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1. 发明授权

US4647403A Ion implanted polydiacetylenes 失效
标题翻译：离子注入聚二乙炔
公开(公告)号：US4647403A
公开(公告)日：1987-03-03
申请号：US630484
申请日：1984-07-13
申请人： Boris S. Elman , Daniel J. Sandman , Sukant K. Tripathy , Mrinal K. Thakur
发明人： Boris S. Elman , Daniel J. Sandman , Sukant K. Tripathy , Mrinal K. Thakur
IPC分类号： C08F8/00 , C08L49/00 , H01B1/12 , H01L51/30 , H01B1/06
CPC分类号： H01B1/125 , C08F8/00 , C08L49/00 , H01L51/004
摘要： Ion implanted polydiacetylenes prepared by implanting ions into substituted polydiacetylenes at fluence levels from about 1.times.10.sup.13 ions/cm.sup.2 to about 1.times.10.sup.17 ions/cm.sup.2 are disclosed. Ion implanted polydiacetylenes exhibit electrical and/or optical properties which are different from those of untreated polydiacetylenes.
摘要翻译：公开了通过以约1×10 13离子/ cm 2至约1×10 17离子/ cm 2的注量水平将离子注入取代的聚二乙炔中制备的离子注入的聚二乙炔。离子注入的聚二乙炔表现出不同于未处理的聚二乙炔的电学和/或光学性质。

2. 发明授权

US4698121A Methods for the preparation of oriented thin large-area single crystals of diacetylenes and polydiacetylenes 失效
标题翻译：制备二乙炔和聚二乙炔取向薄的大面积单晶的方法
公开(公告)号：US4698121A
公开(公告)日：1987-10-06
申请号：US705586
申请日：1985-02-26
申请人： Mrinal K. Thakur , Sukant K. Tripathy , Daniel J. Sandman
发明人： Mrinal K. Thakur , Sukant K. Tripathy , Daniel J. Sandman
IPC分类号： C30B11/00
CPC分类号： C30B11/00 , Y10S117/919
摘要： Methods for preparing thin large-area single crystals of diacetylenes and polydiacetylenes having surface dimensions greater than or equal to about 0.1 mm on all sides and a uniform thickness less than or equal to about 100 microns. The methods involve forming a liquid layer, preferably by melting crystals of a pure diacetylene monomer between two opposed surfaces, one surface being movable with respect to the other; applying pressure to the molten monomer layer disposed between the two surfaces; shearing the molten layer by sliding the movable surface in a single direction that is in a straight line across the molten monomer layer while keeping the molten monomer layer under constant pressure; and crystallizing the shorn molten monomer layer while the shorn molten monomer layer is kept under constant pressure to form a thin large-area single crystal of pure diacetylene monomer. The method for preparing thin large-area single crystals of polydiacetylene further involves exposing a surface of the thin large-area single crystal of diacetylene monomer to ultraviolet or gamma radiation to form a thin large-area single crystal of polydiacetylene.
摘要翻译：制备表面尺寸大于或等于约0.1mm的薄壁大面积单面二乙炔和聚二乙炔的方法，均匀厚度小于或等于约100微米。所述方法包括形成液体层，优选通过在两个相对的表面之间熔化纯双乙炔单体的晶体，一个表面可相对于另一表面移动; 向设置在两个表面之间的熔融单体层施加压力; 通过使可动表面沿着熔融单体层的直线的单一方向滑动，同时使熔融单体层保持恒定的压力来剪切熔融层; 并在将熔融的单体层保持在恒定压力下，使已熔融的单体层结晶，形成纯的乙炔单体薄的大面积单晶。制备聚二乙炔薄的大面积单晶的方法还包括将薄的大面积单乙炔单体的表面暴露于紫外线或γ射线以形成薄的大面积单二聚乙炔单晶。

3. 发明授权

US4793893A Methods for the preparation of thin large-area single crystals of diacetylenes and polydiacetylenes 失效
标题翻译：制备二乙炔和聚二乙炔的薄大面积单晶的方法
公开(公告)号：US4793893A
公开(公告)日：1988-12-27
申请号：US46499
申请日：1987-05-07
申请人： Mrinal K. Thakur , Sukant K. Tripathy , Daniel J. Sandman
发明人： Mrinal K. Thakur , Sukant K. Tripathy , Daniel J. Sandman
IPC分类号： C30B7/00
CPC分类号： C30B7/00 , C30B29/54 , C30B29/58 , C30B7/005
摘要： A method for preparing thin large-area single crystals of diacetylene monomer represented by the formula:R--C.tbd.C--C.tbd.C--R'wherein R and R' are side groups selected such that the diacetylene monomer is polymerizable by a 1,4-addition solid state reaction upon exposure to actinic radiation. The method involves forming a liquid layer containing pure diacetylene monomer between two opposed surfaces; applying pressure to the liquid layer disposed between the two opposed surfaces; and crystallizing the liquid layer disposed between the two opposed surfaces while by evaporation the liquid layer is kept under constant pressure to form a thin large-area single crystal of pure diacetylene monomer.A method for preparing thin large-area single crystals of polydiacetylene is also provided. The method further involves exposing a surface of a thin large-area single crystal of diacetylene monomer to ultraviolet or gamma radiation to form a thin large-area single crystal of polydiacetylene.
摘要翻译：制备由式：RC 3BOND CC 3BOND CR'表示的双乙炔单体的薄的大面积单晶的方法，其中R和R'是选择的侧基，使得二乙炔单体可通过1,4-加成固相反应暴露于光化辐射。该方法包括在两个相对的表面之间形成含有纯双乙炔单体的液体层; 对设置在两个相对表面之间的液体层施加压力; 并且通过蒸发使配置在两个相对表面之间的液体层结晶，将液体层保持在恒定压力下，形成纯的双乙炔单体的薄的大面积单晶。还提供了制备聚二乙炔薄的大面积单晶的方法。该方法还包括将薄的大面积单乙炔单体的表面暴露于紫外或γ射线以形成薄的大面积单二聚乙炔单晶。

4. 发明授权

US4684434A Method for the preparation of thin large-area single crystals of diacetylenes and polydiacetylenes 失效
标题翻译：制备二乙炔和聚二乙炔的薄大面积单晶的方法
公开(公告)号：US4684434A
公开(公告)日：1987-08-04
申请号：US705587
申请日：1985-02-26
申请人： Mrinal K. Thakur , Sukant K. Tripathy , Daniel J. Sandman
发明人： Mrinal K. Thakur , Sukant K. Tripathy , Daniel J. Sandman
IPC分类号： C30B7/00
CPC分类号： C30B7/00 , C30B29/54 , C30B29/58 , C30B7/005 , Y10S117/919
摘要： A method for preparing thin large-area single crystals of diacetylene monomer represented by the formula:R--CX.tbd.C--C.tbd.C--R'wherein R and R' are side groups selected such that the diacetylene monomer is polymerizable by a 1,4-addition solid state reaction upon exposure to actinic radiation, is provided. The method involves forming a liquid layer containing pure diacetylene monomer between two opposed surfaces; applying pressure to the liquid layer disposed between the two opposed surfaces; and crystallizing the liquid layer disposed between the two opposed surfaces while the liquid layer is kept under constant pressure to form thin large-area single crystals of pure diacetylene monomer.A method for preparing thin large-area single crystals of polydiacetylene is also provided. The method involves forming a liquid layer containing diacetylene monomer represented by the formula:R--C.tbd.C--C.tbd.C--R'wherein R and R' are side groups selected such that the diacetylene monomer is polymerizable by a 1,4-addition solid state reaction upon exposure to actinic radiation in pure form between two opposed surfaces; applying pressure to the liquid layer disposed between the two opposed surfaces; crystallizing the liquid layer disposed between the two opposed surfaces while the liquid layer is kept under constant pressure to form thin large-area single crystals of pure diacetylene monomer; and exposing a surface of the thin large-area single crystal of diacetylene monomer to ultraviolet or gamma radiation to form thin large-area single crystals of polydiacetylene.
摘要翻译：制备由下列通式表示的双乙炔单体的薄的大面积单晶的方法：R-CX 3BOND CC 3BOND CR'其中R和R'是选择的侧基，使得乙炔单体可通过1,4-加成固体提供了暴露于光化辐射的状态反应。该方法包括在两个相对的表面之间形成含有纯双乙炔单体的液体层; 对设置在两个相对表面之间的液体层施加压力; 并且在液体层保持恒定压力的同时使设置在两个相对表面之间的液体层结晶，形成纯的乙炔单体的薄的大面积单晶。还提供了制备聚二乙炔薄的大面积单晶的方法。该方法包括形成含有由下式表示的乙炔单体的液体层：RC 3BOND CC 3BOND CR'，其中R和R'是选择的侧基，使得双乙炔单体可通过暴露于1,4-加成固相反应而可聚合在两个相对表面之间的纯粹形式的光化辐射; 对设置在两个相对表面之间的液体层施加压力; 在液体层保持恒定压力的同时使设置在两个相对表面之间的液体层结晶，形成纯的大面积纯双乙炔单体的单晶; 并将该乙炔单体的薄的大面积单晶的表面暴露于紫外线或γ射线以形成多个大面积的聚二乙炔的大面积单晶。

5. 发明授权

US5846753A Chemiluminescence-based method for rapid and sensitive in-situ detection of organophosphorus compounds and metal ions 失效
标题翻译：基于化学发光的方法，用于快速和灵敏地原位检测有机磷化合物和金属离子
公开(公告)号：US5846753A
公开(公告)日：1998-12-08
申请号：US445565
申请日：1995-05-30
申请人： Joseph A. Akkara , David L. Kaplan , Madhu S. R. Ayyagari , Kenneth A. Marx , Sanjay Kamtekar , Rajiv Pande , Sukant K. Tripathy , Jayant Kumar
发明人： Joseph A. Akkara , David L. Kaplan , Madhu S. R. Ayyagari , Kenneth A. Marx , Sanjay Kamtekar , Rajiv Pande , Sukant K. Tripathy , Jayant Kumar
IPC分类号： C12Q1/42 , C07D305/14 , C12Q1/44
CPC分类号： C12Q1/42 , C12Q2334/00
摘要： A method of detecting the presence of a substance being monitored in a medium, selected from the group of substances including organophosphorus compounds and the metal ions Zn, Be and Bi, including the steps of: providing a 1,2-dioxetane phenyl phosphate compound; providing a phosphatase that catalytically degrades the 1,2-dioxetane phenyl phosphate compound to produce light, the catalytic activity of the phosphatase toward 1,2-dioxetane phenyl phosphate compound being altered by the substance being monitored; exposing the 1,2-dioxetane phenyl phosphate compound and the phosphatase together to a medium which may contain the substance being monitored; detecting light produced after the exposing step; and determining, from the detected light, the presence and concentration in the medium of the substance being monitored.
摘要翻译：一种检测在包括有机磷化合物和金属离子Zn，Be和Bi的物质组中的介质中被监测物质的存在的方法，包括以下步骤：提供1,2-二氧环乙烷苯基磷酸酯化合物; 提供催化降解1,2-二氧杂环丁烷苯基磷酸酯化合物以产生光的磷酸酶，磷酸酯对正在监测的物质的1,2-二氧环乙烷苯基磷酸酯化合物的催化活性改变; 将1,2-二氧环乙烷苯基磷酸酯化合物和磷酸酶一起暴露于可能含有被监测物质的介质中; 检测曝光步骤后产生的光; 并且从检测到的光中确定被监测物质的介质中的存在和浓度。

6. 发明授权

US5433895A Silicon-containing networked non-linear optical compositions 失效
标题翻译：含硅网络非线性光学组合物
公开(公告)号：US5433895A
公开(公告)日：1995-07-18
申请号：US950398
申请日：1992-09-23
申请人： Ru J. Jeng , Yong M. Chen , Aloke K. Jain , Jayant Kumar , Sukant K. Tripathy
发明人： Ru J. Jeng , Yong M. Chen , Aloke K. Jain , Jayant Kumar , Sukant K. Tripathy
IPC分类号： G02F1/355 , G02F1/361 , F21V9/00
CPC分类号： G02F1/3555 , G02F1/361 , G02F1/3615
摘要： A nonlinear optical composition and a method of forming the nonlinear optical composition are disclosed. The nonlinear optical composition includes a silicon-containing component and a nonlinear optical component which causes the nonlinear optical composition to exhibit second order nonlinear optical polarization of electromagnetic radiation, such as light. The method includes forming a sol of the silicon-containing component and the nonlinear optical component of the composition. A gel is formed from the sol. The nonlinear optical component is then poled while the gel is exposed to conditions sufficient to cause formation of a nonlinear optical composition which exhibits second order nonlinear optical polarization of electromagnetic radiation.
摘要翻译：公开了非线性光学组合物和形成非线性光学组合物的方法。非线性光学组合物包括含硅组分和非线性光学组分，其使得非线性光学组合物显示诸如光的电磁辐射的二阶非线性光学偏振。该方法包括形成含硅组分的溶胶和该组合物的非线性光学组分。由溶胶形成凝胶。然后将非线性光学部件极化，同时将凝胶暴露于足以形成非线性光学组合物的条件，其呈现电磁辐射的二阶非线性光学偏振。

7. 发明授权

US5143828A Method for synthesizing an enzyme-catalyzed polymerized monolayer 失效
标题翻译：合成酶催化聚合单层的方法
公开(公告)号：US5143828A
公开(公告)日：1992-09-01
申请号：US815213
申请日：1991-12-31
申请人： Joseph A. Akkara , David L. Kaplan , Lynne A. Samuelson , Braja K. Mandal , Sukant K. Tripathy , Ferdinando F. Bruno , Kenneth A. Marx
发明人： Joseph A. Akkara , David L. Kaplan , Lynne A. Samuelson , Braja K. Mandal , Sukant K. Tripathy , Ferdinando F. Bruno , Kenneth A. Marx
IPC分类号： B05D1/20 , C08G61/10 , C08G73/02 , C12P7/22 , C12P13/00
CPC分类号： B82Y30/00 , B05D1/204 , B82Y40/00 , C08G61/10 , C08G73/0266 , C12P13/001 , C12P7/22
摘要： A method for synthesizing enzyme-catalyzed polymers using the Langmuir-Blodgett technique. In one embodiment, the process comprises spreading one or more enzyme-polymerizable monomers on a water-miscible solvent. The monomers are sufficiently surface active that they align themselves on the air-solvent interface. Next, pressure is applied to the interface to form a monolayer made up of the monomers. An enzyme is then introduced into the solvent, causing polymerization of the monomers in the monolayer. The polymeric monolayers produced by the present method are easier to process and have reduced cross-linking and branching as compared to similar polymers produced in bulk by enzyme-catalyzed reactions.
摘要翻译：使用Langmuir-Blodgett技术合成酶催化聚合物的方法。在一个实施方案中，该方法包括将一种或多种可酶聚合的单体铺在水混溶性溶剂上。单体具有足够的表面活性，使得它们自己在空气 - 溶剂界面上对准。接下来，向界面施加压力以形成由单体组成的单层。然后将酶引入溶剂中，引起单体在单层中的聚合。通过本发明方法制备的聚合物单层与通过酶催化反应在本体产生的类似聚合物相比更容易加工并且具有减少的交联和支化。

8. 发明授权

US6018018A Enzymatic template polymerization 失效
标题翻译：酶模板聚合
公开(公告)号：US6018018A
公开(公告)日：2000-01-25
申请号：US999542
申请日：1997-11-21
申请人： Lynne A. Samuelson , K. Shridhara Alva , Jayant Kumar , Sukant K. Tripathy
发明人： Lynne A. Samuelson , K. Shridhara Alva , Jayant Kumar , Sukant K. Tripathy
IPC分类号： C08G73/02 , H01B1/12 , C08G73/00
CPC分类号： C08G73/0266 , H01B1/128 , Y10S977/747
摘要： Polymers are formed enzymatically in the presence of an oligomeric or polymeric template. The method includes combining at least one redox monomer or, in some cases, a redox oligomer, with a template and an enzyme, such as horseradish peroxidase, to form a reaction mixture. The redox monomer or oligomer aligns along the template before or during the polymerization, the template thereby affecting at least one physical property of the resulting polymer, such as the molecular weight or shape of the polymer. In one embodiment, the template can be a polyelectrolyte or an optically active polymer.
摘要翻译：在低聚或聚合物模板存在下，酶促形成聚合物。该方法包括将至少一种氧化还原单体，或在一些情况下，将氧化还原低聚物与模板和酶如辣根过氧化物酶组合以形成反应混合物。氧化还原单体或低聚物在聚合之前或期间沿模板排列，从而影响所得聚合物的至少一种物理性能，例如聚合物的分子量或形状。在一个实施方案中，模板可以是聚电解质或旋光聚合物。

9. 发明授权

US5260004A Process of making Langmuir-Blodgett films having photo-electronic properties 失效
标题翻译：制作具有光电特性的Langmuir-Blodgett薄膜的工艺
公开(公告)号：US5260004A
公开(公告)日：1993-11-09
申请号：US802675
申请日：1991-12-02
申请人： Lynne A. Samuelson , David L. Kaplan , Kenneth A. Marx , Sukant K. Tripathy , Jayant Kumar
发明人： Lynne A. Samuelson , David L. Kaplan , Kenneth A. Marx , Sukant K. Tripathy , Jayant Kumar
IPC分类号： B05D1/20 , B29C41/12 , B29C67/24 , B29C41/02 , B29C71/02 , B29C71/04
CPC分类号： B82Y30/00 , B05D1/202 , B29C41/12 , B29C67/24 , B82Y40/00 , B29K2089/00
摘要： Langmuir-Blodgett films having photo-electronic properties and methods of making the same. The instant films may be made, for example, by spreading a mixture of one or more types of biotinylated lipids and one or more types of electrically-conductive lipids over a water-miscible liquid subphase. Conjugated molecules comprising a biotin-binding component made up of an avidin or streptavidin molecule or a fragment or derivative thereof having biotin-binding activity and a photodynamic proteinaceous component are then injected into the subphase. Because of the affinity between biotin and the biotin-binding component, the conjugated molecules bind to the biotinylated lipids. The air-subphase interface is then compressed, causing the biotinylated lipids and electrically-conductive lipids to form a monolayer thereat. In one embodiment, the biotin-binding component has biotin-binding sites available on its underside which may be used to bind biotinylated derivatives of one or more different species of photodynamic proteinaceous components and/or to build up a multilayered complex of biotin-binding molecules and functional proteinaceous components using biotinylated rigid or flexible couplers.
摘要翻译：具有光电特性的Langmuir-Blodgett薄膜及其制造方法。可以例如通过将一种或多种类型的生物素化脂质和一种或多种类型的导电脂质的混合物铺在水混溶液体相上来制备即时膜。然后将包含由具有生物素结合活性的抗生物素蛋白或链霉抗生物素蛋白分子或其片段或衍生物的生物素结合组分的结合分子和光动力学蛋白质组分注入到亚相中。由于生物素与生物素结合成分之间的亲和力，共轭分子与生物素化的脂质结合。然后将空气 - 亚相界面压缩，导致生物素化的脂质和导电脂质在其上形成单层。在一个实施方案中，生物素结合组分在其下侧具有可用的生物素结合位点，其可用于结合一种或多种不同种类的光动力蛋白质组分的生物素化衍生物和/或建立生物素结合分子的多层复合物和使用生物素化的刚性或柔性耦合剂的功能蛋白质组分。

10. 发明授权

US06569651B1 Enzymatic polymerization of anilines or phenols around a template 失效
标题翻译：苯胺或酚类在模板周围的酶聚合
公开(公告)号：US06569651B1
公开(公告)日：2003-05-27
申请号：US09334105
申请日：1999-06-16
申请人： Lynne A. Samuelson , Sukant K. Tripathy , Ferdinando Bruno , Ramaswamy Nagarajan , Jayant Kumar , Wei Liu
发明人： Lynne A. Samuelson , Sukant K. Tripathy , Ferdinando Bruno , Ramaswamy Nagarajan , Jayant Kumar , Wei Liu
IPC分类号： C12P1300
CPC分类号： C12P13/001 , C12P7/22 , Y10S435/817 , Y10S977/898
摘要： The micelle contains multiple units, each of which contains a hydrophobic part and a hydrophilic part. A preferred unit is dodecyl benzene sulfonic acid. Borate-containing electrolytes include trifluoroborate, trimethylborate and hydrobis(pyridine)boron. Enzymes include peroxidases such as horseradish peroxidase or lignin peroxidase, and laccase. Monomers include unsubstituted and substituted anilines and unsubstituted and substituted phenols. A method is provided for enzymatic polymerization which includes (1) obtaining a reaction mixture including a monomer, a template, and an enzyme; and (2) incubating the reaction mixture for a time and under conditions sufficient for the monomer to align along the template and polymerize to form a polymer-template complex. The template can be a micelle, a borate-containing electrolyte, or lignin sulfonate. The polymer-template complex may be conductive, and possesses exceptional electrical and optical stability, water solubility, and processibility, and can be used in applications such as light-weight energy storage devices (e.g., rechargeable batteries), electrolytic capacitors, anti-static and anti-corrosive coatings for smart windows, and biological sensors.
摘要翻译：胶束含有多个单元，每个单元含有疏水部分和亲水部分。优选的单元是十二烷基苯磺酸。含硼酸盐的电解质包括三氟硼酸盐，硼酸三甲酯和氢化双（吡啶）硼。酶包括过氧化物酶如辣根过氧化物酶或木质素过氧化物酶，以及漆酶。单体包括未取代的和取代的苯胺和未取代的和取代的酚。提供了一种用于酶促聚合的方法，其包括（1）获得包含单体，模板和酶的反应混合物; 和（2）将反应混合物温育一段时间并在足以使单体沿着模板排列的聚合物形成聚合物 - 模板复合物的条件下。模板可以是胶束，含硼酸盐的电解质或木质素磺酸盐。聚合物 - 模板复合物可以是导电的，并且具有优异的电和光学稳定性，水溶性和可加工性，并且可以用于诸如轻量储能装置（例如可再充电电池），电解电容器，防静电以及智能窗户和生物传感器的防腐涂料。

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