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1. 发明授权

US4861612A Method of separating oleaginous matter into components having various melting points 失效
标题翻译：将含油物质分解成具有各种熔点的成分的方法
公开(公告)号：US4861612A
公开(公告)日：1989-08-29
申请号：US149733
申请日：1988-01-29
申请人： Akira Nakano , Hiroshi Higashioka , Masaki Nomura , Yoshiharu Kawahara , Ko Yamashita , Yoshito Sano , Minoru Kase
发明人： Akira Nakano , Hiroshi Higashioka , Masaki Nomura , Yoshiharu Kawahara , Ko Yamashita , Yoshito Sano , Minoru Kase
IPC分类号： C11B7/00
CPC分类号： C11B7/0091
摘要： Oleaginous material is fractionated into two fractions having different melting points from each other by emulsifying all the oleaginous material with water and using with a surfactant having an HLB value of 5 to 10 as an emulsifier, at a temperature at which all the oleaginous material is substantially melted. The emulsion is cooled to a temperature at which one fraction of the oleaginous material crystallizes so that the emulsion forms a lighter phase containing the other fraction of the oleaginous material and a heavier phase comprising an aqueous phase containing crystals of said first fraction dispersed therein. The lighter phase is separated from the heavier phase and then the crystals of the first fraction are separated from the remainder of the heavier phase.

2. 发明授权

US08927039B2 Method for manufacturing refined fat or oil 有权
标题翻译：制造精制脂肪或油的方法
公开(公告)号：US08927039B2
公开(公告)日：2015-01-06
申请号：US13516415
申请日：2010-12-14
申请人： Minoru Kase , Tetsuya Abe , Shinpei Fukuhara , Toshiteru Komatsu , Keiji Shibata
发明人： Minoru Kase , Tetsuya Abe , Shinpei Fukuhara , Toshiteru Komatsu , Keiji Shibata
IPC分类号： C11B3/10 , C11B3/14 , A23D9/02 , A23D7/02
CPC分类号： A23D7/02 , C11B3/10 , C11B3/14
摘要： Provided is a method for manufacturing refined fats and oils. Here fats and oils are brought into contact with an adsorbent and subsequently treated with water vapor under at least one condition of the following conditions. In condition I, the time for which the fats and oils are brought into contact with the water vapor in a temperature range of 175° C. to 205° C. for from 5 to 110 minutes. In condition 2, the fats and oils are brought into contact with the water vapor in a temperature range of 205° C. to 215° C. for from 5 to 50 minutes. In condition 3, the fats and oils are brought into contact with the water vapor in a temperature range of 215° C. to 230° C. for from 5 to 30 minutes.
摘要翻译：提供了一种制造精炼脂肪和油的方法。这里使脂肪和油与吸附剂接触，随后在至少一种以下条件的条件下用水蒸气处理。在条件I中，使脂肪和油在175℃至205℃的温度范围内与水蒸气接触的时间为5至110分钟。在条件2中，使油脂与水蒸汽在205〜215℃的温度范围内接触5〜50分钟。在条件3中，使油脂与水蒸气在215〜230℃的温度范围内接触5〜30分钟。

3. 发明申请

US20120259133A1 OIL OR FAT COMPOSITION 有权
标题翻译：油或脂肪组合物
公开(公告)号：US20120259133A1
公开(公告)日：2012-10-11
申请号：US13516560
申请日：2010-12-14
申请人： Rika Homma , Masao Shimizu , Junya Moriwaki , Minoru Kase , Tetsuya Abe , Shinpei Fukuhara , Toshiteru Komatsu , Keiji Shibata
发明人： Rika Homma , Masao Shimizu , Junya Moriwaki , Minoru Kase , Tetsuya Abe , Shinpei Fukuhara , Toshiteru Komatsu , Keiji Shibata
IPC分类号： C11C3/00
CPC分类号： A23D7/001 , A23D7/003 , A23D9/007 , A23D9/02 , C11B3/14
摘要： Provided is an oil or fat composition, which has an MCPD-FS content (ppm) of 13 ppm or less, the content being measured by a Deutsche Gesellschaft für Fettwissenschaft (DGF) standard method C-III 18(09), has a diacylglycerol content of 15 mass % or more, and is subjected to deodorization treatment.
摘要翻译：本发明提供一种油或脂肪组合物，其具有13ppm或更低的MCPD-FS含量（ppm），其含量由Deutsche GesellschaftfürFettwissenschaft（DGF）标准方法C-III 18（09）测量）具有二酰基甘油含量为15质量％以上，进行除臭处理。

4. 发明申请

US20050214914A1 Process for the production of diglycerides 有权
标题翻译：生产甘油二酯的方法
公开(公告)号：US20050214914A1
公开(公告)日：2005-09-29
申请号：US10499819
申请日：2002-12-27
申请人： Manabu Sato , Masami Shimizu , Jun Kohori , Minoru Kase , Takaaki Watanabe , Kazuhiro Onozuka
发明人： Manabu Sato , Masami Shimizu , Jun Kohori , Minoru Kase , Takaaki Watanabe , Kazuhiro Onozuka
IPC分类号： C12P7/62 , C12P7/64
CPC分类号： C12P7/6454 , C12P7/62
摘要： Provided is a preparation process of diglycerides which comprises reacting a fatty acid or lower alkyl ester thereof with glycerin in the presence of an immobilized partial glyceride lipase while removing water, which is generated upon reaction, out of the system. The reaction is preferably terminated when the acid value (AV) of the reaction mixture satisfies the following range: 50R-60>AV>70R-150 (with the proviso that AV>0). The present process makes it possible to efficiently prepare a high purity of diglycerides without impairing lipase activity even under reduced pressure. The present process is effective without being influenced by variations in reaction conditions such as fatty acid/glycerin ratio, reaction temperature or enzyme concentration. Particularly, even when the fatty acid/glycerin ratio is high, a high purity of diglycerides can be produced at a high reaction yield.
摘要翻译：提供了一种甘油二酯的制备方法，其包括在固定化的部分甘油酯脂肪酶的存在下使脂肪酸或其低级烷基酯与甘油反应，同时将反应后产生的水除去系统。当反应混合物的酸值（AV）满足以下范围：50R-60> AV> 70R-150（条件是AV> 0）时，反应优选终止。本方法使得即使在减压下也能有效地制备高纯度甘油二酯而不损害脂肪酶活性。本方法不受脂肪酸/甘油比，反应温度或酶浓度等反应条件的变化的影响而有效。特别是，即使脂肪酸/甘油的比例高，也能够以高的反应收率生产高纯度的甘油二酯。

5. 发明授权

US09006474B2 Method for producing refined a fat or oil 有权
标题翻译：生产精制脂肪或油的方法
公开(公告)号：US09006474B2
公开(公告)日：2015-04-14
申请号：US13635542
申请日：2011-02-25
申请人： Shinpei Fukuhara , Minoru Kase , Tetsuya Abe , Toshiteru Komatsu , Keiji Shibata
发明人： Shinpei Fukuhara , Minoru Kase , Tetsuya Abe , Toshiteru Komatsu , Keiji Shibata
IPC分类号： C11B3/04 , A23D9/013 , C11B3/00 , C11B3/14
CPC分类号： A23D9/013 , C11B3/001 , C11B3/04 , C11B3/14
摘要： A method for manufacturing a refined fat or oil, including: carrying out a first steam treatment of bringing a fat or oil into contact with water vapor; and subsequently carrying out a second steam treatment of bringing the fat or oil having a temperature lower by 10° C. or more than a temperature of the fat or oil in the first steam treatment into contact with water vapor in the presence of an organic acid.
摘要翻译：一种精制油脂的制造方法，其特征在于，包括：进行使油脂与水蒸气接触的第一蒸汽处理; 然后进行第二次蒸汽处理，使第一蒸汽处理中的脂肪或油的温度低于10℃或更高的脂肪或油，在有机酸存在下与水蒸气接触。

6. 发明授权

US08846963B2 Production process for refined fat or oil 有权
标题翻译：精制油脂的生产工艺
公开(公告)号：US08846963B2
公开(公告)日：2014-09-30
申请号：US13634895
申请日：2011-02-25
申请人： Testuya Abe , Minoru Kase , Shinpei Fukuhara , Toshiteru Komatsu , Keiji Shibata
发明人： Testuya Abe , Minoru Kase , Shinpei Fukuhara , Toshiteru Komatsu , Keiji Shibata
IPC分类号： C11B3/14 , C11B3/10 , C11B3/12 , A23D9/013 , C11B3/00
CPC分类号： A23D9/013 , C11B3/001 , C11B3/14
摘要： A method for manufacturing a refined fat or oil, including: carrying out a first steam treatment of bringing a fat or oil into contact with water vapor; subsequently carrying out a treatment of bringing the fat or oil into contact with an adsorbent; and further carrying out a second steam treatment of bringing the fat or oil having a temperature lower by 10° C. or more than a temperature of the fat or oil in the first steam treatment into contact with water vapor.
摘要翻译：一种精制油脂的制造方法，其特征在于，包括：进行使油脂与水蒸气接触的第一蒸汽处理; 随后进行使脂肪或油与吸附剂接触的处理; 进一步进行第二蒸汽处理，使第一蒸汽处理中的脂肪或油的温度低于10℃或更高的脂肪或油，使其与水蒸气接触。

7. 发明授权

US08323934B2 Process for producing fatty acids 有权
标题翻译：生产脂肪酸的方法
公开(公告)号：US08323934B2
公开(公告)日：2012-12-04
申请号：US12067245
申请日：2006-10-06
申请人： Minoru Kase , Toshiteru Komatsu
发明人： Minoru Kase , Toshiteru Komatsu
IPC分类号： C12N11/00 , C12N11/14 , C12N11/16 , C12P1/00 , C12P7/00 , C12P7/40 , C12P7/64
CPC分类号： C11C1/045 , C12P7/6418
摘要： A process for producing fatty acid by hydrolyzing oil and fat, which comprises: a first step of partially hydrolyzing oil and fat by either of the following method (a) or (b), and a second step of hydrolysis by the other method: (a) enzymatic hydrolysis using an immobilized enzyme which is an enzyme immobilized on a support and (b) high pressure and temperature hydrolysis. A method of efficiently producing fatty acid with a reduced content of trans-unsaturated fatty acid in the constituent fatty acids and having a good appearance with reduced coloring by hydrolysis of oil and fat is provided.
摘要翻译：一种通过水解油脂生产脂肪酸的方法，其包括：通过以下方法（a）或（b）之一部分水解油脂的第一步骤和通过其它方法水解的第二步骤：（ a）使用固定化酶（其是固定在载体上的酶）和（b）高压和高温水解的酶水解。提供了一种在构成脂肪酸中有效地生产具有降低的反式不饱和脂肪酸含量的脂肪酸的方法，并且具有外观良好，油脂脂肪水解降低着色的方法。

8. 发明授权

US06716610B2 Esterification or hydrolysis with substrate treated un-dried immobilized lipolytic enzyme 失效
标题翻译：用底物处理的未干燥的固定化脂肪分解酶进行酯化或水解
公开(公告)号：US06716610B2
公开(公告)日：2004-04-06
申请号：US09453078
申请日：1999-12-02
申请人： Masami Shimizu , Toshiteru Komatsu , Masao Shimizu , Minoru Kase
发明人： Masami Shimizu , Toshiteru Komatsu , Masao Shimizu , Minoru Kase
IPC分类号： C12P764
CPC分类号： C12P7/6418 , C12N11/08 , C12P7/6454
摘要： A lipolytic enzyme such as lipase is adsorbed on a porous anion-exchange resin carrier to obtain an immobilized enzyme without drying. The un-dried immobilized enzyme is contacted with a fat or oil for a time which may be about 2 hours to about 24 hours to stabilize the immobilized enzyme, and the immobilized enzyme is recovered from the fat or oil. The recovered immobilized enzyme is then used for esterifying or hydrolyzing a substrate. Water content of the un-dried immobilized enzyme may be 20% or more be weight such as 20-60%. Prior to immobilization, the resin carrier may be treated with a lypophylic aliphatic acid which preferably has 8 to 18 carbons.
摘要翻译：将脂肪酶等脂肪分解酶吸附在多孔阴离子交换树脂载体上，得到不干燥的固定化酶。将未干燥的固定化酶与脂肪或油接触约2小时至约24小时以稳定固定化酶的时间，并且从脂肪或油中回收固定化酶。然后将回收的固定化酶用于酯化或水解底物。未干燥固定化酶的含水量可以为20〜20重量％的20重量％以上。在固定之前，树脂载体可以用优选具有8至18个碳原子的脂环族脂族酸处理。

9. 发明授权

US08884043B2 Oil or fat composition 有权
标题翻译：油脂组成
公开(公告)号：US08884043B2
公开(公告)日：2014-11-11
申请号：US13516560
申请日：2010-12-14
申请人： Rika Homma , Masao Shimizu , Junya Moriwaki , Minoru Kase , Tetsuya Abe , Shinpei Fukuhara , Toshiteru Komatsu , Keiji Shibata
发明人： Rika Homma , Masao Shimizu , Junya Moriwaki , Minoru Kase , Tetsuya Abe , Shinpei Fukuhara , Toshiteru Komatsu , Keiji Shibata
IPC分类号： A23D9/00 , A23D7/00 , A23D9/007 , A23D9/02 , C11B3/14
CPC分类号： A23D7/001 , A23D7/003 , A23D9/007 , A23D9/02 , C11B3/14
摘要： Provided is an oil or fat composition, which has an MCPD-FS content (ppm) of 13 ppm or less, the content being measured by a Deutsche Gesellschaft für Fettwissenschaft (DGF) standard method C-III 18(09), has a diacylglycerol content of 15 mass % or more, and is subjected to deodorization treatment.
摘要翻译：本发明提供一种油或脂肪组合物，其具有13ppm或更低的MCPD-FS含量（ppm），其含量由Deutsche GesellschaftfürFettwissenschaft（DGF）标准方法C-III 18（09）测量）具有二酰基甘油含量为15质量％以上，进行除臭处理。

10. 发明申请

US20110206804A1 METHOD FOR PRODUCING DIACYLGLYCEROL-RICH FAT AND/OR OIL 审中-公开
标题翻译：生产二油酸镁和/或油的方法
公开(公告)号：US20110206804A1
公开(公告)日：2011-08-25
申请号：US12672285
申请日：2008-08-08
申请人： Minoru Kase , Toshiteru Komatsu
发明人： Minoru Kase , Toshiteru Komatsu
IPC分类号： C12P7/64 , C11C1/04
CPC分类号： C12P7/6454 , C11C1/08 , C11C3/02 , C12P7/6418
摘要： It is intended to provide a method for efficiently producing a diacylglycerol-rich fat and/or oil that has a low content of trans-unsaturated fatty acids and has a good color and a good flavor characteristic to diacylglycerols.A method for producing a diacylglycerol-rich fat and/or oil, by hydrolyzing a raw fat and/or oil by an enzymatic splitting method, and subjecting the fatty acids and glycerin obtained thereby to an esterification reaction, wherein a raw fat and/or oil containing undeodorized fat and/or oil in an amount of 50% by weight or more is used, and a deodorization treatment is carried out after the esterification reaction, to the extent that the relationship between the deodorization time (x) and the deodorization temperature (y) satisfies the following conditions (i) and (ii): y≧−2.59x+566 (i) y≦617x−0.0455 (provided that 475≦y≦563) (ii) wherein x represents the deodorization time (minutes), and y represents the deodorization temperature (K).
摘要翻译：旨在提供一种有效制备富含二酰基甘油的脂肪和/或油，其具有低含量的反式不饱和脂肪酸并且具有良好的颜色和对二酰基甘油的良好风味特性。一种生产富含二酰基甘油的脂肪和/或油的方法，其通过酶裂解方法水解原始脂肪和/或油，并使由其获得的脂肪酸和甘油进行酯化反应，其中将生的脂肪和/或使用含有50重量％以上的未脱臭脂肪和/或油的油，在酯化反应后进行除臭处理，除去除臭时间（x）与脱臭温度（y）满足以下条件（i）和（ii）：y≥-2.59x + 566（i）y＆nlE; 617x-0.0455（条件是475＆nlE; y＆nlE; 563）（ii）其中x表示除臭时间），y表示除臭温度（K）。

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