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1. 发明授权

US4000050A Photochemical preparation of polycycloalkyl oxyalkanes and oxyalkenes 失效
标题翻译：聚环烷基氧基烷烃和氧辛烯的光化学制备
公开(公告)号：US4000050A
公开(公告)日：1976-12-28
申请号：US551030
申请日：1975-02-19
申请人： Braja Dulal Mookherjee , Venkatesh Kamath , Ramanlal Ranchodji Patel , Edward J. Shuster
发明人： Braja Dulal Mookherjee , Venkatesh Kamath , Ramanlal Ranchodji Patel , Edward J. Shuster
IPC分类号： A61K8/34 , A61K8/49 , A61Q13/00 , C07C27/00 , C07C31/137 , C07C33/05 , C07C67/00 , C07D303/04 , C11B9/00 , B01J1/10
CPC分类号： C11B9/0042 , C07D303/04 , C11B9/0046 , Y10S204/904 , Y10S204/912
摘要： Processes and compositions are described for altering the aroma of consumable products including perfumes, perfume compositions and perfumed articles utilizing as the essential ingredient one or more of the polycycloalkyl oxyalkanes and/or oxyalkenes (broadly hereinafter referred to as polycycloalkyl oxyhydrocarbons) having the generic formula: ##STR1## the polycyclic moiety being bicyclic or tricyclic, wherein X is one of the moieties: ##STR2## provided that the polycyclic moiety is tricyclic only when X contains an epoxide moiety; and wherein one of the dashed lines is a carbon-carbon bond and each of the wavy lines is a carbon-carbon single bond, one of the carbon-carbon single bonds represented by the wavy line being epimeric with respect to the other of the carbon-carbon single bonds represented by the wavy line; and processes for preparing individual compounds or mixtures of these compounds including the steps of:I. Subjecting one or more santalene hydrocarbons having the generic structure: ##STR3## TO PHOTOOXIDATION WITH OXYGEN, BASE AND ULTRA VIOLET LIGHT TO FORM A MIXTURE OF COMPOUNDS HAVING THE GENERIC STRUCTURES: ##STR4## ii. Optionally fractionally distilling the resulting reaction products for utilization; orIii. Optionally reacting .alpha.-santalene, beta-santalene, epi-beta-santalene or mixtures thereof with a peracid to produce onr or more epoxide compounds having the generic structure: ##STR5## IV. Optionally fractionally distilling the resulting reaction product(s) for utilization; and/orV. Optionally reducing the resulting epoxide with lithium aluminum hydride to form one or more tertiary alcohols having the generic structure: ##STR6## vi. Optionally fractionally distilling the thus formed tertiary alcohol(s); orvii. Rearranging the epoxide compounds having the generic formula: ##STR7## using diphenyl diselenide and sodium borohydride to form one or more allylic tertiary alcohols having the generic formula: ##STR8## viii. Optionally rearranging the epoxide compounds having the structure: ##STR9## using aluminum isopropoxide to form allylic secondary alcohols having the generic structure: ##STR10## ix. Optionally fractionally distilling the allylic secondary alcohols. In addition the novel compounds having the generic structure: ##STR11## as well as the structure: ##STR12## wherein X is one of the moieties: ##STR13## are described.
摘要翻译：描述的方法和组合物用于改变消耗性产品的香味，包括香料，香料组合物和使用作为必需成分的一种或多种多环烷基氧基烷烃和/或氧烯烃（以下简称为多环烷基氧代烃）的香料，其具有以下通式：多环部分是双环或三环的，其中X是部分之一：

2. 发明授权

US4119577A Substituted-norbornane perfumes compositions 失效
标题翻译：取代的降冰片烷香料组合物
公开(公告)号：US4119577A
公开(公告)日：1978-10-10
申请号：US860125
申请日：1977-12-13
申请人： Kenneth K. Light , James Milton Sanders , Manfred Hugo Vock , Edward J. Shuster , Joaquin Vinals , William L. Schreiber , John B. Hall , Denis E. Hruza, Sr. , Venkatesh Kamath , Braja Dulal Mookherjee , Ching Y. Tseng , Mark A. Sprecker
发明人： Kenneth K. Light , James Milton Sanders , Manfred Hugo Vock , Edward J. Shuster , Joaquin Vinals , William L. Schreiber , John B. Hall , Denis E. Hruza, Sr. , Venkatesh Kamath , Braja Dulal Mookherjee , Ching Y. Tseng , Mark A. Sprecker
IPC分类号： A23L27/20 , A24B15/34 , A24D3/14 , C07C29/09 , C07C29/17 , C07C29/40 , C07C29/42 , C07C29/68 , C07C31/137 , C07C33/12 , C07C45/29 , C07C45/30 , C07C45/58 , C07C45/62 , C07C45/66 , C07C45/67 , C07C45/68 , C07C45/74 , C07C49/323 , C07C49/35 , C07C49/557 , C07C49/577 , C07D301/14 , C07D303/04 , C11B9/00 , C11D3/50 , C11D9/44
CPC分类号： C11D3/0084 , A23L27/203 , A24B15/345 , A24D3/14 , C07C29/09 , C07C29/17 , C07C29/40 , C07C29/42 , C07C29/68 , C07C31/137 , C07C33/12 , C07D301/14 , C07D303/04 , C11B9/0046 , C11D3/50 , C11D9/442 , C07C2102/42 , Y10S514/974
摘要： Substituted-norbornane derivatives are described for use as perfumes, colognes and in perfume aroma augmenting, modifying, enhancing, and imparting compositions. The substituted norbornane derivatives having the following structure: ##STR1## wherein R is C.sub.3 or C.sub.4 alkenyl.
摘要翻译：描述了取代的降冰片烷衍生物用作香料，古龙水和香料香气增强，改性，增强和赋予组合物。具有以下结构的取代的降冰片烷衍生物：其中R是C 3或C 4链烯基。

3. 发明授权

US4076853A Flavoring with substituted norbornane derivatives 失效
标题翻译：用取代的降冰片烷衍生物调味
公开(公告)号：US4076853A
公开(公告)日：1978-02-28
申请号：US765847
申请日：1977-02-04
申请人： Kenneth K. Light , James Milton Sanders , Manfred Hugo Vock , Edward J. Shuster , Joaquin Vinals , William L. Schreiber , John B. Hall , Denis E. Hruza, Sr. , Venkatesh Kamath , Braja Dulal Mookherjee , Ching Y. Tseng , Mark A. Sprecker
发明人： Kenneth K. Light , James Milton Sanders , Manfred Hugo Vock , Edward J. Shuster , Joaquin Vinals , William L. Schreiber , John B. Hall , Denis E. Hruza, Sr. , Venkatesh Kamath , Braja Dulal Mookherjee , Ching Y. Tseng , Mark A. Sprecker
IPC分类号： A23L27/20 , A24B15/34 , A24D3/14 , C07C29/09 , C07C29/17 , C07C29/40 , C07C29/42 , C07C29/68 , C07C31/137 , C07C33/12 , C07C45/29 , C07C45/30 , C07C45/58 , C07C45/62 , C07C45/66 , C07C45/67 , C07C45/68 , C07C45/74 , C07C49/323 , C07C49/35 , C07C49/557 , C07C49/577 , C07D301/14 , C07D303/04 , C11B9/00 , C11D3/50 , C11D9/44 , A23L1/226
CPC分类号： C11D3/0084 , A23L27/203 , A24B15/345 , A24D3/14 , C07C29/09 , C07C29/17 , C07C29/40 , C07C29/42 , C07C29/68 , C07C31/137 , C07C33/12 , C07D301/14 , C07D303/04 , C11B9/0046 , C11D3/50 , C11D9/442 , C07C2102/42 , Y10S514/974
摘要： Norbornane derivatives are used in foodstuffs and flavorings. Specifically, alpha-allyl-3, 3-dimethyl-2-norbornanemethanol, alpha-methallyl-3,3-dimethyl-2-norbornanemethanol, and alpha-allyl-alpha-3,3-trimethyl-2-norbornanemethanol are used.
摘要翻译：降冰片烷衍生物用于食品和调味品。具体地，使用α-烯丙基-3,3-二甲基-2-降冰片烷甲醇，α-甲代烯丙基-3,3-二甲基-2-降冰片烷甲醇和α-烯丙基-α3,3-三甲基-2-降冰片烷甲醇。

4. 发明授权

US4014823A .pi.-Tricyclene-9-alkanone perfumes 失效
标题翻译： {90-三环烯-9-烷酮香料
公开(公告)号：US4014823A
公开(公告)日：1977-03-29
申请号：US646608
申请日：1976-01-05
申请人： Braja Dulal Mookherjee , Venkatesh Kamath , Edward J. Shuster
发明人： Braja Dulal Mookherjee , Venkatesh Kamath , Edward J. Shuster
IPC分类号： A23L27/20 , C07C47/115 , C07C49/115 , C07C49/21 , C11B9/00 , C11D9/44
CPC分类号： C07C49/21 , A23L27/203 , C07C47/115 , C07C49/115 , C11B9/0042 , C11D9/442 , C11D9/444 , C07C2103/64
摘要： Processes and compositions are described for altering the aroma of consumable products including perfumes, perfume compositions and perfumed articles utilizing as the essential ingredient a novel organic .pi.-tricyclene derivative having one of the formulae: ##STR1## wherein X is a moiety selected from the group consisting of: ##STR2## and wherein R.sub.1 and R.sub.2 are each selected from the group consisting of hydrogen and methyl, at least one of R.sub.1 or R.sub.2 being hydrogen. This Application is a continuation-in-part of application for U.S. Letters Patent Ser. No. 556,862, filed on Mar. 10, 1975, now U.S. Pat. No. 3,944,621 issued on Mar. 16, 1976.
摘要翻译：描述了用于改变包含香料，香料组合物和香料制品在内的消耗品的香气的方法和组合物，其利用具有下列结构式之一的新型有机p-三环类衍生物作为必需成分：其中X是选自下组的部分由以下组成：，其中R 1和R 2各自选自氢和甲基，R 1或R 2中的至少一个为氢。

5. 发明授权

US3944621A Pi-tricyclene derivatives and process for preparing pi-tricyclene derivatives 失效
标题翻译：皮质三环衍生物及其制备方法
公开(公告)号：US3944621A
公开(公告)日：1976-03-16
申请号：US556862
申请日：1975-03-10
申请人： Braja Dulal Mookherjee , Venkatesh Kamath , Edward J. Shuster
发明人： Braja Dulal Mookherjee , Venkatesh Kamath , Edward J. Shuster
IPC分类号： A23L27/20 , C07C1/32 , C07C47/115 , C07C49/115 , C07C49/21 , C11B9/00 , C11D9/44 , C07C45/21 , C07C45/00 , C07C49/61
CPC分类号： C11D9/444 , A23L27/203 , C07C1/328 , C07C47/115 , C07C49/115 , C07C49/21 , C11B9/0042 , C11D9/442 , C07C2103/64
摘要： A process for the preparation of a mixture of compounds of the structure ##SPC1##Is disclosed whereby a Pi-halotricyclene having the structure ##SPC2##Where Y is chloro, bromo or iodo is reacted with an alkali metal cyanide to prepare the corresponding nitrile; the nitrile is reacted with diisobutylaluminum hyhdride to prepare the corresponding aldehyde, a nortricycloekasantalal which is then condensed with butanone to prepare the above mentioned mixture of compounds. Also claimed are the product ketones which are useful for altering the aroma of consumable products including perfumes, perfume compositions and perfumed articles.
摘要翻译：一种制备结构化合物的混合物的方法，其中包括具有Y为氯，溴或碘的结构的靛红三环与碱金属氰化物反应以制备相应的腈; 腈与二异丁基铝化合物反应以制备相应的醛，一种北方环己酮，然后与丁酮缩合以制备上述化合物的混合物。还要求的是产品酮，其可用于改变消费品的香气，包括香料，香料组合物和香料制品。

6. 发明授权

US4120308A Substituted norbornane derivatives used in the process of flavoring tobacco and the product thereof 失效
标题翻译：用于调味烟草及其制品过程中的取代的降冰片烷衍生物
公开(公告)号：US4120308A
公开(公告)日：1978-10-17
申请号：US860134
申请日：1977-12-13
申请人： Kenneth K. Light , James Milton Sanders , Manfred Hugo Vock , Edward J. Shuster , Joaquin Vinals , William L. Schreiber , John B. Hall , Denis E. Hruza, Sr. , Venkatesh Kamath , Braja Dulal Mookherjee , Ching Y. Tseng , Mark A. Sprecker
发明人： Kenneth K. Light , James Milton Sanders , Manfred Hugo Vock , Edward J. Shuster , Joaquin Vinals , William L. Schreiber , John B. Hall , Denis E. Hruza, Sr. , Venkatesh Kamath , Braja Dulal Mookherjee , Ching Y. Tseng , Mark A. Sprecker
IPC分类号： A23L27/20 , A24B15/34 , A24D3/14 , C07C29/09 , C07C29/17 , C07C29/40 , C07C29/42 , C07C29/68 , C07C31/137 , C07C33/12 , C07C45/29 , C07C45/30 , C07C45/58 , C07C45/62 , C07C45/66 , C07C45/67 , C07C45/68 , C07C45/74 , C07C49/323 , C07C49/35 , C07C49/557 , C07C49/577 , C07D301/14 , C07D303/04 , C11B9/00 , C11D3/50 , C11D9/44 , A24B3/12
CPC分类号： C11D3/0084 , A23L27/203 , A24B15/345 , A24D3/14 , C07C29/09 , C07C29/17 , C07C29/40 , C07C29/42 , C07C29/68 , C07C31/137 , C07C33/12 , C07D301/14 , C07D303/04 , C11B9/0046 , C11D3/50 , C11D9/442 , C07C2102/42 , Y10S514/974
摘要： The use of substituted norbornane derivatives used in the process of flavoring tobacco and the product thereof.
摘要翻译：在烟草调味过程中使用的取代的降冰片烷衍生物及其产物的用途。

7. 发明授权

US3977418A Tobacco article comprising the flavoring composition tricyclene-9-butenone and the process for making the same 失效
标题翻译：含有挥发性组合物三甲基-9-丁酮的烟草制品及其制备方法
公开(公告)号：US3977418A
公开(公告)日：1976-08-31
申请号：US556873
申请日：1975-03-10
申请人： Joaquin Francisco Vinals , Manfred Hugo Vock , Braja Dulal Mookherjee , Venkatesh Kamath
发明人： Joaquin Francisco Vinals , Manfred Hugo Vock , Braja Dulal Mookherjee , Venkatesh Kamath
IPC分类号： A24B15/34 , A24B3/12
CPC分类号： A24B15/345
摘要： Described is a process comprising adding to homogenized or reconstituted tobacco (for subsequent incorporation into smoking articles along with tobacco blend) an amount sufficient to alter the flavor or aroma of the ultimate tobacco mixture of tricyclene-9-butenone (1,7-dimethyl-7(1-pent-2-en-4-onyl) nortricyclene) having the structure: ##SPC1##

8. 发明授权

US3991123A Tetracyclic alcohols 失效
标题翻译：四环醇
公开(公告)号：US3991123A
公开(公告)日：1976-11-09
申请号：US614077
申请日：1975-09-17
申请人： Braja Dulal Mookherjee , Robert Walter Trenkle , Kenneth K. Light , Edward J. Shuster
发明人： Braja Dulal Mookherjee , Robert Walter Trenkle , Kenneth K. Light , Edward J. Shuster
IPC分类号： C11B9/00 , C07C35/22
CPC分类号： C07C35/37 , C07C35/44 , C11B9/0042 , C07C2103/66 , C07C2103/86
摘要： Described is a genus of novel compounds, defined by the generic structure: ##SPC1##Wherein n is 0 or 1 and X is selected from the group consisting of 1,2-cyclo-propylene having the structure: ##SPC2##And 1,2-ethenylene having the structure: ##SPC3##X being cyclopropylene when n is 1, useful for altering, enhancing, modifying or imparting an aroma of or to consumable products including perfumes, perfume comositions and perfumed articles.
摘要翻译：描述了由通用结构定义的新型化合物属：

9. 发明授权

US4040987A 2-Alkyl-substituted-4,5-dimethyl thiazoline perfume and cologne compositions 失效
标题翻译： 2-烷基取代-4,5-二甲基噻唑啉香料和古龙水组合物
公开(公告)号：US4040987A
公开(公告)日：1977-08-09
申请号：US730653
申请日：1976-10-07
申请人： Edward J. Shuster , Donald Arthur Withycombe , Braja Dulal Mookherjee , Cynthia J. Mussinan
发明人： Edward J. Shuster , Donald Arthur Withycombe , Braja Dulal Mookherjee , Cynthia J. Mussinan
IPC分类号： C07D277/10 , C11B9/00
CPC分类号： C11D3/0084 , C07D277/10 , C11B9/0096
摘要： Perfume and fragrance compositions and perfumed articles including soaps, detergents, powders, as well as colognes containing 2-alkyl-substituted-4,5-dimethyl thiazolines having the structure: ##STR1## wherein R.sub.1 and R.sub.3 are the same or different, and each is selected from the group consisting of methyl and hydrogen, which impart thereto chocolate-like, fresh ground coffee-like, green, cucumber, dill aromas and yielding on dry-out floral, natural tuberose-like, orris-like nuances.
摘要翻译：香料和香料组合物和香料制品，包括皂，洗涤剂，粉末，以及含有2-烷基取代的-4,5-二甲基噻唑类的古龙香，其结构如下：其中R1和R3相同或不同，选自由甲基和氢组成的组，其赋予巧克力样，新鲜研磨的咖啡状，绿色，黄瓜，莳萝香气，并且产生干燥的花卉，天然晚香玉样，或棱镜状的细微差别。

10. 发明授权

US3996296A Novel compounds, 4-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl)-2-butanol and 4-(6,6-dimethyl-2-methylene-3-cyclohexen-1-yl)-2-butanol 失效
标题翻译： 4-（2,6,6-三甲基-1,3-环己二烯-1-基）-2-丁醇和4-（6,6-二甲基-2-亚甲基-3-环己烯-1-基） -2-丁醇
公开(公告)号：US3996296A
公开(公告)日：1976-12-07
申请号：US561187
申请日：1975-03-24
申请人： Braja Dulal Mookherjee , Manfred Hugo Vock , Carlos Benaim , Edward J. Shuster
发明人： Braja Dulal Mookherjee , Manfred Hugo Vock , Carlos Benaim , Edward J. Shuster
IPC分类号： A23L27/20 , C11B9/00 , C07C31/13
CPC分类号： C11B9/0034 , A23L27/203
摘要： Described are the novel compounds, 4-(2,6,6-trimethyl-1,3-cyclohexadien-1-yl)-2-butanol and 4-(6,6-dimethyl-2-methylene-3-cyclohexen-1-yl)-2-butanol, and processes for preparing the aforementioned alcohols and acetate esters thereof.
摘要翻译：描述了新化合物4-（2,6,6-三甲基-1,3-环己二烯-1-基）-2-丁醇和4-（6,6-二甲基-2-亚甲基-3-环己烯-1 - 基）-2-丁醇，以及制备上述醇及其乙酸酯的方法。

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