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1. 发明授权

US09388315B2 Fluorinated ether composition, its production method, coating liquid, and method for producing substrate having surface-treated layer 有权
标题翻译：氟化醚组合物，其制造方法，涂布液以及具有表面处理层的基材的制造方法
公开(公告)号：US09388315B2
公开(公告)日：2016-07-12
申请号：US14221609
申请日：2014-03-21
申请人： ASAHI GLASS COMPANY, LIMITED
发明人： Taiki Hoshino
IPC分类号： C09D5/00 , C09D4/00 , C08L71/00 , C08G65/00 , C09D5/16 , C09D171/02 , C08L71/02 , C09D171/00
CPC分类号： C09D5/1625 , C08G65/007 , C08G2650/48 , C08L71/00 , C08L71/02 , C09D4/00 , C09D5/1637 , C09D171/00 , C09D171/02
摘要： A fluorinated ether composition comprising at least two types of fluorinated ether compounds represented by A-O—RF—B, differing in group B, in a proportion of group (5-1) being from 90 to 95 mol % and a proportion of group (5-2) being from 5 to 10 mol % to the total amount of groups B. A is a C1-6 perfluoroalkyl group or B. RF is —(CF2CF2O)b(CF(CF3)CF2O)c(CF2O)d(CF2CF2CF2O)e—, and the binding order of repeating units is not limited. b, c, d and e are each independently an integer of at least 0, and b+c+d+e is from 5 to 150. —(CF2)aCFXCH2OCH2CH2CH2SiLmRn Group (5-1) —(CF2)aCFXCH2OCH2CH(SiLmRn)CH3 Group (5-2) —(CF2)aCFXCH2OCH2CH═CH2 Group (5-3) —(CF2)aCFXCH2OCH═CHCH3 Group (5-4) a is 0 or 1, X is F or CF3, L is a hydrolyzable group, R is a hydrogen atom or a monovalent hydrocarbon group, m is an integer of from 1 to 3, n is an integer of from 0 to 2, and m+n=3.
摘要翻译：包含由组（5-1）的比例不同的AO-RF-B所代表的至少两种氟化醚化合物的组合物（5-1）为90-95摩尔％和基团（5 -2（CF 2 CF 2 O）b（CF（CF 3）CF 2 O）c（CF 2 O）d（CF 2 CF 2 CF 2 O））e-，重复单元的结合顺序不受限制。 b，c，d和e各自独立地为至少为0的整数，b + c + d + e为5至150. - （CF 2）a CFXCH 2 OCH 2 CH 2 CH 2 SiLmR n（5-1） - （CF 2）a CFXCH 2 OCH 2 CH（SiLmRn） CH3（5-2） - （CF2）aCFXCH2OCH2CH=CH2组（5-3） - （CF2）aCFXCH2OCH = CHCH3组（5-4）a为0或1，X为F或CF3，L为可水解基团 R为氢原子或一价烃基，m为1〜3的整数，n为0〜2的整数，m + n = 3。

2. 发明申请

US20140287240A1 FLUORINATED ETHER COMPOUND, FLUORINATED ETHER COMPOSITION AND COATING LIQUID, AND SUBSTRATE HAVING SURFACE-TREATED LAYER AND METHOD FOR ITS PRODUCTION 有权
标题翻译：氟化醚化合物，氟化醚组合物和涂料液体，以及具有表面处理层的基材及其生产方法
公开(公告)号：US20140287240A1
公开(公告)日：2014-09-25
申请号：US14298267
申请日：2014-06-06
申请人： ASAHI GLASS COMPANY, LIMITED
发明人： Eisuke MUROTANI , Taiki Hoshino , Akira Isobe , Daisuke Shirakawa , Daisuke Jomuta , Nobuyuki Otozawa
IPC分类号： C09D7/12 , C23C14/12 , B05D1/02 , B05D1/28 , B05D1/18 , C07C43/12 , B05D1/00
CPC分类号： C09D7/63 , B05D1/005 , B05D1/02 , B05D1/18 , B05D1/28 , C07C43/126 , C07F7/1804 , C08G65/007 , C08G65/336 , C08G2650/48 , C09D5/1637 , C09D171/00 , C23C14/12 , Y10T428/31504
摘要： To provide a fluorinated ether compound, a fluorinated ether composition and a coating liquid, whereby it is possible to form a surface-treated layer which has high initial water/oil repellency and which is excellent in abrasion resistance and fingerprint stain removability, and a substrate having a surface-treated layer and a method for its production.A fluorinated ether compound which has a poly(oxyperfluoroalkylene) chain (αβ) having a C4 oxyperfluoroalkylene unit (α) and an oxyperfluoroalkylene unit (β) other than the unit (α) and which has a hydrolysable silyl group on at least one terminal of the poly(oxyperfluoroalkylene) chain (αβ) via a linking group.
摘要翻译：为了提供氟化醚化合物，氟化醚组合物和涂布液，由此可以形成具有高的初始拒水拒油性并且耐磨性和指纹污渍除去性优异的表面处理层，以及基材具有表面处理层及其制造方法。具有除了单元（α）之外的具有C4全氟亚烷基单元（α）和氧全氟亚烷基单元（＆bgr）的聚（全氟全氟亚烷基）链（α＆bgr））并且在至少一个上具有可水解甲硅烷基的氟化醚化合物通过连接基团的聚（全氟亚烷基）链（α和bgr）的末端。

3. 发明授权

US08754183B2 Water/oil repellent agent and water/oil repellent composition 有权
标题翻译：防水/防油剂和防水/防油剂组合物
公开(公告)号：US08754183B2
公开(公告)日：2014-06-17
申请号：US13693654
申请日：2012-12-04
申请人： Asahi Glass Company, Limited
发明人： Taiki Hoshino
IPC分类号： C08G18/28
CPC分类号： C09D5/00 , C07C235/84 , C07C275/42 , C08G18/2885 , C08G18/7621 , C08G18/7664 , C08G18/7671 , C08G18/7831 , C08G18/792 , C09D175/04 , D06M15/572 , D06M15/576 , D06M2200/11 , D06M2200/12
摘要： To provide a water/oil repellent agent and a water/oil repellent composition which are capable of imparting sufficient water/oil repellency to the surface of an article and which have low environmental impact. One comprising a reaction product obtained by reacting a fluorinated alcohol or amine having a polyfluoroalkyl moiety having at most 6 carbon atoms with a polyisocyanate compound, which is, when applied to an article, capable of imparting sufficient water/oil repellency, while presenting little environmental impact. When applied to an article, the water/oil repellent composition of the present invention is capable of imparting a high quality water/oil repellency to the article.
摘要翻译：提供一种能够赋予制品表面足够的防水/防油性且具有低环境影响性的拒水/拒油剂和斥水斥油剂组合物。一种包括通过使具有至多6个碳原子的多氟烷基部分的氟化醇或胺与多异氰酸酯化合物反应而得到的反应产物，当应用于制品时，能够赋予足够的斥水斥油性，同时呈现少量环境影响。当应用于制品时，本发明的斥水斥油剂组合物能够赋予制品高质量的斥水斥油性。

4. 发明申请

US20180148606A1 FLUORINATED ETHER COMPOUND, FLUORINATED ETHER COMPOSITION, COATING LIQUID AND ARTICLE 审中-公开
公开(公告)号：US20180148606A1
公开(公告)日：2018-05-31
申请号：US15877489
申请日：2018-01-23
申请人： Asahi Glass Company, Limited
发明人： Taiki Hoshino , Kiyotaka Takao , Kazue Toda , Kenji Ishizeki , Akira Isobe
IPC分类号： C09D201/04 , C09D201/10 , C08F259/08 , B32B33/00
CPC分类号： C09D201/04 , B32B33/00 , B32B2307/7265 , B32B2307/746 , C07F7/1804 , C08F259/08 , C08G65/007 , C08G65/329 , C08G65/336 , C09D171/00 , C09D201/10
摘要： To provide a fluorinated ether compound, a fluorinated ether composition and a coating liquid that are able to form a surface layer which is excellent in water/oil repellency, abrasion resistance, fingerprint stain removability, lubricity and outer appearance, and an article having such a surface layer. A fluorinated ether compound represented by A1—O—(Rf1O)m1-Q1-[C(O)N(R1)]p1—R11—C[—R12—SiR13n1X13−n1]3, wherein A1 is a C1-20 perfluoroalkyl group; Rf1 is a fluoroalkylene group having no branched structure; m1 is an integer from 2 to 210; Q1 is a single bond or a fluoroalkylene group having no branched structure; R1 is a hydrogen atom, etc.; p1 is 0 or 1; R11 is a single bond, an alkylene group, etc.; R12 is an alkylene group, etc.; R13 is a monovalent hydrocarbon group, etc.; X1 is a hydrolyzable group; and n1 is an integer of from 0 to 2.

5. 发明申请

US20180022851A1 FLUORINATED COMPOUND, PHOTOCURABLE COMPOSITION, COATING LIQUID, HARD COAT LAYER-FORMING COMPOSITION AND ARTICLE 审中-公开
公开(公告)号：US20180022851A1
公开(公告)日：2018-01-25
申请号：US15679246
申请日：2017-08-17
申请人： Asahi Glass Company, Limited
发明人： Kiyotaka Takao , Taiki Hoshino
IPC分类号： C08F290/06 , C09D151/08 , C08G18/50 , C08G18/79 , C08G18/28
CPC分类号： C08F290/067 , C08G18/2885 , C08G18/5015 , C08G18/672 , C08G18/792 , C08G18/8087 , C08G18/8175 , C09D151/08 , C09D175/16
摘要： To provide a fluorinated compound capable of imparting excellent antifouling properties (oily ink repellency and fingerprint-stain removability) and abrasion resistance of the antifouling properties to an object (such as a hard coat layer). It is a reaction product of a compound (a1) having a poly(oxyperfluoroalkylene) chain and one active hydrogen-containing group, a compound (a2) having a poly(oxyperfluoroalkylene) chain and two active hydrogen-containing groups, a compound (b) having a polymerizable carbon-carbon double bond and an active hydrogen-containing group, and a polyisocyanate (c), wherein the proportion of the portion derived from the compound (a1) to the total (100 mass %) of the portion derived from the compound (a1) and the portion derived from the compound (a2) is from 60 to 99.9 mass %.

6. 发明授权

US09738789B2 Method for producing silicon compound 有权
公开(公告)号：US09738789B2
公开(公告)日：2017-08-22
申请号：US15162908
申请日：2016-05-24
申请人： Asahi Glass Company, Limited
发明人： Taiki Hoshino , Eisuke Murotani , Akira Isobe
IPC分类号： C09D4/00 , C09D7/12 , C09D171/02 , C08G65/336 , C08L71/02 , C08G65/00 , C04B41/82 , C23C16/56 , C07F7/08
CPC分类号： C09D4/00 , C04B41/82 , C07F7/081 , C07F7/0829 , C08G65/007 , C08G65/336 , C08L71/02 , C09D5/00 , C09D7/40 , C09D171/02 , C23C16/56
摘要： To provide a method for producing a silicon compound, whereby a hydrosilylation reaction of a compound having a 2-propenyl group, can be conducted with high selectivity by a simple and easy method. The method for producing a silicon compound comprises reacting a compound (3) having a group represented by —CH2CH═CH2 and a silicon compound (4) having an H—Si bond in the presence of a transition metal catalyst (C) and a compound (D) having a group represented by —S(═O)— to obtain a compound (5) having a group represented by —CH2CH2CH2Si≡.

7. 发明申请

US20150344703A1 FLUORINATED ETHER COMPOUND, COMPOSITION FOR FORMING HARD COATING LAYER, AND ARTICLE HAVING HARD COATING LAYER 有权
标题翻译：氟化合物，形成硬涂层的组合物和具有硬涂层的物品
公开(公告)号：US20150344703A1
公开(公告)日：2015-12-03
申请号：US14821941
申请日：2015-08-10
申请人： ASAHI GLASS COMPANY, LIMITED
发明人： Kiyotaka TAKAO , Nobuyuki Otozawa , Daisuke Jomuta , Kuniko Okano , Taiki Hoshino
IPC分类号： C09D5/16 , C07C43/12 , C07C271/22 , C09D133/14 , C07C69/63
CPC分类号： C09D5/16 , C07C43/126 , C07C69/63 , C07C271/22 , C08G65/007 , C08G65/329 , C08G65/33348 , C08G2650/48 , C09D4/00 , C09D133/14 , C09D171/00 , G02B1/14 , Y10T428/3154
摘要： To provide a fluorinated ether compound capable of imparting excellent antifouling properties (oil-based ink repellency, fingerprint stain removability) to a hard coating layer, etc., a composition for forming a hard coating layer, containing such a compound, and an article having an antifouling hard coating layer formed from such a composition.A fluorinated ether compound which has either a poly(oxyperfluoroalkylene) chain having a unit repeated that comprises a group constituted by one to three of at least one type of a C1-2 oxyperfluoroalkylene group and a group constituted by one to three of at least one type of a C3-6 oxyperfluoroalkylene group, bonded to each other, or a poly(oxyperfluoroalkylene) chain having a unit repeated that comprises a C4 oxyperfluoroalkylene group and an oxyperfluoroalkylene group other than such a group, bonded to each other, a linking group bonded to a first terminal of the above poly(oxyperfluoroalkylene) chain, and at least one (meth)acryloyl group bonded to the above linking group; a composition for forming a hard coating layer containing such a compound; and an article having such a hard coating layer.
摘要翻译：为了提供能够赋予硬涂层等优异的防污性（油基拒油性，指纹色斑去除性）的含氟醚化合物，含有这种化合物的硬质涂层形成用组合物和具有由这种组合物形成的防污硬涂层。具有重复单元的聚（全氟全氟亚烷基）链的氟化醚化合物，其包含由至少一种类型的C1-2氧全氟亚烷基中的一至三个构成的基团和由至少一个或相互键合的C3-6氧全氟亚烷基的类型或重复单元的聚（全氟亚烷基）链，其包含除了这些基团之外的C4全氟代亚烷基和氧全氟亚烷基，彼此键合，到上述聚（全氟亚烷基）链的第一末端，和至少一个与上述连接基团键合的（甲基）丙烯酰基; 用于形成含有这种化合物的硬质涂层的组合物; 以及具有这样的硬涂层的制品。

8. 发明申请

US20150315443A1 COMPOSITION FOR FORMING WATER REPELLENT FILM, AND ITS USE 审中-公开
标题翻译：用于形成水膜的组合物及其用途
公开(公告)号：US20150315443A1
公开(公告)日：2015-11-05
申请号：US14799697
申请日：2015-07-15
申请人： ASAHI GLASS COMPANY, LIMITED
发明人： Yosuke TAKEDA , Taiki Hoshino , Kenji Ishizeki
IPC分类号： C09K3/18 , C03C17/42 , C03C17/30
CPC分类号： C09K3/18 , C03C17/30 , C03C17/42 , C09D5/00 , C09D183/08 , Y10T428/31612
摘要： To provide a composition for forming a water repellent film capable of forming a water repellent film excellent in chemical resistance and light resistance; a water repellent film formed by using such a composition for forming a water repellent film; a substrate with a water repellent film having such a water repellent film formed on at least a part of a substrate; and an article for a transport equipment comprising such a substrate with a water repellent film.A composition for forming a water repellent film, which comprises (A) a compound of the formula (1) and/or its partially hydrolyzed condensate, and (B) a compound of the formula (2) having a number average molecular weight of at least 2,600 and/or its partially hydrolyzed condensate, or a partially hydrolyzed co-condensate of the component (A) and the component (B); a water repellent film formed by using such a composition for forming a water repellent film; a substrate with a water repellent film having such a water repellent film formed on at least a part of a substrate; and an article for a transport equipment comprising such a substrate with a water repellent film.
摘要翻译：提供一种能够形成耐化学性和耐光性优异的防水膜的防水膜的组合物; 通过使用这种用于形成防水膜的组合物形成的防水膜; 具有在基材的至少一部分上形成有防水膜的防水膜的基材; 以及包括具有防水膜的基板的运输设备的物品。一种用于形成防水膜的组合物，其包含（A）式（1）的化合物和/或其部分水解的缩合物，和（B）数均分子量为至少2,600和/或其部分水解的缩合物或组分（A）和组分（B）的部分水解的共缩合物; 通过使用这种用于形成防水膜的组合物形成的防水膜; 具有在基材的至少一部分上形成有防水膜的防水膜的基材; 以及包括具有防水膜的基板的运输设备的物品。

9. 发明授权

US10138391B2 Fluorinated compound, composition for forming hard coat layer, and article having hard coat layer 有权
公开(公告)号：US10138391B2
公开(公告)日：2018-11-27
申请号：US14857018
申请日：2015-09-17
申请人： ASAHI GLASS COMPANY, LIMITED
发明人： Kiyotaka Takao , Toyomichi Shimada , Taiki Hoshino
IPC分类号： C07D251/30 , C09D135/02 , C08G65/00 , C08G18/02 , C09D4/00 , C08F290/06 , C09D171/00 , C08J7/04 , C08G65/332 , C08G65/333 , C08L71/00
摘要： A fluorinated compound represented by D1-Rf1—O—CH2—(CmF2mO)n-A (wherein D1 is CF3— or CF3—O—, Rf1 is a C1-20 fluoroalkylene group containing at least one hydrogen atom, a C2-20 fluoroalkylene group containing at least one hydrogen atom and having an etheric oxygen atom between carbon-carbon atoms, etc., m is an integer of from 1 to 6, n is an integer of from 1 to 200, and A is a monovalent organic group having at least one (meth)acryloyl group), which is capable of imparting excellent antifouling properties (oily ink repellency, fingerprint stain removability) and lubricity to e.g. a hard coat layer; a hard coat layer-forming composition which contains such a fluorinated compound; and an article having a hard coat layer formed from such a composition.

10. 发明授权

US10138315B2 Fluorinated compound-containing composition, method for its production, coating liquid, hard coat layer-forming composition and article 有权
公开(公告)号：US10138315B2
公开(公告)日：2018-11-27
申请号：US15679198
申请日：2017-08-17
申请人： ASAHI GLASS COMPANY, LIMITED
发明人： Kiyotaka Takao , Taiki Hoshino
IPC分类号： C08F2/46 , C08F2/50 , C08G61/04 , C08F290/06 , C08G18/67 , C09D4/00 , C09D175/08 , C09D175/14 , C08G18/28 , C08G18/79 , C09D151/08 , C09J4/00
摘要： A composition including a fluorinated compound (A), a compound (B) and a solvent (S1), wherein the content of the fluorinated compound (A) in the composition is from 5 to 30 mass % to the composition, and the content of the compound (B) is from 0.1 to 2 mass % to the composition, wherein the fluorinated compound (A) has no isocyanate group and has a portion derived from a compound (a) having a poly(oxyperfluoroalkylene) chain and an active hydrogen-containing group, a portion derived from a compound (b) having a polymerizable carbon-carbon double bond and an active hydrogen-containing group, and a portion derived from a polyisocyanate (c), and wherein the compound (B) has a polymerizable carbon-carbon double bond and an active hydrogen-containing group.

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