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1. 发明授权

US5312850A Polylactide and starch containing hot melt adhesive 失效
标题翻译：聚丙交酯和淀粉含热熔胶
公开(公告)号：US5312850A
公开(公告)日：1994-05-17
申请号：US153
申请日：1993-01-04
申请人： Carmine P. Iovine , Thomas F. Kauffman , Jules E. Schoenberg , Paul P. Puletti
发明人： Carmine P. Iovine , Thomas F. Kauffman , Jules E. Schoenberg , Paul P. Puletti
IPC分类号： C08L93/04 , C09J167/04 , C09J193/04 , C08L3/02 , C08L3/04
CPC分类号： C08L93/04 , C09J167/04 , C09J193/04
摘要： Hot melt adhesive compositions are prepared from 20 to 98% by weight of a polylactide homo- or copolymer containing at least 20 molar percent of the lactide component; 2 to 80% by weight of a polar tackifier having a Ring and Ball softening point (as described by ASTM E-26) greater than about 60.degree. C.; 0 to 50% by weight of a plasticizer; 0 to 30% by weight of a wax diluent; 0-3% by weight of a stabilizer; and 0-20% of starch. By utilizing a naturally occurring, thermoplastic, biodegradable copolymer as the base polymer, these adhesives advance the state of the art of hot melt adhesives by alleviating the dependence on petroleum based materials and by allowing for the development of hot melt adhesives which either degrade naturally after coming in contact with the soil or which can be composted.
摘要翻译：由20至98重量％的含有至少20摩尔％丙交酯组分的聚丙交酯均聚物或共聚物制备热熔粘合剂组合物; 2至80重量％的具有环球软化点（如ASTM E-26所述）的极性增粘剂大于约60℃; 0〜50重量％的增塑剂; 0至30重量％的蜡稀释剂; 0-3重量％的稳定剂; 和0-20％的淀粉。通过使用天然存在的，热塑性的，可生物降解的共聚物作为基础聚合物，这些粘合剂通过减轻对石油基材料的依赖性和通过允许开发热熔粘合剂来促进热熔粘合剂的技术水平，其自然降解接触土壤或可以堆肥。

2. 发明授权

US5252646A Polylactide containing hot melt adhesive 失效
标题翻译：聚丙交酯含热熔胶
公开(公告)号：US5252646A
公开(公告)日：1993-10-12
申请号：US968564
申请日：1992-10-29
申请人： Carmine P. Iovine , Thomas F. Kauffman , Jules E. Schoenberg , Paul P. Puletti
发明人： Carmine P. Iovine , Thomas F. Kauffman , Jules E. Schoenberg , Paul P. Puletti
IPC分类号： C09J167/04 , C08L93/04
CPC分类号： C09J167/04
摘要： Hot melt adhesive compositions are prepared from 20 to 98% by weight of a polylactide homo- or copolymer containing at least 20 molar percent of the lactide component; 2 to 80% by weight of a polar tackifier having a Ring and Ball softening point (as described by ASTM E-26) greater than about 60.degree. C.; 0 to 50% by weight of a plasticizer; 0 to 30% by weight of a wax diluent; 0-3% by weight of a stabilizer; and 0-20% of a polymer. By utilizing a naturally occurring, thermoplastic, biodegradable copolymer as the base polymer, these adhesives advance the state of the art of hot melt adhesives by alleviating the dependence on petroleum based materials and by allowing for the development of hot melt adhesives which either degrade naturally after coming in contact with the soil or which can be composted.
摘要翻译：由20至98重量％的含有至少20摩尔％丙交酯组分的聚丙交酯均聚物或共聚物制备热熔粘合剂组合物; 2至80重量％的具有环球软化点（如ASTM E-26所述）的极性增粘剂大于约60℃; 0〜50重量％的增塑剂; 0至30重量％的蜡稀释剂; 0-3重量％的稳定剂; 和0-20％的聚合物。通过使用天然存在的，热塑性的，可生物降解的共聚物作为基础聚合物，这些粘合剂通过减轻对石油基材料的依赖性和通过允许开发热熔粘合剂来促进热熔粘合剂的技术水平，其自然降解接触土壤或可以堆肥。

3. 发明授权

US3975323A Copolyesters, method of manufacturing same, and hot melt adhesive compositions incorporating same 失效
标题翻译：共聚酯，其制造方法，以及加入其的热熔粘合剂组合物
公开(公告)号：US3975323A
公开(公告)日：1976-08-17
申请号：US542692
申请日：1975-01-21
申请人： Paul C. Georgoudis , Jules E. Schoenberg , Dilip K. Ray-Chaudhuri , Paul P. Puletti
发明人： Paul C. Georgoudis , Jules E. Schoenberg , Dilip K. Ray-Chaudhuri , Paul P. Puletti
IPC分类号： C08G63/00 , C08G63/08 , C08G63/16 , C08G63/181 , C08G63/52 , C08G63/60 , C09J167/00 , C08L91/00
CPC分类号： C08G63/52 , C08G63/08 , C08G63/16
摘要： A copolyester is formed of at least one symmetrical aromatic dicarboxylic acid member, at least one dimer acid, and at least one C.sub.2 --C.sub.10 glycol, and at least one polyester polyol member. The polyester polyol member is either a polycaprolactone polyol having a molecular weight of 500-5,000, or a mixture of a polycaprolactone diol having a molecular weight of 300-5,000 and a nonpolymeric polyol. The resultant thermoplastic copolyester has a glass transition temperature of less than 25.degree.C and a polymer melting temperature greater than 70.degree.C, and is useful both as a hot melt adhesive by itself and as an ingredient of both pressure sensitive and non-pressure sensitive hot melt adhesive formulations. In producing the copolyester, an intermediate copolyester of the symmetrical aromatic dicarboxylic acid member, the dimer acid, and the glycol is chain extended by reaction with the polyester polyol member in a 2-6 hour reaction at about 225.degree.-270.degree.C under a vacuum of about 1-30 mm. Hg. pressure.
摘要翻译：共聚酯由至少一种对称的芳族二羧酸构件，至少一种二聚酸和至少一种C 2 -C 10二元醇和至少一种聚酯多元醇构件形成。聚酯多元醇构件是分子量为500-5,000的聚己内酯多元醇或分子量为300-5,000的聚己内酯二醇和非聚合多元醇的混合物。所得的热塑性共聚酯的玻璃化转变温度低于25℃，聚合物熔融温度大于70℃，并且作为热熔粘合剂本身可用作压敏和非压敏成分热熔胶配方。在共聚酯的制造中，对称的芳族二羧酸成
分，二聚酸和二醇的中间共聚酯在约225-270℃的2-6小时反应中，与聚酯多元醇成
分反应，在真空度约1-30毫米。汞。压力。

4. 发明授权

US06177540B1 Use of star-branched polymers in pressure sensitive adhesives 失效
标题翻译：星形支链聚合物在压敏粘合剂中的应用
公开(公告)号：US06177540B1
公开(公告)日：2001-01-23
申请号：US09190157
申请日：1998-11-12
申请人： Robert D. Harlan , Jules E. Schoenberg , Christopher G. Gore , Deepak Hariharan , Smita M. Shah
发明人： Robert D. Harlan , Jules E. Schoenberg , Christopher G. Gore , Deepak Hariharan , Smita M. Shah
IPC分类号： C08G6368
CPC分类号： C09J7/38 , Y10T156/10
摘要： This invention relates to pressure sensitive adhesives, and processes of preparing such adhesives, comprising random star polymers which are crosslinked by reaction with multifunctional crosslinking agent. These adhesives can be used in coated articles.
摘要翻译：本发明涉及压敏粘合剂和制备这种粘合剂的方法，包括通过与多官能交联剂反应而交联的无规星状聚合物。这些粘合剂可用于涂覆制品。

5. 发明授权

US4588767A Hot-melt adhesives based on vinyl polymer and process for adhering surfaces therewith 失效
标题翻译：基于乙烯基聚合物的热熔粘合剂和用于粘合表面的工艺
公开(公告)号：US4588767A
公开(公告)日：1986-05-13
申请号：US737647
申请日：1985-05-24
申请人： Jules E. Schoenberg , Thomas P. Flanagan , Dilip K. Ray-Chaudhuri
发明人： Jules E. Schoenberg , Thomas P. Flanagan , Dilip K. Ray-Chaudhuri
IPC分类号： A61L15/58 , C08F220/12 , C09J133/08 , C08F210/14
CPC分类号： C09J133/08 , A61L15/58 , C08F220/12 , C09J2201/61
摘要： A hot-melt adhesive especially useful in the construction of disposable diapers contains a vinyl polymer of 40-90% by weight of a C.sub.1 -C.sub.12 alkyl acrylate and 10-60% by weight of an alpha-olefin of C.sub.20 -C.sub.40, wherein the alkyl acrylate may be partially replaced with vinyl acetate or with a C.sub.6 -C.sub.12 olefin or with mixtures thereof, provided that the polymer contain at least 10% by weight of the alkyl acrylate. The adhesive may also contain a tackifying resin, a wax, an oil or a stabilizer depending on the specific end-use desired. In a preferred embodiment the polymer contains 20-45% by weight of the alpha-olefin.
摘要翻译：特别可用于一次性尿布结构的热熔粘合剂包含40-90重量％的丙烯酸C1-C12烷基酯和10-60重量％的C20-C40的α-烯烃的乙烯基聚合物，其中丙烯酸烷基酯可以用乙酸乙烯酯或与C 6 -C 12烯烃或其混合物部分替代，条件是聚合物含有至少10重量％的丙烯酸烷基酯。粘合剂还可以含有增粘树脂，蜡，油或稳定剂，这取决于所需的特定最终用途。在优选的实施方案中，聚合物含有20-45重量％的α-烯烃。

6. 发明授权

US4139693A 2-Cyanoacrylate adhesive compositions having enhanced bond strength 失效
标题翻译：具有增强的粘合强度的2-氰基丙烯酸酯粘合剂组合物
公开(公告)号：US4139693A
公开(公告)日：1979-02-13
申请号：US891375
申请日：1978-03-29
申请人： Jules E. Schoenberg
发明人： Jules E. Schoenberg
IPC分类号： C09J4/04 , C09J4/00 , C08F120/34
CPC分类号： C09J4/00 , C08K5/13 , Y10T428/31649 , Y10T428/31699 , Y10T428/31935
摘要： Adhesive compositions having enhanced bond strength are obtained by mixing a monomeric ester of 2-cyanoacrylic acid with an anionic polymerization inhibitor and from 1 to 30 mmoles per kg. of adhesive of an adhesion promoter of the formula: ##STR1## wherein R' is hydrogen or an alkyl, aryl or cycloalkyl group having 1-10 carbon atoms. Such compositions may be used on a wide variety of substrates and are particularly useful on metals.
摘要翻译：通过将2-氰基丙烯酸的单体酯与阴离子聚合抑制剂混合并且每公斤1至30毫摩尔来获得具有增强粘合强度的粘合剂组合物。粘合促进剂的粘合剂，其具有下式：其中R'是氢或具有1-10个碳原子的烷基，芳基或环烷基。这样的组合物可以用于各种各样的基底上，并且特别适用于金属。

7. 发明授权

US4975221A High purity epoxy formulations for use as die attach adhesives 失效
标题翻译：高纯度环氧树脂配方，用作贴片粘合剂
公开(公告)号：US4975221A
公开(公告)日：1990-12-04
申请号：US350987
申请日：1989-05-12
申请人： Shuhchung S. Chen , Jules E. Schoenberg , Song Park
发明人： Shuhchung S. Chen , Jules E. Schoenberg , Song Park
IPC分类号： C08L63/00 , C08G59/00 , C09J9/02 , C09J163/00 , H01L21/52
CPC分类号： C09J163/00 , H01L24/29 , H01L2924/10253 , H01L2924/15747 , Y10T428/31511 , Y10T428/31529
摘要： This invention presents improved epoxy-based die attach adhesives which are of low viscosity, high ionic purity, and stable toward thermal cycling. This improvement is obtained by including in the formulation carboxy terminated polymers which are the reaction products of polyether diols with cyclic dianhydrides.

8. 发明授权

US4405770A Novel polyimides, and polyamic acid and ester intermediates thereof 失效
标题翻译：新型聚酰亚胺及其聚酰胺酸及其酯中间体
公开(公告)号：US4405770A
公开(公告)日：1983-09-20
申请号：US292257
申请日：1981-08-12
申请人： Jules E. Schoenberg , Stephen P. Anderson
发明人： Jules E. Schoenberg , Stephen P. Anderson
IPC分类号： C08G73/10 , C08G73/12
CPC分类号： C08G73/1064 , C08G73/105 , Y10T428/31721
摘要： Novel polyimides, optionally end-capped with polymerizable or inert groups, and the polyamic acid or ester intermediates thereof are prepared by reacting a tetracarboxylic acid compound (e.g. pyromellitic dianhydride or 3,3',4,4'-benzophenone tetracarboxylic acid dianhydride or its methyl diester) with diamines having the general formula ##STR1## wherein Z is oxygen or sulfur, X and/or Y are carbonyl or carbinol groups, the amine groups may be in the 2-, 3-, and/or 4-position, and isomerism is present when X and/or Y is a carbinol group. The polyimides may be end-capped by reaction, during or after their formation, with polymerizable groups such as 3-aminophenyl acetylene or 3,6-endomethylene-1,2,3,6-tetrahydrophthalic anhydride. The diamines are novel classes of amines when Z is sulfur and when Z is oxygen and X, Y, or X and Y are carbinol groups.
摘要翻译：可选地用可聚合或惰性基团封端的新型聚酰亚胺，其聚酰胺酸或酯中间体是通过使四羧酸化合物（例如均苯四酸二酐或3,3'，4,4'-二苯甲酮四羧酸二酐或其甲基二酯）与具有通式为“IMAGE”的二胺，其中Z是氧或硫，X和/或Y是羰基或甲醇基，胺基可以是2-，3-和/或4-位，并且当X和/或Y是甲醇基团时存在异构体。聚酰亚胺可以通过其形成过程中或之后的反应，可聚合基团如3-氨基苯基乙炔或3,6-内亚甲基-1,2,3,6-四氢邻苯二甲酸酐封端。当Z是硫时，当Z是氧而X，Y或X和Y是甲醇基时，二胺是新的胺类。

9. 发明授权

US4182823A Anionic polymerization inhibitor for cyanoacrylate adhesives 失效
标题翻译：氰基丙烯酸酯胶粘剂的阴离子聚合抑制剂
公开(公告)号：US4182823A
公开(公告)日：1980-01-08
申请号：US934856
申请日：1978-08-18
申请人： Jules E. Schoenberg
发明人： Jules E. Schoenberg
IPC分类号： C08F2/40 , C08F22/32 , C08F120/50
CPC分类号： C08F22/32 , Y10T428/31855
摘要： An adhesive composition based on 2-cyanoacrylate esters contains as an anionic polymerization inhibitor an acid chelate formed of boric acid or a derivative thereof and a selected polyhydroxy compound. The chelate is conveniently formed in situ in the 2-cyanoacrylate ester, but may also be prepared separately and added to the ester directly. An exemplary acid chelate used as stabilizer is prepared from boric acid and pyrogallol. The resulting stabilized adhesive compositions have a rapid cure rate and may be used on a wide variety of substrates.
摘要翻译：基于2-氰基丙烯酸酯的粘合剂组合物含有由硼酸或其衍生物和选择的多羟基化合物形成的酸螯合物作为阴离子聚合抑制剂。螯合物方便地在2-氰基丙烯酸酯中原位形成，但也可以单独制备并直接加入到酯中。由硼酸和连苯三酚制备用作稳定剂的示例性酸螯合物。所得到的稳定的粘合剂组合物具有快速的固化速率，并可用于各种各样的基材上。

10. 发明授权

US5506298A Polyamide graft-modified rubbery block copolymer compositions 失效
标题翻译：聚酰胺接枝改性橡胶嵌段共聚物组合物
公开(公告)号：US5506298A
公开(公告)日：1996-04-09
申请号：US226613
申请日：1994-04-12
申请人： Charles W. Paul , Jules E. Schoenberg
发明人： Charles W. Paul , Jules E. Schoenberg
IPC分类号： C08G81/02 , C08L77/06 , C08L77/08
CPC分类号： C08G81/028
摘要： Polyamide graft-modified rubbery block copolymer compositions are provided by reaction of maleated rubbery block copolymers with polymeric dimer fatty acid based polyamide wherein the molar ratio of maleated rubbery block copolymer to the dimer fatty acid polyamide is greater than 2 to 1. The compositions find use as hot melt adhesive components.
摘要翻译：聚酰胺接枝改性橡胶嵌段共聚物组合物通过马来化橡胶嵌段共聚物与聚合二聚脂肪酸基聚酰胺的反应提供，其中马来橡胶嵌段共聚物与二聚脂肪酸聚酰胺的摩尔比大于2:1。该组合物使用作为热熔胶成分。

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