann , Klaus-Peter Stefan
IPC分类号： A61C5/00 , A61K6/02 , A61K6/083 , A61F2/00 , C08K3/00
CPC分类号： A61K6/0835 , C08L33/00
摘要： The invention relates to dental materials containing at least one polyacid or at least one polyacid and at least one salt of at least one polyacid with a molar mass distribution Mw/Mn ranging from 1.0 to 1.7, whereby the polyacid has a molecular weight Mw ranging from 1,000 to 500,000.
摘要翻译：本发明涉及含有至少一种多酸或至少一种多酸和至少一种摩尔质量分布Mw / Mn范围为1.0至1.7的多酸的至少一种盐的牙科材料，其中多酸的分子量Mw范围为 1,000到50万。

7. 发明授权

US08129444B2 Self-adhesive dental materials 有权
标题翻译：自粘牙科材料
公开(公告)号：US08129444B2
公开(公告)日：2012-03-06
申请号：US11220004
申请日：2005-09-06
申请人： Reinhold Hecht , Manfred Ludsteck , Thomas Luchterhandt , Markus Mikulla
发明人： Reinhold Hecht , Manfred Ludsteck , Thomas Luchterhandt , Markus Mikulla
IPC分类号： A61K6/083 , A61K6/08 , A61L24/06 , A61C5/04 , A61C5/00
CPC分类号： A61K6/0067 , C09J4/00 , C08F230/02 , A61K6/0835 , C08L33/08 , C08L33/10 , C08L25/16 , A61K6/0023 , A61K6/0017
摘要： The invention relates to a composition which is self-adhesive to the hard tooth tissue, comprising: (A) 5 to 75 percent by weight of one or more mono or higher functional ethylenically unsaturated compounds which additionally have an acid functional group, wherein one of said compounds has a P—OH group, for instance a phosphoric, phosphonic or phosphinic acid group; (B) 2 to 50 percent by weight of one or more mono or higher functional ethylenically unsaturated compounds without any acid functional group; (C) 22.8 to 85 percent by weight of filling material(s), comprising at least one filling material that may react with component (A) in the sense of causing a ion exchange, neutralization, salt formation and/or chelate formation reaction; (D) 0.1 to 8 percent by weight of one or more initiators and optionally activators; (E) 0.1 to 20 percent by weight of further additives, for example, modifiers, wherein the weight ration in % of component (A) relative to component (B) ranges from 21 to 90: 10 to 79.
摘要翻译：本发明涉及一种与硬牙齿组织自粘的组合物，其包含：（A）5至75重量％的一种或多种另外具有酸官能团的单官能或高官能烯键式不饱和化合物，其中，所述化合物具有P-OH基团，例如磷酸，膦酸或次膦酸基团; （B）2至50重量％的一种或多种不具有酸官能团的单官能或高官能烯属不饱和化合物; （C）22.8至85重量％的填充材料，其包含至少一种填充材料，其可在引起离子交换，中和，形成盐和/或螯合形成反应的意义上与组分（A）反应; （D）0.1至8重量％的一种或多种引发剂和任选的活化剂; （E）0.1〜20重量％的其他添加剂，例如改性剂，其中组分（A）相对于组分（B）的重量比例为21至90：10至79。

8. 发明申请

US20080200585A1 Sulfonium Initiators, Process For Production And Use In Cationic Polymerizable Compositions 有权
标题翻译：锍引发剂，阳离子可聚合组合物的生产和使用方法
公开(公告)号：US20080200585A1
公开(公告)日：2008-08-21
申请号：US11997192
申请日：2006-07-27
申请人： Thomas Klettke , Cornelia B. Fuehrer , Andrea Hailand , Markus Mikulla
发明人： Thomas Klettke , Cornelia B. Fuehrer , Andrea Hailand , Markus Mikulla
IPC分类号： C07C323/03 , C08G73/06 , A61K6/10
CPC分类号： C08K5/372 , C08G59/687
摘要： The invention relates to an initiator comprising at least one structural element characterized by the following formula (I) wherein X− is a non or low coordinating anion, R1, R2, R3, R4 are independently linear, cyclic or branched C1-C20 alkyl or alkylene groups, wherein one or more of the methylene groups contained in the alkyl or alkylene group can be substituted by —CO—, —CONH—, —CON(CH3)—, —S— and/or —O—, and wherein R1, R2, R3 and/or R4 can act as a bridging element connecting two or more structural elements. The invention is also related to a process of producing the initiator and to a curable composition comprising the initiator, a process for producing the curable composition a kit comprising a cationically curable composition and the inventive initiator and the use of the initiator or the curable composition comprising the initiator for various applications, especially in the dental field.
摘要翻译：本发明涉及包含至少一种结构元件的引发剂，其特征在于以下式（I），其中X为 - 非配位阴离子或低配位阴离子，R1，R2，R3，R4独立地为直链，环状或支链C 1 -C 20烷基或亚烷基，其中烷基或亚烷基中所含的一个或多个亚甲基可以被-CO - ， - CONH-，-CON（CH 3） - ， - S-和/或-O-，并且其中R 1，R 2，R 3和/或R 4可以作为连接两个或多个结构元素。本发明还涉及制备引发剂的方法和包含引发剂的可固化组合物的方法，制备可固化组合物的方法，包括阳离子可固化组合物和本发明引发剂的试剂盒以及引发剂或可固化组合物的用途，所述引发剂或可固化组合物包含用于各种应用的引发剂，特别是在牙科领域。

9. 发明授权

US07947757B2 Sulfonium initiators, process for production and use in cationic polymerizable compositions 有权
标题翻译：锍引发剂，生产和使用于阳离子可聚合组合物的方法
公开(公告)号：US07947757B2
公开(公告)日：2011-05-24
申请号：US11997192
申请日：2006-07-27
申请人： Thomas Klettke , Cornelia B. Fuehrer , Andrea Hailand , Markus Mikulla
发明人： Thomas Klettke , Cornelia B. Fuehrer , Andrea Hailand , Markus Mikulla
IPC分类号： A61K6/10 , A61C9/00 , C07C381/12
CPC分类号： C08K5/372 , C08G59/687
摘要： The invention relates to an initiator comprising at least one structural element characterized by the following formula (I) wherein X− is a non or low coordinating anion, R1, R2, R3, R4 are independently linear, cyclic or branched C1-C20 alkyl or alkylene groups, wherein one or more of the methylene groups contained in the alkyl or alkylene group can be substituted by —CO—, —CONH—, —CON(CH3)—, —S— and/or —O—, and wherein R1, R2, R3 and/or R4 can act as a bridging element connecting two or more structural elements. The invention is also related to a process of producing the initiator and to a curable composition comprising the initiator, a process for producing the curable composition a kit comprising a cationically curable composition and the inventive initiator and the use of the initiator or the curable composition comprising the initiator for various applications, especially in the dental field.
摘要翻译：本发明涉及包含至少一种结构元件的起始剂，其特征在于以下式（I），其中X是非或低配位阴离子，R 1，R 2，R 3，R 4独立地为直链，环状或支链C 1 -C 20烷基或亚烷基，其中烷基或亚烷基中所含的一个或多个亚甲基可以被-CO - ， - CONH - ， - CON（CH 3） - ， - S - 和/或-O-取代，其中R 1 R2，R3和/或R4可以作为连接两个或多个结构元件的桥接元件。本发明还涉及制备引发剂的方法和包含引发剂的可固化组合物的方法，制备可固化组合物的方法，包括阳离子可固化组合物和本发明引发剂的试剂盒以及引发剂或可固化组合物的用途，所述引发剂或可固化组合物包含用于各种应用的引发剂，特别是在牙科领域。

10. 发明授权

US06403671B1 Polymerizable composition and the application thereof as a coupling agent 失效
标题翻译：可聚合组合物及其作为偶联剂的应用
公开(公告)号：US06403671B1
公开(公告)日：2002-06-11
申请号：US09486992
申请日：2000-03-06
申请人： Robert May , Markus Mikulla , Peter Bissinger
发明人： Robert May , Markus Mikulla , Peter Bissinger
IPC分类号： C08F246
CPC分类号： A61K6/0017 , A61K6/0023 , C08F220/26 , C08F222/06 , C08L33/00
摘要： The invention relates to a polymerizable, cross-linkable composition which contains: (A) 1-99.99 wt.-% of at least one conversion product of OH-functional (meth)acrylates with (i) oligomers from unsaturated rings or heterocyclic rings and maleic anhydride and/or with (ii) at least one ring-shaped polycarboxylic acid with at least 4 ring-carbon atoms and/or the anhydrides thereof with a saturated ring system, at least 4 carboxyl groups, and 0 or 1 heterocyclic ring atoms from the group N, O, S, whereby at least one carboxyl group and/or anhydride group of the above described substance groups is reacted with unsaturated polymerizable groups; (B) 0 to 98.99 wt.-% of one or more polymerizable, unsaturated organic compounds with at least one CH2═C(R10)—COO-group, whereby R10 represents H or methyl; (C) 0.01 to 5 wt.-% initiators and optional activators; (D) 0 to 90 wt.-% common solvents; (E) 10 to 90 wt.-% common fillers, pigments, thixotropy auxiliary agents, softening agents, diluting agents, rigidifying monomers, free-radical scavengers, stabilizing agents, and other auxiliary agents. The given wt.-% refers to the sum of all components (A) to (E). The composition is suited for bonding, casting or coating substrates and is especially suited as dental coupling agents, dental filling materials, dental cements, or dental sealers in the fields of dentistry and dental technology.
摘要翻译：本发明涉及可聚合的可交联组合物，其包含：（A）1-99.99重量％的至少一种OH官能（甲基）丙烯酸酯与（i）不饱和环或杂环的低聚物的转化产物和马来酸酐和/或与（ii）具有至少4个环碳原子的至少一个环状多元羧酸和/或其酸酐具有饱和环系，至少4个羧基和0或1个杂环环原子由上述物质基团中的至少一个羧基和/或酸酐基与不饱和可聚合基团反应; （B）0至98.99重量％的一种或多种具有至少一个CH 2 = C（R 10）-COO-基团的可聚合不饱和有机化合物，其中R 10表示H或甲基; （C）0.01至5重量％的引发剂和任选的活化剂; （D）0至90重量％的常用溶剂; （E）10至90重量％的常用填料，颜料，触变助剂，软化剂，稀释剂，硬化单体，自由基清除剂，稳定剂和其它助剂。给定的重量％是指所有组分（A）至（E）的总和。该组合物适用于粘合，铸造或涂覆基材，并且特别适用于牙科和牙科技术领域中的牙科偶联剂，牙科填充材料，牙科粘固剂或牙科密封剂。

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