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1. 发明授权

US4969953A Alcohol mixture for plasticizer and method for producing the same 失效
标题翻译：增塑剂用酒精混合物及其制造方法
公开(公告)号：US4969953A
公开(公告)日：1990-11-13
申请号：US423986
申请日：1989-10-19
申请人： Chihiro Miyazawa , Akio Tsuboi
发明人： Chihiro Miyazawa , Akio Tsuboi
IPC分类号： C07C29/38 , C08K5/05
CPC分类号： C08K5/05 , C07C29/38
摘要： A C.sub.10 alcohol mixture for plasticizer, which comprises 2-propylheptanol (hereinafter referred to as "PRH"), an alcohol having a structure of condensation product of n-valeraldehyde and 2-methylbutyraldehyde (hereinafter referred to as "Component A"), an alcohol having a structure of condensation product of n-valeraldehyde and 3-methylbutyraldehyde (hereinafter referred to as "Component B"), an alcohol having a structure of condensation product of n-valeraldehyde and pivalaldehyde (hereinafter referred to as "Component C"), and other C.sub.10 alcohols (hereinafter referred to as "Component D"), characterized in that the respective components are present in the following molar ratios:Component A/PRH=0.04-1Component B/PHR=0.002-0.3Component C/PRH=0.001-0.3Component D/PRH.ltoreq.0.3.

2. 发明授权

US4822917A Process for the hydroformylation of an olefin 失效
标题翻译：烯烃加氢甲酰化的方法
公开(公告)号：US4822917A
公开(公告)日：1989-04-18
申请号：US133807
申请日：1987-12-16
申请人： Chihiro Miyazawa , Hiroshi Mikami , Akio Tsuboi , Katsuhide Hamano
发明人： Chihiro Miyazawa , Hiroshi Mikami , Akio Tsuboi , Katsuhide Hamano
IPC分类号： C07C45/50
CPC分类号： B01J31/4046 , B01J31/1875 , B01J31/4053 , C07C45/50 , B01J2231/321 , B01J2531/822 , Y02P20/584
摘要： A process for the hydroformylation of an olefin, which comprises hydroformylating an olefinic compound by reacting it with carbon monoxide and hydrogen in a hydroformylation reaction zone in the presence of a catalyst solution containing rhodium and an oxide of an organic trivalent phosphorus compound to form an aldehyde having a carbon number larger by one than that of the olefinic compound; adding an organic trivalent phosphorus compound to the reaction mixture, followed by distillation to separate a distillate containing the aldehyde from a high-boiling residue containing rhodium; oxidizing the high-boiling residue at the same time as or subsequent to the distillation to convert the organic trivalent phosphorus compound to its oxide; and recycling the oxidized residue to the hydroformylation reaction zone as a recycling catalyst solution, wherein the hydroformylation reaction is conducted under a condition such that the proportion of an alcohol content supplied as contained in the recycling catalyst solution is maintained at a level of not higher than 14% by weight based on the total amount of the olefinic compound and the catalyst solution supplied to the hydroformylation reaction zone.

3. 发明授权

US5468419A Preparation of C.sub.9 alcohol mixture and plasticizer 失效
标题翻译：制备C9醇混合物和增塑剂
公开(公告)号：US5468419A
公开(公告)日：1995-11-21
申请号：US740403
申请日：1991-08-05
申请人： Chihiro Miyazawa , Souichi Orita , Akio Tsuboi
发明人： Chihiro Miyazawa , Souichi Orita , Akio Tsuboi
IPC分类号： C07C29/16 , C07C45/50 , C09K3/00 , C07C27/20
CPC分类号： C07C45/50 , C07C29/16
摘要： A C.sub.9 alcohol mixture for plasticizer obtained by the hydroformylation and hydrogenation of a C.sub.8 olefin mixture as the starting material obtained by the dimerization of a butene fraction, said alcohol mixture comprising from 8 to 50% by weight of a first group component having a retention time not longer than the retention time of isobutyl n-caprylate, from 8 to 40% by weight of a second group component having a retention time longer than that of isobutyl n-caprylate and not longer than that of methyl n-caprate and from 20 to 80% by weight of a third group component having a retention time longer than that of methyl n-caprate, as divided into such three components by gas chromatography using a capillary column packed with a polyethylene glycol having a number average molecular weight of 15,000 to 20,000 as an isomer separating agent.
摘要翻译：一种C9醇混合物，其用于通过C8烯烃混合物的加氢甲酰化和氢化得到的增塑剂，该C8烯烃混合物作为通过丁烯馏分二聚获得的起始原料，所述醇混合物包含8至50重量％的具有保留时间的第一组分不超过正辛酸异丁酯的保留时间，8至40重量％的保留时间比正辛酸异丁酯的保留时间长的第二组组分，不超过正癸酸甲酯的保留时间，并且从20至 80重量％的保持时间比正癸酸甲酯的保留时间长的第三组分，通过使用填充有数均分子量为15,000至20,000的聚乙二醇的毛细管柱的气相色谱分为三种组分作为异构体分离剂。

4. 发明授权

US5189105A Alcohol mixture for plasticizer 失效
标题翻译：酒精混合物用于增塑剂
公开(公告)号：US5189105A
公开(公告)日：1993-02-23
申请号：US738916
申请日：1991-08-01
申请人： Chihiro Miyazawa , Souichi Orita , Akio Tsuboi
发明人： Chihiro Miyazawa , Souichi Orita , Akio Tsuboi
IPC分类号： C07C29/16 , C07C45/50
CPC分类号： C07C45/50 , C07C29/16
摘要： A C.sub.9 alcohol mixture used to make a plasticizer obtained by the hydroformylation and hydrogenation of a C.sub.8 olefin mixture as the starting material obtained by the dimerization of a butene fraction, said alcohol mixture comprising from 8 to 50% by weight of a first group component having a retention time not longer than the retention time of isobutyl n-caprylate, from 8 to 40% by weight of a second group component having a retention time longer than that of isobutyl n-caprylate and not longer than that of methyl n-caprate and from 20 to 80% by weight of a third group component having a retention time longer than that of methyl n-caprate, as divided into such three components by gas chromatography using a capillary column packed with a polyethylene glycol having a number average molecular weight of 15,000 to 20,000 as an isomer separating agent.
摘要翻译：一种C9醇混合物，用于制备通过C8烯烃混合物的加氢甲酰化和氢化获得的增塑剂，其作为通过丁烯级分的二聚获得的起始原料，所述醇混合物包含8至50重量％的具有不超过正辛酸异丁酯的保留时间的保留时间，8至40重量％的保留时间比正丁酸正丁酯的保留时间长的第二组组分，并且不超过正癸酸甲酯的保留时间， 20至80重量％的保留时间比正癸酸甲酯的保留时间长的第三组分，通过气相色谱分离成三种组分，使用填充有数均分子量为 15,000至20,000作为异构体分离剂。

5. 发明授权

US5865958A Method for separating cyclohexene 失效
标题翻译：分离环己烯的方法
公开(公告)号：US5865958A
公开(公告)日：1999-02-02
申请号：US732724
申请日：1996-10-18
申请人： Yu Kanda , Toshio Uchibori , Takeshi Ishikawa , Akio Tsuboi
发明人： Yu Kanda , Toshio Uchibori , Takeshi Ishikawa , Akio Tsuboi
IPC分类号： C07C7/08 , B01D3/40
CPC分类号： C07C7/08 , C07C2101/14 , C07C2101/16
摘要： Cyclohexene is separated from a mixture of cyclohexene and at least one of cyclohexane and benzene by subjecting the mixture to extractive distillation in the presence of an extraction solvent the formula: ##STR1## wherein R.sup.1 and R.sup.2 each is a C.sub.1-10 alkyl group or hydrogen, and n is an integer of from 2-4, thereby preparing a fraction rich in cyclohexene.
摘要翻译：将环己烯与环己烯和环己烷和苯中的至少一种的混合物分离，通过在萃取溶剂存在下进行萃取蒸馏，式中：其中R 1和R 2各自为C 1-10烷基基团或氢，n为2-4的整数，由此制备富含环己烯的级分。

6. 发明授权

US4535901A Blow-molded multi-ply vessel 失效
标题翻译：吹塑多层容器
公开(公告)号：US4535901A
公开(公告)日：1985-08-20
申请号：US341425
申请日：1982-01-21
申请人： Tadashi Okudaira , Akio Tsuboi , Yoshihisa Hama , Mamoru Hara
发明人： Tadashi Okudaira , Akio Tsuboi , Yoshihisa Hama , Mamoru Hara
IPC分类号： B29C45/16 , B29C49/22 , B65D1/02 , B65D23/00 , B32B27/00
CPC分类号： B32B1/02 , B29C45/1646 , B29C49/221 , B32B27/08 , B32B27/20 , B32B27/28 , B32B27/30 , B32B27/34 , B32B27/36 , B65D1/0215 , B29B2911/1402 , B29B2911/14026 , B29B2911/14066 , B29B2911/14073 , B29B2911/1408 , B29B2911/14093 , B29B2911/14113 , B29B2911/1412 , B29B2911/14146 , B29B2911/14593 , B29B2911/14646 , B29B2911/14653 , B29B2911/14713 , B29C2045/1648 , B29K2077/00 , B29K2105/253 , Y10T428/1352 , Y10T428/1383
摘要： A blow-molded multi-ply vessel having excellent physical properties and good appearance which comprises two or more kinds of thermoplastic resins, at least one of which is a thermoplastic polyester resin, said vessel having a multi-ply structure of three or more layers at least at the thin wall part of the body thereof and a single layer structure at least at the open end of the mouth part thereof, and at least the thin wall part of the body being biaxially orientated. The vessel is produced by sequently and alternatively injecting two or more kinds of molten thermoplastic resins into one mold with shifting injection timing from a molding machine having plural injection cylinders with one mold closing operation to form a multi-ply parison and then blow-molding the parison at an orientating temperature.
摘要翻译：一种具有优异的物理性能和良好外观的吹塑多层容器，其包含两种或更多种热塑性树脂，其中至少一种是热塑性聚酯树脂，所述容器具有三层或更多层的多层结构至少在其本体的薄壁部分处至少在其口部的开口端处具有单层结构，并且至少该主体的薄壁部分被双向定向。该容器是通过随机地和替代地将两种或更多种熔融热塑性树脂注射到一个模具中，从具有多个注射缸的成型机以一个模具关闭操作移动喷射正时，形成多层型坯，然后吹塑成型型坯在定向温度。

7. 发明授权

US4358491A Process for producing a hollow vessel having a frosted glass-like surface 失效
标题翻译：具有磨砂玻璃状表面的中空容器的制造方法
公开(公告)号：US4358491A
公开(公告)日：1982-11-09
申请号：US937699
申请日：1978-08-29
申请人： Akiho Ota , Masanori Nishikawa , Masao Hattori , Akio Tsuboi , Yoshihisa Hama , Tadashi Okudaira , Shigeharu Sugihara
发明人： Akiho Ota , Masanori Nishikawa , Masao Hattori , Akio Tsuboi , Yoshihisa Hama , Tadashi Okudaira , Shigeharu Sugihara
IPC分类号： B29B11/08 , B29B11/10 , B29C49/00 , B29C49/04 , B29C49/06 , B29C49/12 , B29C49/24 , B29C49/64 , B29C49/68 , B29C65/00 , B29K67/00 , B29L23/00 , B65D23/00 , B29C17/07
CPC分类号： B29C49/0005 , B29C49/0073 , B29C49/6445 , B29B2911/1402 , B29B2911/14026 , B29B2911/14033 , B29B2911/1404 , B29B2911/14106 , B29B2911/14133 , B29B2911/1416 , B29B2911/14593 , B29B2911/14666 , B29B2911/14693 , B29B2911/14713 , B29B2911/14726 , B29K2067/00 , B29K2995/004 , Y10S264/907 , Y10T428/1352
摘要： A process for producing a hollow vessel having a frosted glass-like surface which comprises molding a crystalline thermoplastic polyester copolymer comprising units of ethylene terephthalate as the main component into a transparent parison, crystallizing at least the surface layer portion of the parison and then subjecting it to blow molding.
摘要翻译：一种制造具有磨砂玻璃状表面的中空容器的方法，包括将包含对苯二甲酸乙二醇酯单元作为主要成分的结晶性热塑性聚酯共聚物成型为透明型坯，至少将型坯的表层部分结晶，然后使其吹塑成型。

8. 发明授权

US4398642A Multi-ply vessel and method for production thereof 失效
标题翻译：多层容器及其生产方法
公开(公告)号：US4398642A
公开(公告)日：1983-08-16
申请号：US269056
申请日：1981-06-02
申请人： Tadashi Okudaira , Akio Tsuboi , Shigeharu Sugihara , Yoshihisa Hama
发明人： Tadashi Okudaira , Akio Tsuboi , Shigeharu Sugihara , Yoshihisa Hama
IPC分类号： B32B27/08 , B65D65/40 , B65D23/00
CPC分类号： B32B27/08 , Y10S428/91 , Y10T428/1352 , Y10T428/31736 , Y10T428/31786
摘要： A multi-ply vessel which comprises an inner layer (A) composed of a thermoplastic polyester resin, a middle layer (B) composed of a metaxylylene group-containing polyamide resin and an outer layer (C) composed of a synthetic resin having impermeability to moisture, said inner layer (A) and middle layer (B) being oriented in at least one direction at the thin part of the vessel wall. This vessel is produced by orienting a parison having a multi-ply structure of the inner layer (A), the middle layer (B) and the outer layer (C) in a draw ratio of 1 to 4 times in longitudinal direction and of 2 to 7 times in crosswise direction at a temperature of from Tg+15.degree. C. to 2(Tg)+15.degree. C. (wherein Tg is the glass transition temperature of the thermoplastic polyester resin). This vessel has high transparency as well as excellent chemical resistance, impact resistance and the like because a thermoplastic polyester resin is used as the inner layer (A) and also has excellent gas barrier properties against oxygen because the metaxylylene group-containing polyamide resin is used as the middle layer (B).
摘要翻译： PCT No.PCT / JP80 / 00269 Sec。 371日期：1981年6月2日 102（e）日期1981年6月2日PCT提交1980年10月29日PCT公布。公开号WO81 / 01265 日期：1981年5月14日。一种多层容器，其特征在于，包括由热塑性聚酯树脂构成的内层（A），由含有间亚甲苯基的聚酰胺树脂构成的中间层（B）和由具有不透水性的合成树脂，所述内层（A）和中间层（B）在容器壁的薄部至少沿一个方向取向。该容器是通过将内层（A），中间层（B）和外层（C）的多层结构的型坯的纵向取向为1〜4倍的拉伸倍数和2 在Tg + 15℃至2（Tg）+15℃的温度下横向上为7倍（其中Tg是热塑性聚酯树脂的玻璃化转变温度）。由于使用热塑性聚酯树脂作为内层（A），该容器具有高透明性以及优异的耐化学性，耐冲击性等，并且由于使用含有间亚二甲苯基团的聚酰胺树脂，所以具有优异的耐氧气的阻气性作为中间层（B）。

9. 发明申请

US20090005392A1 CRYSTAL OF 6-[4-(4-PYRIDYLAMINO) PHENYL]-4,5-DIHYDRO-3(2H-PYRIDAZINONE HYDROCHLORIDE TRIHYDRATE 审中-公开
标题翻译： 6- [4-（4-吡啶基）苯基] -4,5-二氢-3（2H-吡啶酮氢氯化物三水合物）的晶体
公开(公告)号：US20090005392A1
公开(公告)日：2009-01-01
申请号：US12029208
申请日：2008-02-11
申请人： Haruki Asatani , Akio Tsuboi , Suojiang Zhang , Shinji Ohura
发明人： Haruki Asatani , Akio Tsuboi , Suojiang Zhang , Shinji Ohura
IPC分类号： A61K31/501 , C07D401/12 , A61P9/12 , A61P9/00
CPC分类号： C07D401/12 , A61K31/501
摘要： The present invention provides crystals of 6-[4-(4-pyridylamino)phenyl]-4,5-dihydro-3(2H)-pyridazinone hydrochloride trihydrate useful as a medicament for therapeutic treatment of cardiac failure, and the like; and a pharmaceutical composition comprising said crystals as an active ingredient.The crystal of the present invention has characteristic absorption peaks (2θ degrees) at 12.9 (±0.2°) and 19.0 (±0.2°), for example, in powder X-ray diffractometry.
摘要翻译：本发明提供可用作治疗心力衰竭的药物的6- [4-（4-吡啶基氨基）苯基] -4,5-二氢-3（2H） - 哒嗪酮盐酸盐三水合物的晶体等。以及包含所述晶体作为活性成分的药物组合物。本发明的晶体在例如粉末X射线衍射中具有12.9（±0.2°）和19.0（±0.2°）的特征吸收峰（2θ）。

10. 发明授权

US5750816A Process for the preparation of .alpha.-olefin oligomers 失效
标题翻译：制备α-烯烃低聚物的方法
公开(公告)号：US5750816A
公开(公告)日：1998-05-12
申请号：US609431
申请日：1996-03-01
申请人： Yoshitaka Araki , Takashi Ishikawa , Hirofumi Nakamura , Akio Tsuboi , Yoshiaki Nanba , Takeshi Okano , Takayuki Aoshima , Shinji Iwade
发明人： Yoshitaka Araki , Takashi Ishikawa , Hirofumi Nakamura , Akio Tsuboi , Yoshiaki Nanba , Takeshi Okano , Takayuki Aoshima , Shinji Iwade
IPC分类号： B01J31/02 , B01J31/04 , B01J31/12 , B01J31/14 , C07C2/30 , C07C11/02
CPC分类号： C07C11/02 , B01J31/0237 , B01J31/0244 , B01J31/0247 , B01J31/04 , B01J31/143 , C07C2/30 , B01J2231/20 , C07C2531/02 , C07C2531/04 , C07C2531/14
摘要： An oligomerization of .alpha.-olefins is carried out in a solvent using a chromium-based catalyst system comprising at least (a) a chromium compound, (b) at least one nitrogen-containing compound selected from amines, amides and imides, and (c) an alkylaluminum compound, and the catalyst components and by-product polymers are recovered simultaneously from the reaction solution. Such process is an industrially advantageous process for producing .alpha.-olefin oligomers by using a chromium-based catalyst, and is simple and capable of efficiently recovering the by-product polymers and the catalyst components simultaneously.
摘要翻译： α-烯烃的低聚反应在溶剂中使用至少包含（a）铬化合物的铬基催化剂体系，（b）至少一种选自胺，酰胺和酰亚胺的含氮化合物和（c ）烷基铝化合物，并且从反应溶液中同时回收催化剂组分和副产物聚合物。这种方法是通过使用铬基催化剂生产α-烯烃低聚物的工业上有利的方法，并且简单且能够同时有效地回收副产物聚合物和催化剂组分。

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