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1. 发明授权

US5723685A Preparation of monovinyl ethers 失效
标题翻译：单乙烯基醚的制备
公开(公告)号：US5723685A
公开(公告)日：1998-03-03
申请号：US548739
申请日：1995-10-26
申请人： Marc Heider , Thomas Ruhl , Herbert Helfert , Martin Schmidt-Radde , Jochem Henkelmann
发明人： Marc Heider , Thomas Ruhl , Herbert Helfert , Martin Schmidt-Radde , Jochem Henkelmann
IPC分类号： B01J23/02 , B01J31/02 , B01J31/12 , C07B61/00 , C07C41/06 , C07C41/08 , C07C43/178 , C07C41/00
CPC分类号： C07C41/08 , C07C41/54
摘要： The preparation of monovinyl ethers of the general formula I ##STR1## in which A stands for a chemical bond or for a methylene or ethylene group, the radicals R.sup.1 and R.sup.2 independently stand for hydrogen, alkyl, cycloalkyl, or aryl groups or R.sup.1 and R.sup.2 together form a C.sub.3 -C.sub.5 alkylene bridging member, by the reaction of a diol of the general formula II ##STR2## in which the variables have the above meanings, with acetylene in the presence of a base, in which the reaction is carried out at 150.degree.-250.degree. C. under an acetylene partial pressure of 5-25 bar until 40-80% of the diol has been converted, at which point the reaction is stopped and the monovinyl ether of the formula I is isolated.
摘要翻译：制备通式I的单乙烯基醚（I）其中A代表化学键或亚甲基或亚乙基，基团R 1和R 2分别代表氢，烷基，环烷基或芳基或 R 1和R 2一起形成C 3 -C 5亚烷基桥连体，通过其中变量具有上述含义的通式II的二醇（II）与乙炔在碱的存在下反应，其中反应在150-250℃，乙炔分压为5-25巴下进行，直到二醇的40-80％转化为止，此时反应停止，式I的单乙烯基醚是孤立的

2. 发明授权

US5646293A Preparation of N-alkenylazoles 失效
标题翻译： N-链烯基唑的制备
公开(公告)号：US5646293A
公开(公告)日：1997-07-08
申请号：US675588
申请日：1996-07-03
申请人： Jochem Henkelmann , Marc Heider , Thomas Ruhl
发明人： Jochem Henkelmann , Marc Heider , Thomas Ruhl
IPC分类号： B01J31/02 , C07B61/00 , C07D233/56 , C07D233/58 , C07D235/06 , C07D249/08 , C07D521/00 , C07D235/08 , C07D235/18
CPC分类号： C07D235/06 , C07D231/12 , C07D233/56 , C07D249/08
摘要： A process for preparing N-alkenylazoles of the general formula I ##STR1## where X is CH--R.sup.6 or nitrogen,R.sup.1 and R.sup.2 are hydrogen or C.sub.1 - to C.sub.8 -alkyl,R.sup.3,R.sup.4,R.sup.5 and R.sup.6 are hydrogen, C.sub.1 - to C.sub.40 -alkyl, C.sub.2 - to C.sub.40 -alkenyl, C.sub.3 - to C.sub.20 -cycloalkyl, C.sub.4 - to C.sub.20 -alkylcycloalkyl, C.sub.4 - to C.sub.20 -cycloalkylalkyl, aryl, C.sub.7 - to C.sub.20 -alkylaryl or C.sub.7 - to C.sub.20 -aralkyl, or aryl, C.sub.7 - to C.sub.20 -alkylaryl or C.sub.7 - to C.sub.20 -aralkyl which are mono- to pentasubstituted by C.sub.1 - to C.sub.8 -alkyl, C.sub.1 - to C.sub.8 -alkoxy or halogen, or R.sup.3 and R.sup.4 or R.sup.4 and R.sup.5 or R.sup.5 and R.sup.6 together are a C.sub.2 - to C.sub.10 -alkylene chain which is unsubstituted or mono- to hexasubstituted by C.sub.1 - to C.sub.8 -alkylby reaction of azoles of the general formula II ##STR2## where X, R.sup.3, R.sup.4 and R.sup.5 have the abovementioned meanings, with an alkenyl carboxylate of the general formula III ##STR3## where R.sup.1 and R.sup.2 have the abovementioned meanings and R.sup.7 is hydrogen, C.sub.1 - to C.sub.40 -alkyl, C.sub.3 - to C.sub.20 -cycloalkyl, C.sub.4 - to C.sub.20 -alkylcycloalkyl, aryl, C.sub.7 - to C.sub.20 -alkylaryl, C.sub.7 - to C.sub.20 -aralkyl, or aryl or C.sub.7 - to C.sub.20 -aralkyl which is mono- to trisubstituted by C.sub.1 - to C.sub.8 -alkyl, at from 0.degree. to 180.degree. C. and from 0.01 to 10 bar, which comprises carrying out the reaction in the presence of a base and of a quaternary salt, is described.
摘要翻译：制备通式I（I）的N-烯基唑的方法，其中X是CH-R6或氮，R1和R2是氢或C1-至C8-烷基，R3，R4，R5和R6是氢， C 1至C 40 - 烷基，C 2至C 40 - 烯基，C 3 -C 20 - 环烷基，C 4至C 20 - 烷基环烷基，C 4 -C 20 - 环烷基烷基，芳基，C 7 -C 20烷基芳基或C 7 -C 20 - 芳烷基，或被C 1〜C 8 - 烷基，C 1 -C 8 - 烷氧基或卤素单 - 五取代的芳基，C 7〜C 20 - 烷基芳基或C 7〜C 20 - 芳烷基，或者R 3和R 4或R 4和R 5或R 5 和R6一起是C2至C10亚烷基链，其未被取代或被C 1 -C 8 - 烷基单取代或被六取代的通式II（II）的唑类，其中X，R 3，R 4和R 5 具有上述含义，具有通式III（III）的烯基羧酸酯，其中R 1和R 2具有上述含义，并且R 7是氢，C 1至C 40烷基，C 3 -C 20环烷基，C 4至 C20-烷基环烷基，芳基，C7-至C20-烷基芳基，C7-至C20-芳基烷基或芳基或被C 1 -C 8烷基单取代三取代的C 7 -C 20 - 芳烷基，其中0至180℃和0.01至10巴，其包括在存在下进行反应的碱和季盐。

3. 发明授权

US4541369A Cooling apparatus for combustion engine 失效
标题翻译：内燃机冷却装置
公开(公告)号：US4541369A
公开(公告)日：1985-09-17
申请号：US600815
申请日：1984-04-16
申请人： Thomas Ruhl
发明人： Thomas Ruhl
IPC分类号： F01P5/06 , F01P11/10
CPC分类号： F01P5/06 , F01P11/10
摘要： An air guide ring arrangement is disclosed for guiding air flow around an axial fan of a liquid cooled internal combustion engine having a radiator through which air is drawn by the fan. To facilitate construction of a minimal sized air gap between the air guide ring and the fan blades, the air guide ring is supported by a gibbet or bracket arm fixed to the engine and by a spoked support wheel rotatably borne at the outer circumference of the fan hub.
摘要翻译：公开了一种导风环装置，用于引导具有散热器的液体冷却内燃机的轴流风扇周围的空气流动，风扇通过该散热器吸入空气。为了便于在导风环和风扇叶片之间构造最小尺寸的空气间隙，空气导向环由固定在发动机上的gibbet或支架臂支撑，并且可旋转地支撑在风扇的外圆周上的辐条支撑轮枢纽。

4. 发明授权

US6099601A Ethylene-vinyl formate copolymers, process for their preparation, their use as flow improvers, and fuel and propellant compositions comprising them 失效
标题翻译：乙烯 - 甲酸乙烯酯共聚物，其制备方法，它们作为流动改进剂的用途，以及包含它们的燃料和推进剂组合物
公开(公告)号：US6099601A
公开(公告)日：2000-08-08
申请号：US802906
申请日：1997-02-20
申请人： Andreas Deckers , Bernd Wenderoth , Thomas Ruhl , Hans-Joachim Muller , Roger Klimesch
发明人： Andreas Deckers , Bernd Wenderoth , Thomas Ruhl , Hans-Joachim Muller , Roger Klimesch
IPC分类号： C08F4/38 , C08F210/02 , C10L1/197 , C01L1/18
CPC分类号： C10L1/1973 , C08F210/02
摘要： Copolymer comprising ethylene units and vinyl formate units, the content of free vinyl formate in the polymer preferably being not more than 5000 ppm, based on the weight of the copolymer, a process for its preparation, and its use as flow improver, especially in petroleum distillates, preferably fuel and propellant compositions, especially petroleum middle distillates, and also a fuel and propellant composition comprising a principal quantity of a fuel and propellant and that quantity of a copolymer as above which is effective in improving the flow properties.
摘要翻译：包含乙烯单元和甲酸乙烯酯单元的共聚物，基于共聚物的重量，聚合物中游离乙烯基甲酸酯的含量优选不大于5000ppm，其制备方法及其作为流动改进剂，特别是在石油中的用途馏出物，优选燃料和推进剂组合物，特别是石油中间馏分，以及包含主要量的燃料和推进剂的燃料和推进剂组合物，以及一定量的有效改善流动性能的共聚物。

5. 发明授权

US5976202A Reaction products of polyolefins with vinyl esters and their use as fuel and lubricant additives 失效
标题翻译：聚烯烃与乙烯基酯的反应产物及其作为燃料和润滑剂添加剂的用途
公开(公告)号：US5976202A
公开(公告)日：1999-11-02
申请号：US504584
申请日：1995-07-20
申请人： Hans Peter Rath , Helmut Mach , Harald Schwahn , Hans-Joachim Muller , Wolfgang Reif , Thomas Ruhl
发明人： Hans Peter Rath , Helmut Mach , Harald Schwahn , Hans-Joachim Muller , Wolfgang Reif , Thomas Ruhl
IPC分类号： C10L1/192 , C08F8/12 , C08F8/32 , C08F255/00 , C08F290/00 , C08F290/02 , C10G75/00 , C10L1/14 , C10L1/18 , C10L1/195 , C10L1/197 , C10L1/198 , C10L1/22 , C10L1/236 , C10L1/238 , C10L10/00 , C10L10/08 , C10M129/90 , C10M133/54 , C10M145/04 , C10M145/06 , C10M149/04 , C10N20/04 , C10N30/04 , C10N40/25 , C10N60/02 , C07C69/33 , C07C211/22
CPC分类号： C10M149/04 , C08F255/00 , C08F8/30 , C10L1/143 , C10L1/195 , C10L1/198 , C10L1/236 , C10L1/238 , C10L10/06 , C10M129/90 , C10M133/54 , C10M145/04 , C10L1/188 , C10L1/19 , C10L1/1905 , C10L1/191 , C10L1/1955 , C10L1/1973 , C10L1/1976 , C10L1/1985 , C10L1/2222 , C10L1/224 , C10L1/232 , C10L1/2362 , C10L1/2366 , C10L1/2368 , C10L1/2383 , C10L1/2387 , C10M2207/021 , C10M2209/04 , C10M2209/06 , C10M2209/062 , C10M2215/04 , C10M2215/26 , C10M2217/00 , C10M2217/02 , C10M2217/022 , C10M2217/04
摘要： Reaction products of polyolefins having predominantly a terminal double bond and a number average molecular weight of from 250 to 10,000, which possess an aliphatic hydrocarbon skeleton which is straight-chain or carries C.sub.1 -C.sub.4 -alkyl side chains, with from 1 to 10 mol, per equivalent of double bond, of one or more vinyl esters I ##STR1## are obtainable by reacting the stated polyolefins with the vinyl esters I in the presence of a free radical initiator at from 80 to 200.degree. C., it being possible for these reaction products subsequently to have been hydrolyzed to the corresponding alcohols or converted into the corresponding amines by reductive amination with amines II ##STR2## .
摘要翻译：主要具有末端双键和数均分子量为250至10,000的聚烯烃的反应产物，其具有直链或带有C1-C4烷基侧链的脂族烃骨架，其具有1-10mol，每当量的双键，一种或多种乙烯基酯I可通过在80-200℃自由基引发剂存在下使所述聚烯烃与乙烯基酯I反应而得到，这些反应产物随后可能已经被水解成相应的醇或通过用胺II还原胺化转化成相应的胺。

6. 发明授权

US5902916A Process for reacting an organic compound in the presence of a ruthenium catalyst formed in situ 失效
标题翻译：在原位形成的钌催化剂存在下使有机化合物反应的方法
公开(公告)号：US5902916A
公开(公告)日：1999-05-11
申请号：US845435
申请日：1997-04-25
申请人： Thomas Ruhl , Boris Breitscheidel , Franz Josef Brocker , Wolfgang Reif , Jochem Henkelmann , Karl Heinz Brauch , Andreas Henne
发明人： Thomas Ruhl , Boris Breitscheidel , Franz Josef Brocker , Wolfgang Reif , Jochem Henkelmann , Karl Heinz Brauch , Andreas Henne
IPC分类号： B01J23/46 , C07B35/02 , C07B61/00 , C07C29/132 , C07C29/141 , C07C29/149 , C07C29/20 , C07C35/08 , C07C209/72 , C07C211/40 , C08F8/04 , C07C5/10
CPC分类号： C07C29/20 , B01J23/462 , C07B35/02 , C07C209/72 , C07C29/141 , C07C29/149 , C07C29/19 , C08F8/04 , C07C2101/14 , Y02P20/584
摘要： A process for reacting an organic compound in the presence of a catalyst, wherein the catalyst comprises a homogeneous ruthenium compound or a mixture of two or more thereof deposited in situ on a support.
摘要翻译：一种在催化剂存在下使有机化合物反应的方法，其中催化剂包含在载体上原位沉积的均匀钌化合物或两种或更多种的混合物。

7. 发明授权

US5783706A Process for the preparation of 1,3-disubstituted imidazolidinones 失效
标题翻译： 1,3-二取代的咪唑啉酮的制备方法
公开(公告)号：US5783706A
公开(公告)日：1998-07-21
申请号：US776105
申请日：1997-03-14
申请人： Jochem Henkelmann , Thomas Ruhl
发明人： Jochem Henkelmann , Thomas Ruhl
IPC分类号： C07D233/34 , C07D233/32 , C07D233/58
CPC分类号： C07D233/32
摘要： 2-Imidazolidinones are prepared by reacting 1,3-dioxalan-2-one (ethylene carbonate) with at least one compound of the formula RNH.sub.2 where R can be, inter alia, H, alkyl, aryl, heteroalkyl or heteroaryl.
摘要翻译： PCT No.PCT / EP95 / 02806 Sec。 371日期1997年3月17日 102（e）1997年3月17日PCT PCT 1995年7月18日PCT公布。第WO96 / 02516号公报日期1992年2月1日 - 咪唑啉酮是通过使1,3-二氧杂环丙烷-2-酮（碳酸亚乙酯）与至少一种式RNH2化合物反应制备的，其中R可以是H，烷基，芳基，杂烷基或杂芳基。

8. 发明授权

US5773657A Hydrogenation of aromatic compounds in which at least one amino group is bonded to an aromatic nucleus 失效
标题翻译：其中至少一个氨基与芳香核键合的芳族化合物的氢化
公开(公告)号：US5773657A
公开(公告)日：1998-06-30
申请号：US702262
申请日：1996-08-23
申请人： Heinz Rutter , Thomas Ruhl , Boris Breitscheidel , Jochem Henkelmann , Andreas Henne , Thomas Wettling
发明人： Heinz Rutter , Thomas Ruhl , Boris Breitscheidel , Jochem Henkelmann , Andreas Henne , Thomas Wettling
IPC分类号： B01J23/46 , B01J21/04 , B01J23/89 , B01J35/10 , C07B61/00 , C07C209/72 , C07C211/35
CPC分类号： B01J21/04 , B01J23/462 , B01J23/892 , C07C209/72 , B01J35/0053 , B01J35/1009 , B01J35/1014 , B01J35/1071 , B01J35/1076 , B01J35/109
摘要： Aromatic compounds in which at least one amino group is bonded to an aromatic nucleus are catalytically hydrogenated in the liquid phase by a process in which the catalyst consists essentially of ruthenium and, optionally at least one metal of subgroup I, VII or VIII in an amount of from 0.01 to 30% by weight, based on the total weight of the catalyst, applied to a carrier which has a mean pore diameter of at least 0.1 .mu.m and a surface area of not more than 15 m.sup.2 /g.
摘要翻译：其中至少一个氨基结合到芳香核上的芳香族化合物在液相中通过催化剂基本上由钌和任选的至少一种I，VII或VIII族金属的至少一种金属组成的方法在液相中催化氢化，其量为 0.01至30重量％，基于催化剂的总重量，施加到平均孔径为至少0.1μm并且表面积不大于15m 2 / g的载体上。

9. 发明授权

US5639890A Preparation of N-akenylcarbamic esters 失效
标题翻译： N-烯基氨基甲酸酯的制备
公开(公告)号：US5639890A
公开(公告)日：1997-06-17
申请号：US705682
申请日：1996-08-29
申请人： Jochem Henkelmann , Marc Heider , Thomas Ruhl
发明人： Jochem Henkelmann , Marc Heider , Thomas Ruhl
IPC分类号： C07C269/06 , C07D263/22 , C07D263/14
CPC分类号： C07C269/06 , C07D263/22
摘要： N-Alkenylcarbamic esters of the general formula I ##STR1## where at least one of the R.sup.1 radicals is hydrogen and the second R.sup.1 radical is hydrogen or C.sub.1 -C.sub.4 --alkyl, the R.sup.2 radical is an aliphatic, cycloaliphatic, araliphatic or aromatic radical which can be linked to the R.sup.3 radical to form a 2- to 10-membered bridge, and the R.sup.3 radical is an aliphatic, cycloaliphatic or aromatic radical, from an alkenyl carboxylate of the general formula II ##STR2## where R.sup.1 has the abovementioned meaning, and R.sup.4 is hydrogen, an aliphatic, cycloaliphatic or aromatic radical, and a carbamic ester of the general formula III ##STR3## where the R.sup.2 and R.sup.3 radicals have the abovementioned meanings, are prepared by reacting the starting compounds in the presence of a base.
摘要翻译：其中至少一个R 1基团是氢且第二个R 1基团是氢或C 1 -C 4 - 烷基，R 2基团是脂族，环脂族，芳脂族或芳族基团的通式I的N-烯丙基氨基甲酸酯其可以连接到R 3基团以形成2-至10-元桥，并且R 3基团是脂肪族，脂环族或芳族基团，其通式II的烯基羧酸酯其中R1具有上述并且R 4是氢，脂族，脂环族或芳族基团，和通式III的氨基甲酸酯，其中R 2和R 3基团具有上述含义，是通过使起始化合物在一个基地

10. 发明授权

US5936126A Process for reacting an organic compound in the presence of a supported ruthenium catalyst 失效
标题翻译：在负载型钌催化剂存在下使有机化合物反应的方法
公开(公告)号：US5936126A
公开(公告)日：1999-08-10
申请号：US877819
申请日：1997-06-18
申请人： Thomas Ruhl , Boris Breitscheidel , Jochem Henkelmann , Wolfgang Reif , Helmuth Menig , Sabine Weiguny
发明人： Thomas Ruhl , Boris Breitscheidel , Jochem Henkelmann , Wolfgang Reif , Helmuth Menig , Sabine Weiguny
IPC分类号： B01J23/46 , B01J35/10 , C07B35/02 , C07B61/00 , C07C29/141 , C07C29/149 , C07C29/20 , C07C31/12 , C07C31/125 , C07C31/135 , C07C31/20 , C07C35/08 , C07C35/21 , C07C209/72 , C07C211/35 , C07C211/36
CPC分类号： C07C29/149 , B01J23/462 , C07C209/72 , C07C29/141 , C07C29/20 , C07C2101/14
摘要： A process for the hydrogenation of an aromatic compound, in which at least one hydroxyl group is attached to an aromatic core, or an aromatic compound, in which at least one amino group is attached to an aromatic core, in the presence of a catalyst containing, as active metal, ruthenium and optionally one or more other Group IB, VIIB, or VIIIB metals, applied to a macroporous support.
摘要翻译：一种芳香化合物的氢化方法，其中至少一个羟基连接到芳族核心上，或其中至少一个氨基连接到芳族核心上的芳族化合物，在含有，作为活性金属，钌和任选的一种或多种其它IB，VIIB或VIIIB族金属，应用于大孔载体。

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