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    • 9. 发明申请
    • Mandrel for producing quartz glass and production method for optical fiber mother material, optical fiber and quartz glass body using the same
    • 用于生产石英玻璃的心轴和用于光纤母材的光纤和石英玻璃体的使用方法
    • US20060236724A1
    • 2006-10-26
    • US11455499
    • 2006-06-19
    • Yoshihisa KusanoAtsuyuki ShimadaToshiharu Hiraoka
    • Yoshihisa KusanoAtsuyuki ShimadaToshiharu Hiraoka
    • C03B37/018
    • C03B19/02C03B19/1484C03B37/0126C03B37/01268C03B37/0128C03B37/01486C03B37/02736
    • A mandrel for producing quartz glass, comprising at least two columnar or cylindrical, carbon fiberreinforced carbon composite material made members joined in series by screw thread parts. The mandrel is carbonimpregnated and/or carbon-coated on the screw thread parts, and, in addition, may be provided with reinforcing members on the outer sides of the screw thread parts. Quartz glass fine particles obtained by flame-hydrolyzing a volatile silicon compound are deposited, using this mandrel, on the surface of a heat-resisting substratum or on a starting rod at the end of the mandrel to easily form a large porous quartz glass mother material, the porous quartz glass mother material is dehydrated and transparently vitrified to produce a large optical fiber mother material, and further the optical fiber mother material is drawn to produce a low-cost, high-precision optical fiber. In addition, a columnar or cylindrical mandrel for producing quartz glass is disposed at the center of a heat-resisting mold, is filled with silicon dioxide power, and melt in a heating furnace for vitrifying, thereby producing a large, high precision quartz glass body at low costs.
    • 一种用于生产石英玻璃的心轴,包括由螺纹部分串联连接的至少两个圆柱形或圆柱形碳纤维增强碳复合材料制成的构件。 心轴在螺纹部分上被碳浸渍和/或碳涂覆,并且另外可以在螺纹部分的外侧上设置加强构件。 通过火焰水解挥发性硅化合物获得的石英玻璃细颗粒使用该心轴沉积在耐热基底的表面上或在心轴的端部的起始棒上,以容易地形成大的多孔石英玻璃母体材料 ,将多孔石英玻璃母材脱水透明地玻璃化以产生大的光纤母材,并且进一步拉制光纤母材以生产低成本,高精度的光纤。 另外,在耐热模具的中央配置用于制造石英玻璃的柱状或圆筒状的芯棒,填充二氧化硅粉末,在加热炉中熔融玻璃化,由此制造大型,高精度的石英玻璃体 以低成本。
    • 10. 发明授权
    • Crucible for crystal pulling and method of manufacturing same
    • 坩埚用于晶体拉制和制造方法相同
    • US6136094A
    • 2000-10-24
    • US147446
    • 1999-02-02
    • Masatoshi YamajiKatsuhide NagaokaToshiharu HiraokaTsuyoshi MatsumotoSatoshi Ishikawa
    • Masatoshi YamajiKatsuhide NagaokaToshiharu HiraokaTsuyoshi MatsumotoSatoshi Ishikawa
    • C04B35/83C30B15/10C30B35/00
    • C04B35/83C30B15/10Y10S117/90Y10T117/10
    • The present invention is directed to a single crystal pulling crucible of carbon fiber reinforced carbon composite material formed by the filament windings by combination of axially reinforced layers as well as circumberentially reinforced layers, which combination is given in two or more sets, and to the producing method thereof. The circumferentially reinforced layers resist a force tending to exapand a drum portion of the crucible, and the axially reinforced layers resist a force tending to push down a bottom of the crucible. The axially reinforced layers extending from the bottom portion to the drum portion can be formed by at least either of a level winding of a contact angle of 0.degree. to 10.degree. with respect to the center axis and a poral winding, and the circumferentially reinforced layers in area adjacent to the drum portion out of the drum portion and the bottom portion can be formed by at least either of a parallel winding of a contact angle of 70.degree. to 90.degree. with respect to the center axis and a helical winding. When the axially reinforced layers cover the center of the bottom portion, an integral crucible of C/C composite material with no hole is provided. When the surface of the C/C composite material is impregnated and covered with a pyrolytic carbon, improved resistance to forming SiC is provided.
    • PCT No.PCT / JP97 / 02211 Sec。 371日期1999年2月2日 102(e)1999年2月2日PCT 1997年6月26日PCT公布。 第WO97 / 49844号公报 日期:1997年12月31日本发明涉及一种碳纤维增强碳复合材料的单晶拉制坩埚,其通过轴向加强层以及环形增强层的组合由细丝绕组形成,该组合以两组或多组 ,及其制造方法。 周向加强层抵抗倾向于展开坩埚的鼓部分的力,并且轴向增强层抵抗倾向于将坩埚底部推下的力。 从底部延伸到鼓部的轴向增强层可以通过相对于中心轴线接触角为0°至10°的水平绕组和通孔绕组和周向加强层中的至少一个形成 与滚筒部分相邻的滚筒部分的区域中的至少一个可以由相对于中心轴线的接触角为70°至90°的平行绕组和螺旋形绕组形成。 当轴向增强层覆盖底部的中心时,提供了没有孔的C / C复合材料的整体坩埚。 当C / C复合材料的表面被热解碳浸渍并覆盖时,提供了改善的耐SiC成形性。