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1. 发明授权

US4064190A Removal of acetylenic contaminants by copper-tin and/or lead zinc aluminate 失效
标题翻译：用铜锡和/或铅酸铅锌去除炔属污染物
公开(公告)号：US4064190A
公开(公告)日：1977-12-20
申请号：US751499
申请日：1976-12-17
申请人： Alan D. Eastman , Floyd Farha, Jr.
发明人： Alan D. Eastman , Floyd Farha, Jr.
IPC分类号： C07C7/148 , C07C7/00
CPC分类号： C07C7/148 , Y02P20/584
摘要： Acetylenic compounds are selectively removed by conversion to innocuous materials by contacting hydrocarbon mixtures containing same with a copper-tin and/or lead-zinc aluminate catalyst. In one embodiment, acetylenic compounds are selectively removed from unsaturated hydrocarbon-containing mixtures in a cyclic process comprising alternate contact of the catalyst with a gaseous hydrocarbon phase containing acetylenic contaminants and thereafter of the catalyst with an oxygen-containing gas to regenerate the catalyst.
摘要翻译：通过将含有它们的烃混合物与铜 - 锡和/或铝酸铅 - 锌酸铅催化剂接触，通过转化成无害材料来选择性除去乙炔化合物。在一个实施方案中，炔属化合物以环状方法选择性地从不饱和烃混合物中除去，包括催化剂与含有炔属污染物的气态烃相的交替接触，此后用含氧气体再催化催化剂。

2. 发明授权

US07056744B2 Measurement of short chain branching in olefin copolymers using chemometric analysis 有权
标题翻译：使用化学计量分析测量烯烃共聚物中的短链支化
公开(公告)号：US07056744B2
公开(公告)日：2006-06-06
申请号：US10463849
申请日：2003-06-16
申请人： Paul J. DesLauriers , David C. Rohlfing , Alan D. Eastman , Eric T. Hsieh
发明人： Paul J. DesLauriers , David C. Rohlfing , Alan D. Eastman , Eric T. Hsieh
IPC分类号： G01N33/44 , G01N21/00
CPC分类号： G01N21/359 , G01N21/3577 , G01N2021/3595 , Y10T436/21
摘要： A method of determining the proportion of short-chain branching in an olefin copolymer process stream is disclosed. The short-chain branching may also be determined as a function of molecular weight in a sample having a range of molecular weights. In the method, at least two olefin copolymer training samples are provided. The respective samples have different, known proportions of short-chain branching. The infrared (e.g. FT-IR) absorbance spectra of the training samples in a wavenumber range are obtained. Calibration information is determined from the training samples by chemometrically correlating the differences in the infrared absorbance spectra of the training samples to the differences in the degree of short-chain branching in the training samples. This step generates calibration information that allows the degree of short-chain branching in a sample to be determined once its infrared absorbance spectrum is obtained. A method for determining the statistical error in the measurement of short-chain branching in an olefin polymer sample as a function of its molecular weight distribution is also disclosed.
摘要翻译：公开了一种确定烯烃共聚物工艺流中短链支化比例的方法。短链支化也可以在具有分子量范围的样品中作为分子量的函数来确定。在该方法中，提供至少两种烯烃共聚物训练样品。各样品具有不同的已知比例的短链支化。获得波数范围内训练样本的红外（例如FT-IR）吸收光谱。通过化学方法将训练样本的红外吸收光谱的差异与训练样本中短链分支程度的差异化学相关，从训练样本中确定校准信息。该步骤产生校准信息，其允许在获得样品的红链吸收光谱后测定样品中的短链支化度。还公开了用于确定烯烃聚合物样品中短链支化的测量中的统计误差作为其分子量分布的函数的方法。

3. 发明授权

US06632680B1 Measurement of short chain branching in olefin copolymers using chemometric analysis 有权
标题翻译：使用化学计量分析测量烯烃共聚物中的短链支化
公开(公告)号：US06632680B1
公开(公告)日：2003-10-14
申请号：US09667657
申请日：2000-09-22
申请人： Paul J. DesLauriers , David C. Rohlfing , Alan D. Eastman , Eric T. Hsieh
发明人： Paul J. DesLauriers , David C. Rohlfing , Alan D. Eastman , Eric T. Hsieh
IPC分类号： G01N3344
CPC分类号： G01N21/359 , G01N21/3577 , G01N2021/3595 , Y10T436/21
摘要： A method of determining the proportion of short-chain branching in an olefin copolymer process stream is disclosed. The short-chain branching may also be determined as a function of molecular weight in a sample having a range of molecular weights. In the method, at least two olefin copolymer training samples are provided. The respective samples have different, known proportions of short-chain branching. The infrared (e.g. FT-IR) absorbance spectra of the training samples in a wavenumber range are obtained. Calibration information is determined from the training samples by chemometrically correlating the differences in the infrared absorbance spectra of the training samples to the differences in the degree of short-chain branching in the training samples. This step generates calibration information that allows the degree of short-chain branching in a sample to be determined once its infrared absorbance spectrum is obtained. A method for determining the statistical error in the measurement of short-chain branching in an olefin polymer sample as a function of its molecular weight distribution is also disclosed.
摘要翻译：公开了一种确定烯烃共聚物工艺流中短链支化比例的方法。短链支化也可以在具有分子量范围的样品中作为分子量的函数来确定。在该方法中，提供至少两种烯烃共聚物训练样品。各样品具有不同的已知比例的短链支化。获得波数范围内训练样本的红外（例如FT-IR）吸收光谱。通过化学方法将训练样本的红外吸收光谱的差异与训练样本中短链分支程度的差异化学相关，从训练样本中确定校准信息。该步骤产生校准信息，其允许在获得样品的红链吸收光谱后测定样品中的短链支化度。还公开了用于确定烯烃聚合物样品中短链支化测量中的统计误差作为其分子量分布函数的方法。

4. 发明授权

US5276245A Alkylation catalyst regeneration 失效
标题翻译：烷基化催化剂再生
公开(公告)号：US5276245A
公开(公告)日：1994-01-04
申请号：US904938
申请日：1992-06-26
申请人： Alan D. Eastman , Ronald G. Abbott
发明人： Alan D. Eastman , Ronald G. Abbott
IPC分类号： B01J38/00 , B01D15/00 , B01J27/32 , B01J31/40 , B01J38/50 , C07B37/00 , C07B61/00 , C07C2/20 , C07C2/58 , C07C2/62 , C07C9/16
CPC分类号： B01J31/0222 , B01J31/4092 , B01J38/50 , C07C2/62 , B01J21/08 , B01J21/18 , B01J2231/4205 , B01J27/12 , C07C2527/1206 , Y02P20/584
摘要： Described is a novel acid-soluble oil composition produced as a by-product from an alkylation reaction catalyzed by a sulfone-containing catalyst. Also described is a novel process for regenerating an alkylation catalyst which contains a sulfone component.
摘要翻译：描述了一种由含有砜的催化剂催化的烷基化反应产生的作为副产物的新型酸溶性油组合物。还描述了一种用于再生含有砜成分的烷基化催化剂的新方法。

5. 发明授权

US5237122A Alkylation catalyst regeneration 失效
标题翻译：烷基化催化剂再生
公开(公告)号：US5237122A
公开(公告)日：1993-08-17
申请号：US935089
申请日：1992-08-24
申请人： Alan D. Eastman , Robert B. Eldridge , Richard L. Anderson , David P. Mann
发明人： Alan D. Eastman , Robert B. Eldridge , Richard L. Anderson , David P. Mann
IPC分类号： B01J31/02 , B01D17/00 , B01J31/40 , B01J38/00 , B01J38/48 , C07B61/00 , C07C2/20 , C07C2/58 , C07C2/62 , C07C9/16
CPC分类号： B01J31/4092 , B01J31/0222 , B01J38/48 , C07C2/62 , B01J2231/4205 , B01J2531/96 , B01J27/12 , C07C2527/1206 , Y02P20/584 , Y10S585/901
摘要： Disclosed is a process for removing acid soluble oils, produced as an undesirable by-product of an HF catalyzed alkylation reaction, from a liquid containing a sulfone compound. The process includes the use of water to induce the formation of the two immiscible liquid phases of ASO and sulfone with water. The two immiscible phases can subsequently be separated from each other.

6. 发明授权

US4370259A Oxidative dehydrogenation catalyst 失效
标题翻译：氧化脱氢催化剂
公开(公告)号：US4370259A
公开(公告)日：1983-01-25
申请号：US308980
申请日：1981-10-06
申请人： Alan D. Eastman , John H. Kolts
发明人： Alan D. Eastman , John H. Kolts
IPC分类号： B01J27/18 , C07C5/48 , B01J27/14 , B01J31/12
CPC分类号： B01J27/1802 , C07C5/48 , Y02P20/52
摘要： Hydrocarbons are oxidatively dehydrogenated in the presence of a catalyst comprising a mixture of oxides of manganese, phosphorus, and an alkali metal, optionally, supported on a refractory oxide. In one embodiment, ethane is converted to ethylene in the presence of a catalyst comprising a mixture of oxides of manganese, phosphorus, and sodium supported on alumina.
摘要翻译：在包含锰，磷和碱金属的氧化物的混合物的催化剂的存在下，碳氢化合物被氧化脱氢，任选负载在难熔氧化物上。在一个实施方案中，在包含负载在氧化铝上的锰，磷和钠的氧化物的混合物的催化剂存在下，将乙烷转化为乙烯。

7. 发明授权

US4327238A Dehydrogenation of organic compounds with a promoted zinc titanate catalyst 失效
标题翻译：用促进的钛酸锌催化剂脱氢有机化合物
公开(公告)号：US4327238A
公开(公告)日：1982-04-27
申请号：US125436
申请日：1980-02-28
申请人： Alan D. Eastman
发明人： Alan D. Eastman
IPC分类号： B01J23/06 , B01J23/10 , B01J23/12 , B01J23/18 , B01J23/26 , C07C5/333 , C07C5/32
CPC分类号： B01J23/26 , B01J23/06 , B01J23/10 , B01J23/12 , B01J23/18 , C07C5/3332 , Y02P20/52
摘要： The catalytic dehydrogenation of at least one dehydrogenatable organic compound which has at least one ##STR1## grouping is carried out in the presence of a zinc titanate catalyst. The selectivity of the zinc titanate catalyst is improved by at least one promoter selected from the group consisting of chromium oxide, antimony oxide, bismuth oxide, oxides of the lanthanides, oxides of the actinides, oxides thereof, and compounds convertible to the oxides thereof.
摘要翻译：具有至少一个组分的至少一种可脱氢有机化合物的催化脱氢在钛酸锌催化剂存在下进行。钛酸锌催化剂的选择性由选自氧化铬，氧化锑，氧化铋，镧系元素的氧化物，锕系元素的氧化物，氧化物和可转化为氧化物的化合物组成的组中的至少一种促进剂提高。

8. 发明授权

US06294078B1 Antifoulant control process 失效
标题翻译：防污染控制过程
公开(公告)号：US06294078B1
公开(公告)日：2001-09-25
申请号：US09611606
申请日：2000-07-07
申请人： Alan D. Eastman , Ronald E. Brown
发明人： Alan D. Eastman , Ronald E. Brown
IPC分类号： C01G916
CPC分类号： C10G75/04
摘要： A process is provided by the invention which comprises: (a) providing a tubular reactor having an inlet and an outlet, a furnace for heating the reactor, and a cooler having an inlet in communication with the reactor outlet and also having an outlet; (b) introducing a substantially constant flow of feed gas comprising steam to the reactor inlet while the reactor is heated by the furnace to produce a predetermined and substantially constant reactor outlet temperature; and (c) controlling, during at least a portion of (b), the concentration of an antifoulant in the feed gas based on cooler outlet temperature.
摘要翻译：本发明提供了一种方法，其包括：（a）提供具有入口和出口的管式反应器，用于加热反应器的炉子和具有与反应器出口连通并具有出口的入口的冷却器; （b）当反应器被炉加热以产生预定且基本上恒定的反应器出口温度时，将包含蒸汽的基本恒定的进料气流引入反应器入口; 和（c）在（b）的至少一部分期间基于较冷的出口温度来控制进料气体中防污剂的浓度。

9. 发明授权

US5347067A Alkylation catalyst regeneration 失效
标题翻译：烷基化催化剂再生
公开(公告)号：US5347067A
公开(公告)日：1994-09-13
申请号：US119861
申请日：1993-08-24
申请人： Alan D. Eastman , Ronald G. Abbott
发明人： Alan D. Eastman , Ronald G. Abbott
IPC分类号： B01J38/00 , B01D15/00 , B01J27/32 , B01J31/40 , B01J38/50 , C07B37/00 , C07B61/00 , C07C2/20 , C07C2/58 , C07C2/62 , C07C9/16
CPC分类号： B01J31/0222 , B01J31/4092 , B01J38/50 , C07C2/62 , B01J21/08 , B01J21/18 , B01J2231/4205 , B01J27/12 , C07C2527/1206 , Y02P20/584
摘要： Described is a novel acid-soluble oil composition produced as a by-product from an alkylation reaction catalyzed by a sulfone-containing catalyst. Also described is a novel process for regenerating an alkylation catalyst which contains a sulfone component. The regeneration process utilizes alumina adsorbent to remove a substantial portion of the hydrogen halide from the spent catalyst, thereby producing a neutralized stream, which is then treated with carbon to remove a substantial portion of the reaction by-product to produce a sulfone stream substantially free of reaction by-product and hydrogen halide.
摘要翻译：描述了一种由含有砜的催化剂催化的烷基化反应产生的作为副产物的新型酸溶性油组合物。还描述了一种用于再生含有砜成分的烷基化催化剂的新方法。再生方法利用氧化铝吸附剂从废催化剂中除去大部分的卤化氢，从而产生中和的流，然后用碳处理，以除去大部分反应副产物，从而产生基本上没有的砜流的反应副产物和卤化氢。

10. 发明授权

US5306859A Alkylation catalyst regeneration utilizing polyvinylpyridine and amine substituted styrene divinylbenzene copolymer contact materials 失效
标题翻译：使用聚乙烯吡啶和胺取代苯乙烯二乙烯基苯共聚物接触材料的烷基化催化剂再生
公开(公告)号：US5306859A
公开(公告)日：1994-04-26
申请号：US77142
申请日：1993-06-16
申请人： Alan D. Eastman , Ronald G. Abbott , Robert B. Eldridge
发明人： Alan D. Eastman , Ronald G. Abbott , Robert B. Eldridge
IPC分类号： B01J31/40 , C07C2/62
CPC分类号： B01J31/0222 , B01J31/4092 , B01J2231/4205 , B01J27/08 , B01J27/12 , B01J31/08
摘要： Described is a novel process for regenerating an ASO contaminated alkylation catalyst containing a sulfone component and a hydrogen halide component. A sulfone-containing mixture containing ASO and which is derived by the removal of a major portion of the hydrogen halide component of the alkylation catalyst is contacted with a reversable base selected from the group consisting of polyvinyl pyridine, amine-substituted styrene divinyl benzene copolymer and mixtures thereof so as to remove at least a portion of the ASO component from the sulfone-containing mixture to thereby produce a treated sulfone-containing mixture. The treated sulfone-containing mixture can further be processed by contacting it with an absorbent material which can include carbon and alumina.
摘要翻译：描述了一种用于再生含有砜组分和卤化氢组分的ASO污染的烷基化催化剂的新方法。含有ASO的含砜混合物，其通过除去烷基化催化剂的卤化氢组分的主要部分得到，与可选择的碱接触，所述可逆碱选自聚乙烯基吡啶，胺取代的苯乙烯二乙烯基苯共聚物和其混合物，以便从含砜混合物中除去至少一部分ASO组分，从而产生经处理的含砜混合物。经处理的含砜混合物可以通过与可包括碳和氧化铝的吸收材料接触来进一步加工。

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