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1. 发明授权

US5290824A Photocrosslinked second order nonlinear optical polymers 失效
标题翻译：光交联二阶非线性光学聚合物
公开(公告)号：US5290824A
公开(公告)日：1994-03-01
申请号：US881609
申请日：1992-05-12
申请人： Braja K. Mandal , Sukant K. Tripathy , Jan-Chuan Huang , Jayant Kumar
发明人： Braja K. Mandal , Sukant K. Tripathy , Jan-Chuan Huang , Jayant Kumar
IPC分类号： C08F2/46 , C08F8/14 , G02F1/361 , G03F7/00 , G03F7/038
CPC分类号： G03F7/001 , C08F8/14 , G02F1/3617 , G03F7/0388 , C08F2810/30 , Y10S430/12
摘要： A novel photocrosslinkable polymeric system has been developed for processing into films having stable second-order nonlinear optical properties. In the present system, polymers bearing photo-crosslinkable chromophores, such as polyvinylcinnamate and are reacted with appropriately designed nonlinear optical molecules with the cinnamate or other photocrosslinkable functionalities for photocrosslinking at one, two or more points. The system can be poled and photocrosslinked in the poled state to yield a material with stable optical nonlinearity and large electro-optic coefficients.
摘要翻译：已经开发了一种新颖的可光交联聚合物体系，用于加工成具有稳定二阶非线性光学性质的膜。在本系统中，含有光可交联发色团的聚合物如聚乙烯基肉桂酸酯，并与适当设计的非线性光学分子与肉桂酸酯或其它可光交联官能团反应，用于在一个，两个或更多个点进行光致交联。该系统可以在极化状态下被极化和光交联，以产生具有稳定的光学非线性和大的电光系数的材料。

2. 发明授权

US5112881A Photocrosslinked second order nonlinear optical polymers 失效
标题翻译：光交联二阶非线性光学聚合物
公开(公告)号：US5112881A
公开(公告)日：1992-05-12
申请号：US573253
申请日：1990-08-24
申请人： Braja K. Mandal , Sukant K. Tripathy , Jan-Chan Huang , Jayant Kumar
发明人： Braja K. Mandal , Sukant K. Tripathy , Jan-Chan Huang , Jayant Kumar
IPC分类号： C08F2/46 , C08F8/14 , G02F1/361 , G03F7/00 , G03F7/038
CPC分类号： G03F7/001 , C08F8/14 , G02F1/3617 , G03F7/0388 , C08F2810/30 , Y10S430/12
摘要： A novel photocrosslinkable polymeric system has been developed for processing into films having stable second-order nonlinear optical properties. In the present system, polymers bearing photocrosslinkable chromophores, such as polyvinylcinnamate and are reacted with appropriately designed nonlinear optical molecules with the cinnamate or other photocrosslinkable functionalities for photocrosslinking at one, two or more points. The system can be poled and photocrosslinked in the poled state to yield a material with stable optical nonlinearity and large electro-optic coefficients.
摘要翻译：已经开发了一种新颖的可光交联聚合物体系，用于加工成具有稳定二阶非线性光学性质的膜。在本系统中，含有光可交联发色团的聚合物如聚乙烯基肉桂酸酯，并与适当设计的非线性光学分子与肉桂酸酯或其它可光交联官能团反应，以在一个，两个或更多个点进行光致交联。该系统可以在极化状态下被极化和光交联，以产生具有稳定的光学非线性和大的电光系数的材料。

3. 发明授权

US5484821A Photocrosslinked second order nonlinear optical polymers 失效
标题翻译：光交联二阶非线性光学聚合物
公开(公告)号：US5484821A
公开(公告)日：1996-01-16
申请号：US192785
申请日：1994-02-07
申请人： Braja K. Mandal , Sukant K. Tripathy , Jan-Chan Huang , Jayant Kumar
发明人： Braja K. Mandal , Sukant K. Tripathy , Jan-Chan Huang , Jayant Kumar
IPC分类号： C08F2/46 , C08F8/14 , G02F1/361 , G03F7/00 , G03F7/038 , C08J3/28
CPC分类号： G03F7/001 , C08F8/14 , G02F1/3617 , G03F7/0388 , C08F2810/30 , Y10S430/12
摘要： A novel photocrosslinkable polymeric system has been developed for processing into films having stable second-order nonlinear optical properties. In the present system, polymers bearing photo-crosslinkable chromophores, such as polyvinylcinnamate and are reacted with appropriately designed nonlinear optical molecules with the cinnamate or other photocrosslinkable functionalities for photocrosslinking at one, two or more points. The system can be poled and photocrosslinked in the poled state to yield a material with stable optical nonlinearity and large electro-optic coefficients.
摘要翻译：已经开发了一种新颖的可光交联聚合物体系，用于加工成具有稳定二阶非线性光学性质的膜。在本系统中，含有光可交联发色团的聚合物如聚乙烯基肉桂酸酯，并与适当设计的非线性光学分子与肉桂酸酯或其它可光交联官能团反应，用于在一个，两个或更多个点进行光致交联。该系统可以在极化状态下被极化和光交联，以产生具有稳定的光学非线性和大的电光系数的材料。

4. 发明授权

US5223356A Photocrosslinked second order nonlinear optical polymers 失效
标题翻译：光交联二阶非线性光学聚合物
公开(公告)号：US5223356A
公开(公告)日：1993-06-29
申请号：US700261
申请日：1991-05-15
申请人： Jayant Kumar , Sukant K. Tripathy , Braja K. Mandal , Jan-Chan Huang
发明人： Jayant Kumar , Sukant K. Tripathy , Braja K. Mandal , Jan-Chan Huang
IPC分类号： C08F8/14 , G02F1/361 , G03F7/00 , G03F7/038
CPC分类号： C08F8/14 , G02F1/3617 , G03F7/001 , G03F7/0388 , C08F2810/30
摘要： A novel photocrosslinkable polymeric system has been developed for processing into films having stable second-order nonlinear optical properties. In the present system, polymers bearing photo-crosslinkable chromophores, such as polyvinylcinnamate and are reacted with appropriately designed nonlinear optical molecules with the cinnamate or other photocrosslinkable functionalities for photocrosslinking at one, two or more points. The system can be poled and photocrosslinked in the poled state to yield a material with stable optical nonlinearity and large electro-optic coefficients.
摘要翻译：已经开发了一种新颖的可光交联聚合物体系，用于加工成具有稳定二阶非线性光学性质的膜。在本系统中，含有光可交联发色团的聚合物如聚乙烯基肉桂酸酯，并与适当设计的非线性光学分子与肉桂酸酯或其它可光交联官能团反应，用于在一个，两个或更多个点进行光致交联。该系统可以在极化状态下被极化和光交联，以产生具有稳定的光学非线性和大的电光系数的材料。

5. 发明授权

US5143828A Method for synthesizing an enzyme-catalyzed polymerized monolayer 失效
标题翻译：合成酶催化聚合单层的方法
公开(公告)号：US5143828A
公开(公告)日：1992-09-01
申请号：US815213
申请日：1991-12-31
申请人： Joseph A. Akkara , David L. Kaplan , Lynne A. Samuelson , Braja K. Mandal , Sukant K. Tripathy , Ferdinando F. Bruno , Kenneth A. Marx
发明人： Joseph A. Akkara , David L. Kaplan , Lynne A. Samuelson , Braja K. Mandal , Sukant K. Tripathy , Ferdinando F. Bruno , Kenneth A. Marx
IPC分类号： B05D1/20 , C08G61/10 , C08G73/02 , C12P7/22 , C12P13/00
CPC分类号： B82Y30/00 , B05D1/204 , B82Y40/00 , C08G61/10 , C08G73/0266 , C12P13/001 , C12P7/22
摘要： A method for synthesizing enzyme-catalyzed polymers using the Langmuir-Blodgett technique. In one embodiment, the process comprises spreading one or more enzyme-polymerizable monomers on a water-miscible solvent. The monomers are sufficiently surface active that they align themselves on the air-solvent interface. Next, pressure is applied to the interface to form a monolayer made up of the monomers. An enzyme is then introduced into the solvent, causing polymerization of the monomers in the monolayer. The polymeric monolayers produced by the present method are easier to process and have reduced cross-linking and branching as compared to similar polymers produced in bulk by enzyme-catalyzed reactions.
摘要翻译：使用Langmuir-Blodgett技术合成酶催化聚合物的方法。在一个实施方案中，该方法包括将一种或多种可酶聚合的单体铺在水混溶性溶剂上。单体具有足够的表面活性，使得它们自己在空气 - 溶剂界面上对准。接下来，向界面施加压力以形成由单体组成的单层。然后将酶引入溶剂中，引起单体在单层中的聚合。通过本发明方法制备的聚合物单层与通过酶催化反应在本体产生的类似聚合物相比更容易加工并且具有减少的交联和支化。

6. 发明授权

US5846753A Chemiluminescence-based method for rapid and sensitive in-situ detection of organophosphorus compounds and metal ions 失效
标题翻译：基于化学发光的方法，用于快速和灵敏地原位检测有机磷化合物和金属离子
公开(公告)号：US5846753A
公开(公告)日：1998-12-08
申请号：US445565
申请日：1995-05-30
申请人： Joseph A. Akkara , David L. Kaplan , Madhu S. R. Ayyagari , Kenneth A. Marx , Sanjay Kamtekar , Rajiv Pande , Sukant K. Tripathy , Jayant Kumar
发明人： Joseph A. Akkara , David L. Kaplan , Madhu S. R. Ayyagari , Kenneth A. Marx , Sanjay Kamtekar , Rajiv Pande , Sukant K. Tripathy , Jayant Kumar
IPC分类号： C12Q1/42 , C07D305/14 , C12Q1/44
CPC分类号： C12Q1/42 , C12Q2334/00
摘要： A method of detecting the presence of a substance being monitored in a medium, selected from the group of substances including organophosphorus compounds and the metal ions Zn, Be and Bi, including the steps of: providing a 1,2-dioxetane phenyl phosphate compound; providing a phosphatase that catalytically degrades the 1,2-dioxetane phenyl phosphate compound to produce light, the catalytic activity of the phosphatase toward 1,2-dioxetane phenyl phosphate compound being altered by the substance being monitored; exposing the 1,2-dioxetane phenyl phosphate compound and the phosphatase together to a medium which may contain the substance being monitored; detecting light produced after the exposing step; and determining, from the detected light, the presence and concentration in the medium of the substance being monitored.
摘要翻译：一种检测在包括有机磷化合物和金属离子Zn，Be和Bi的物质组中的介质中被监测物质的存在的方法，包括以下步骤：提供1,2-二氧环乙烷苯基磷酸酯化合物; 提供催化降解1,2-二氧杂环丁烷苯基磷酸酯化合物以产生光的磷酸酶，磷酸酯对正在监测的物质的1,2-二氧环乙烷苯基磷酸酯化合物的催化活性改变; 将1,2-二氧环乙烷苯基磷酸酯化合物和磷酸酶一起暴露于可能含有被监测物质的介质中; 检测曝光步骤后产生的光; 并且从检测到的光中确定被监测物质的介质中的存在和浓度。

7. 发明授权

US5433895A Silicon-containing networked non-linear optical compositions 失效
标题翻译：含硅网络非线性光学组合物
公开(公告)号：US5433895A
公开(公告)日：1995-07-18
申请号：US950398
申请日：1992-09-23
申请人： Ru J. Jeng , Yong M. Chen , Aloke K. Jain , Jayant Kumar , Sukant K. Tripathy
发明人： Ru J. Jeng , Yong M. Chen , Aloke K. Jain , Jayant Kumar , Sukant K. Tripathy
IPC分类号： G02F1/355 , G02F1/361 , F21V9/00
CPC分类号： G02F1/3555 , G02F1/361 , G02F1/3615
摘要： A nonlinear optical composition and a method of forming the nonlinear optical composition are disclosed. The nonlinear optical composition includes a silicon-containing component and a nonlinear optical component which causes the nonlinear optical composition to exhibit second order nonlinear optical polarization of electromagnetic radiation, such as light. The method includes forming a sol of the silicon-containing component and the nonlinear optical component of the composition. A gel is formed from the sol. The nonlinear optical component is then poled while the gel is exposed to conditions sufficient to cause formation of a nonlinear optical composition which exhibits second order nonlinear optical polarization of electromagnetic radiation.
摘要翻译：公开了非线性光学组合物和形成非线性光学组合物的方法。非线性光学组合物包括含硅组分和非线性光学组分，其使得非线性光学组合物显示诸如光的电磁辐射的二阶非线性光学偏振。该方法包括形成含硅组分的溶胶和该组合物的非线性光学组分。由溶胶形成凝胶。然后将非线性光学部件极化，同时将凝胶暴露于足以形成非线性光学组合物的条件，其呈现电磁辐射的二阶非线性光学偏振。

8. 发明授权

US6018018A Enzymatic template polymerization 失效
标题翻译：酶模板聚合
公开(公告)号：US6018018A
公开(公告)日：2000-01-25
申请号：US999542
申请日：1997-11-21
申请人： Lynne A. Samuelson , K. Shridhara Alva , Jayant Kumar , Sukant K. Tripathy
发明人： Lynne A. Samuelson , K. Shridhara Alva , Jayant Kumar , Sukant K. Tripathy
IPC分类号： C08G73/02 , H01B1/12 , C08G73/00
CPC分类号： C08G73/0266 , H01B1/128 , Y10S977/747
摘要： Polymers are formed enzymatically in the presence of an oligomeric or polymeric template. The method includes combining at least one redox monomer or, in some cases, a redox oligomer, with a template and an enzyme, such as horseradish peroxidase, to form a reaction mixture. The redox monomer or oligomer aligns along the template before or during the polymerization, the template thereby affecting at least one physical property of the resulting polymer, such as the molecular weight or shape of the polymer. In one embodiment, the template can be a polyelectrolyte or an optically active polymer.
摘要翻译：在低聚或聚合物模板存在下，酶促形成聚合物。该方法包括将至少一种氧化还原单体，或在一些情况下，将氧化还原低聚物与模板和酶如辣根过氧化物酶组合以形成反应混合物。氧化还原单体或低聚物在聚合之前或期间沿模板排列，从而影响所得聚合物的至少一种物理性能，例如聚合物的分子量或形状。在一个实施方案中，模板可以是聚电解质或旋光聚合物。

9. 发明授权

US5260004A Process of making Langmuir-Blodgett films having photo-electronic properties 失效
标题翻译：制作具有光电特性的Langmuir-Blodgett薄膜的工艺
公开(公告)号：US5260004A
公开(公告)日：1993-11-09
申请号：US802675
申请日：1991-12-02
申请人： Lynne A. Samuelson , David L. Kaplan , Kenneth A. Marx , Sukant K. Tripathy , Jayant Kumar
发明人： Lynne A. Samuelson , David L. Kaplan , Kenneth A. Marx , Sukant K. Tripathy , Jayant Kumar
IPC分类号： B05D1/20 , B29C41/12 , B29C67/24 , B29C41/02 , B29C71/02 , B29C71/04
CPC分类号： B82Y30/00 , B05D1/202 , B29C41/12 , B29C67/24 , B82Y40/00 , B29K2089/00
摘要： Langmuir-Blodgett films having photo-electronic properties and methods of making the same. The instant films may be made, for example, by spreading a mixture of one or more types of biotinylated lipids and one or more types of electrically-conductive lipids over a water-miscible liquid subphase. Conjugated molecules comprising a biotin-binding component made up of an avidin or streptavidin molecule or a fragment or derivative thereof having biotin-binding activity and a photodynamic proteinaceous component are then injected into the subphase. Because of the affinity between biotin and the biotin-binding component, the conjugated molecules bind to the biotinylated lipids. The air-subphase interface is then compressed, causing the biotinylated lipids and electrically-conductive lipids to form a monolayer thereat. In one embodiment, the biotin-binding component has biotin-binding sites available on its underside which may be used to bind biotinylated derivatives of one or more different species of photodynamic proteinaceous components and/or to build up a multilayered complex of biotin-binding molecules and functional proteinaceous components using biotinylated rigid or flexible couplers.
摘要翻译：具有光电特性的Langmuir-Blodgett薄膜及其制造方法。可以例如通过将一种或多种类型的生物素化脂质和一种或多种类型的导电脂质的混合物铺在水混溶液体相上来制备即时膜。然后将包含由具有生物素结合活性的抗生物素蛋白或链霉抗生物素蛋白分子或其片段或衍生物的生物素结合组分的结合分子和光动力学蛋白质组分注入到亚相中。由于生物素与生物素结合成分之间的亲和力，共轭分子与生物素化的脂质结合。然后将空气 - 亚相界面压缩，导致生物素化的脂质和导电脂质在其上形成单层。在一个实施方案中，生物素结合组分在其下侧具有可用的生物素结合位点，其可用于结合一种或多种不同种类的光动力蛋白质组分的生物素化衍生物和/或建立生物素结合分子的多层复合物和使用生物素化的刚性或柔性耦合剂的功能蛋白质组分。

10. 发明授权

US06569651B1 Enzymatic polymerization of anilines or phenols around a template 失效
标题翻译：苯胺或酚类在模板周围的酶聚合
公开(公告)号：US06569651B1
公开(公告)日：2003-05-27
申请号：US09334105
申请日：1999-06-16
申请人： Lynne A. Samuelson , Sukant K. Tripathy , Ferdinando Bruno , Ramaswamy Nagarajan , Jayant Kumar , Wei Liu
发明人： Lynne A. Samuelson , Sukant K. Tripathy , Ferdinando Bruno , Ramaswamy Nagarajan , Jayant Kumar , Wei Liu
IPC分类号： C12P1300
CPC分类号： C12P13/001 , C12P7/22 , Y10S435/817 , Y10S977/898
摘要： The micelle contains multiple units, each of which contains a hydrophobic part and a hydrophilic part. A preferred unit is dodecyl benzene sulfonic acid. Borate-containing electrolytes include trifluoroborate, trimethylborate and hydrobis(pyridine)boron. Enzymes include peroxidases such as horseradish peroxidase or lignin peroxidase, and laccase. Monomers include unsubstituted and substituted anilines and unsubstituted and substituted phenols. A method is provided for enzymatic polymerization which includes (1) obtaining a reaction mixture including a monomer, a template, and an enzyme; and (2) incubating the reaction mixture for a time and under conditions sufficient for the monomer to align along the template and polymerize to form a polymer-template complex. The template can be a micelle, a borate-containing electrolyte, or lignin sulfonate. The polymer-template complex may be conductive, and possesses exceptional electrical and optical stability, water solubility, and processibility, and can be used in applications such as light-weight energy storage devices (e.g., rechargeable batteries), electrolytic capacitors, anti-static and anti-corrosive coatings for smart windows, and biological sensors.
摘要翻译：胶束含有多个单元，每个单元含有疏水部分和亲水部分。优选的单元是十二烷基苯磺酸。含硼酸盐的电解质包括三氟硼酸盐，硼酸三甲酯和氢化双（吡啶）硼。酶包括过氧化物酶如辣根过氧化物酶或木质素过氧化物酶，以及漆酶。单体包括未取代的和取代的苯胺和未取代的和取代的酚。提供了一种用于酶促聚合的方法，其包括（1）获得包含单体，模板和酶的反应混合物; 和（2）将反应混合物温育一段时间并在足以使单体沿着模板排列的聚合物形成聚合物 - 模板复合物的条件下。模板可以是胶束，含硼酸盐的电解质或木质素磺酸盐。聚合物 - 模板复合物可以是导电的，并且具有优异的电和光学稳定性，水溶性和可加工性，并且可以用于诸如轻量储能装置（例如可再充电电池），电解电容器，防静电以及智能窗户和生物传感器的防腐涂料。

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