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1. 发明授权

US3794508A Modified alkali hexatitanate and process of producing same 失效
标题翻译：改性的阿拉基十六烷酸酯及其生产方法
公开(公告)号：US3794508A
公开(公告)日：1974-02-26
申请号：US3794508D
申请日：1972-09-29
申请人： BAYER AG
发明人： WINTER G , MANSMANN M
IPC分类号： C01G23/00 , B01J27/12 , C09C1/00 , C09C1/36
CPC分类号： B01J27/12 , C01P2002/52 , C09C1/36
摘要： MODIFIED FIBROUS ALKALI HEXATITANATES CHARACTERIZED BY A CONTENT OF POLYVALENT METAL IONS IN AN AMOUNT OF FROM 0.025 TO 30% BY WEIGHT OF METAL AND BY A CONTENT OF FLUORINE IONS IN AN AMOUNT OF FROM 0.05 TO 10% BY WEIGHT OF FLUORINE, BASED ON THE WEIGHT OF TITANIUM DIOXIDE IN THE ALKALI METAL HEXATITANATE, AND PROCESS OF PRODUCING SAME BY REACTING A TITANIUM COMPOUND WITH AN ALKALI METAL COMPOUND WHICH REACTS BASICALLY IN THE PRESENCE OF A MINERALIZER AT A TEMPERATURE OF FROM 700 TO 1200* C. AND IN THE PRESENCE OF A POLYVALENT METAL FLUORIDE IN AN AMOUNT OF 0.1 TO 15% BY WEIGHT, BASED ON THE WEIGHT OF THE DRY REACTION MIXTURE, AND THE UTILITY THEREOF AS PIGMENTS, INSULATING MATERIALS, CATALYSTS AND CATALYST SUPPORTS.

2. 发明授权

US3794507A Modified alkali metal hexatitanate and process of producing same 失效
标题翻译：改性的碱金属十六烷酸酯及其生产方法
公开(公告)号：US3794507A
公开(公告)日：1974-02-26
申请号：US3794507D
申请日：1972-09-26
申请人： BAYER AG
发明人： WINTER G , MANSMANN M
IPC分类号： C01G23/00 , B01J23/04 , B01J35/06 , C09C1/00 , C09C1/36
CPC分类号： C09C1/36 , B01J23/04 , B01J35/06 , C01P2002/52
摘要： FIBROUS MODIFIED ALKALI METAL HEXATITANATES CHARACTERIZED BY A CONTENT OF POLYVALENT METAL IONS IN AN AMOUNT OF FROM 0 TO 10% BY WEIGHT OF POLYVALENT METAL AND BY A CONTENT OF PHOSPHATE AND/OR ARSENATE IONS IN AN AMOUNT OF FROM 0.02 TO 5% BY WEIGHT OF P2O5 AND/OR AS2O5, BASED ON THE WEIGHT OF TITANIUM DIOXIDE IN THE ALKALI METAL HEXATITANATE, AND PROCESS OF PRODUCING THE SAME BY REACTING A TITANIUM COMPOUND WITH AN ALKALI METAL COMPOUND WHICH REACTS BASICALLY, IN THE PRESENCE OF A MINERALIZER AT A TEMPERATURE OF FROM 700 TO 1200: C. AND IN THE PRESENCE OF PHOSPHATES AND/OR ARSENATES IN AN AMOUNT OF FROM 0.5 TO 10% BY WEIGHT, BASED ON THE WEIGHT OF THE DRY REACTION MIXTURE, AND THE UTILITY THEREOF AS PIGMENTS, INSULATING MATERIALS, CATALYSTS AND CATALYST SUPPORTS.

3. 发明授权

US3821070A Producing novel silicon dioxide fibers 失效
标题翻译：生产新型二氧化硅二氧化硅纤维
公开(公告)号：US3821070A
公开(公告)日：1974-06-28
申请号：US17038171
申请日：1971-08-09
申请人： BAYER AG
发明人： MANSMANN M , WINTER G
IPC分类号： C01B33/113 , C03C13/00 , C04B35/622 , D02G3/00 , C04B35/64
CPC分类号： C04B35/6224 , C01B33/113 , C03C13/005 , Y10S65/901 , Y10S264/19 , Y10T428/2913 , Y10T428/2918
摘要： Silicon dioxide fibers are produced by dry spinning a hydrolysis solution containing poly-lower alkylene oxide, especially polyethylene oxide of high molecular weight, the product preferably being post-heat treated to a temperature of about 200* to 1,500*C at a controlled rate of heating either in an oxygen containing or in an inert atmosphere to produce novel fibers as characterized by physical properties and amorphous Xray diagram. The hydrolysis is effected with less than about 3 moles of water per mole of alkoxy group contained in a tetraalkoxysilane or alkoxypolysiloxane and in the presence of a small amount of hydrochloric acid and a lower alkanol solubilizing agent.

4. 发明授权

US3846527A Production of inorganic fibers 失效
标题翻译：无机纤维生产
公开(公告)号：US3846527A
公开(公告)日：1974-11-05
申请号：US24745772
申请日：1972-04-25
申请人： BAYER AG
发明人： WINTER G , MANSMANN M , SCHON N , SCHNORING H
IPC分类号： D01F9/08 , C04B35/622 , D01F1/10 , D01F9/00 , C04B35/64
CPC分类号： C04B35/62227 , C04B35/62231 , Y10S65/901 , Y10S264/19
摘要： Inorganic fibers are produced by dry-spinning a solution, sol or dispersion of one or more metal compounds which would not normally be spinnable but which is rendered spinnable by inclusion of a small amount of a linear polymeric substance. The resulting fibers are subsequently heated to convert the metal compound to the oxide, carbide or nitride and to produce oxide, carbide or nitride fibers. The linear polymeric substance is characterized by a degree of polymerization in excess of 2,000 and is dissolved in the spinning dope in a concentration of 0.001 to 5 percent by weight.
摘要翻译：无机纤维通过将一种或多种金属化合物的溶液，溶胶或分散体进行干纺来制造，所述金属化合物通常不会是可纺的，但是通过包含少量线性聚合物质可以纺丝。随后加热所得纤维以将金属化合物转化为氧化物，碳化物或氮化物，并生成氧化物，碳化物或氮化物纤维。线性聚合物的特征在于聚合度超过2000，并以0.001至5重量％的浓度溶解在纺丝原液中。

5. 发明授权

US3760068A Production of fibrous alkali metal hexatitanates 失效
标题翻译：生产金属碱金属十六烷基硫酸盐
公开(公告)号：US3760068A
公开(公告)日：1973-09-18
申请号：US3760068D
申请日：1971-03-23
申请人： BAYER AG
发明人： WINTER G , ZIRNGIBL H , MANSMANN M
IPC分类号： C01G23/00 , C04B35/622 , D01F9/08
CPC分类号： C04B35/62231 , C01G23/005 , C01P2004/10 , C01P2004/54 , C01P2004/61
摘要： In the manufacture of fibrous, water-insoluble alkali metal hexatitanates of the composition Me2Ti6O13, wherein Me is an alkali metal except lithium by reaction of TiO2 with an alkali metal compound which gives a basic reaction under the reaction conditions, the improvement which comprises effecting the reaction in a sulfate melt at a temperature up to about 1,300*C. The sulfate melt is preferably an alkali metal sulfate. The TiO2 may be formed in situ by addition of some other titanium compound. The alkali metal compound preferably comprises sodium, potassium, rubidium or caesium and, expressed as the oxide, is present in about one-half to one-sixth the molar amount of the TiO2.
摘要翻译：在制备组合物Me2Ti6O13的纤维状，不溶于水的碱金属六钛酸盐时，其中Me是通过TiO 2与在反应条件下产生碱性反应的碱金属化合物的反应而除了锂之外的碱金属，其改进包括影响在高达约1300℃的温度下在硫酸盐熔体中反应。硫酸盐熔体优选为碱金属硫酸盐。可以通过添加一些其它钛化合物原位形成TiO 2。碱金属化合物优选包含钠，钾，铷或铯，并且以氧化物的形式表现为钛的摩尔量的约二分之一至六分之一。

6. 发明授权

US3723609A Process for the production of carbon fibers 失效
标题翻译：生产碳纤维的工艺
公开(公告)号：US3723609A
公开(公告)日：1973-03-27
申请号：US3723609D
申请日：1970-10-07
申请人： BAYER AG
发明人： MANSMANN M , WINTER G , PAMPUS G , SCHON N
IPC分类号： D01F9/16 , D01F9/17 , D01F9/18 , D01F9/21 , D01F9/24 , D01F9/26 , D01F9/28 , C01B31/07
CPC分类号： D01F9/18 , D01F9/16 , D01F9/17 , D01F9/21 , D01F9/24 , D01F9/245 , D01F9/26 , D01F9/28 , Y10S264/19
摘要： In the production of carbon fibers wherein a carbon-containing fiber-forming material is spun as a solution, the spun-filaments are converted to solid fibrous material, and the fibrous material is carbonized, the improvement which comprises including in said solution at least one fiber-forming high polymer at a concentration of about 0.001 to 10 percent by weight and a greater amount of a carbon source comprising at least one carboncontaining organic material having a softening or melting point in excess of about 80* C., whereby the solution of said carbon containing material is rendered spinnable by addition of said fiber-forming high polymer, said carbon containing organic material serving as the source of carbon for the carbon fiber; the fiber may thereafter be graphitized. The spinning solution used for fiber production is preferably a solution in a volatile solvent so that it may be dry spun. The carbon source in said solvent by itself would not be spinnable and may be a monomer or low polymer.
摘要翻译：在其中将含碳纤维形成材料作为溶液纺丝的碳纤维的生产中，纺丝长丝被转化为固体纤维材料，并且纤维材料被碳化，其改进包括在所述溶液中包含至少一种浓度为约0.001至10重量％的纤维形成高聚物和更大量的包含至少一种软化点或熔点超过约80℃的含碳有机材料的碳源，由此，所述含碳材料的溶液通过加入所述形成纤维的高分子，所述含碳有机材料作为碳纤维的碳源，使其可纺丝; 之后纤维可被石墨化。用于纤维生产的纺丝溶液优选是挥发性溶剂中的溶液，使其可以是干纺的。所述溶剂中的碳源本身不可纺，可以是单体或低聚物。

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