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1. 发明授权

US5542953A 5-halogen-2,4-Bis (alkylamino)-1-alkylbenzenes and hair dye compositions containing same 失效
标题翻译： 5-卤代-2,4-双（烷基氨基）-1-烷基苯和含有它们的染发剂组合物
公开(公告)号：US5542953A
公开(公告)日：1996-08-06
申请号：US142492
申请日：1993-10-22
申请人： Wolfgang R. Balzer , Thomas Clausen , Anke Frank , Alexa Weinges
发明人： Wolfgang R. Balzer , Thomas Clausen , Anke Frank , Alexa Weinges
IPC分类号： A61K8/00 , A61K8/33 , A61K8/40 , A61K8/41 , A61K8/49 , A61Q5/10 , C07C211/52 , C07C215/16 , A61K7/13 , C07C211/51
CPC分类号： A61Q5/10 , A61K8/411 , A61K8/69 , C07C211/52 , C07C215/16
摘要： The composition for the oxidative dyeing of hair contains at least one coupler of the general formula ##STR1## where R is a straight-chain or branched C.sub.1 - to C.sub.4 -alkyl group, X is chlorine or fluorine, and R.sup.1 is a straight-chain or branched C.sub.1 - to C.sub.4 -alkyl group or a straight-chain or branched C.sub.2 - to C.sub.4 -hydroxyalkyl group. The 5-halogen-2,4-bis(alkylamino)-1-alkylbenzenes of the formula (I) are novel. The couplers of the general formula (I) may be obtained through simple chemical reactions, are easily soluble in water and have an outstanding shelf stability, in particular as a constituent of the hair dye composition described here. The dyeing results which can be achieved with the hair dye composition according to the invention are particularly distinguished by the color intensity of the red hues, in addition to the multitude of shades, and by a good purity of color with respect to blue hues.
摘要翻译： PCT No.PCT / EP93 / 00011 Sec。 371日期：1993年10月22日 102（e）日期1993年10月22日PCT 1993年1月7日PCT PCT。出版物WO93 / 16677 日本1993年9月2日头发的氧化染色组合物含有至少一种通式为（I）的成色剂，其中R是直链或支链的C 1 -C 4烷基，X是氯或氟，R 1为直链或支链C 1至C 4烷基或直链或支链C 2至C 4 - 羟基烷基。式（I）的5-卤代-2,4-二（烷基氨基）-1-烷基苯是新颖的。通式（I）的成色剂可以通过简单的化学反应获得，易溶于水并具有优异的贮存稳定性，特别是作为本文所述的染发剂组合物的成分。通过根据本发明的染发剂组合物可以实现的染色结果特别地除了多种色调之外的红色调的颜色强度以及相对于蓝色色调的良好的颜色纯度。

2. 发明授权

US5279313A Two component composition and method for bleaching hair 失效
标题翻译：双组分组成和漂白方法
公开(公告)号：US5279313A
公开(公告)日：1994-01-18
申请号：US777544
申请日：1991-12-12
申请人： Thomas Clausen , Wolfgang R. Balzer
发明人： Thomas Clausen , Wolfgang R. Balzer
IPC分类号： A61K8/04 , A61Q5/08 , C11D3/39 , A61K7/13
CPC分类号： A61K8/0275 , A61Q5/08 , A61K2800/88
摘要： A preparation for use in a hair bleaching composition consists of 30 to 65% by weight of a persulfate granulate having granule diameters from 0.1 to 0.6 cm and at least one other granulated substance including 15 to 45% by weight of granulated alkaline reacting alkali metal salts. The other granulated substance also has particle diameters from about 0.1 to 0.6 cm. It can also contain 0.1 to 3% by weight of a chelating agent, 0.1 to 15% by weight of an anionic, cationic or nonionic surfactant and a water-soluble thickener. The two component composition contains an aqueous solution which is 4 to 18% by weight hydrogen peroxide and the preparation containing the granulated persulfate. Prior to application on the hair the hydrogen peroxide solution is mixed with the preparation.
摘要翻译：本申请涉及制备用于漂白和减轻固体形式呈现的头发的试剂，由此使用各组分颗粒的混合物或其中所含的至少其中的过硫酸盐呈颗粒状。造粒可以通过普通技术方法实现，例如喷雾干燥，其中可以在造粒前将初始物质加入润湿剂，乳化剂或增稠剂。描述的制剂的特点在于保质期良好，避免了以前的减轻剂的缺点，例如，通过氨的损失分离或变化化学成分。本申请还包括使用上述制剂漂白和减轻毛发的2部分药剂和方法。

3. 发明授权

US5224965A Composition for the oxidative dyeing of hair and new 5-halogen-2,4-diamino alkylbenzenes 失效
标题翻译：头发和新5-卤代-2,4-二氨基亚苄基氧化剂的组合物
公开(公告)号：US5224965A
公开(公告)日：1993-07-06
申请号：US847080
申请日：1992-04-07
申请人： Thomas Clausen , Alexa Weinges , Wolfgang R. Balzer
发明人： Thomas Clausen , Alexa Weinges , Wolfgang R. Balzer
IPC分类号： C07C205/12 , C07C211/52 , D06P1/32 , D06P3/08
CPC分类号： A61Q5/10 , A61K8/411 , C07C205/12 , C07C211/52
摘要： The composition for the oxidative dyeing of hair contains at least one coupler substance of the formula ##STR1## where R is a straight-chain or branched C.sub.1 - to C.sub.4 -alkyl group and X is fluorine or bromine, and new 5-halogen-2,4-diaminoalkylbenzenes.The coupler substances of formula (I) are obtainable by simple chemical reactions, easily soluble in water and have a good shelf stability particularly as constituents of the hair dye composition described here.In addition to the multitude of color shades, the dye results which can be achieved with the hair dye composition according to the invention are distinguished particularly by the intensity of color of the red tones and good uniformity of color of the blue tones.
摘要翻译： PCT No.PCT / EP91 / 01565 Sec。 371日期：1992年4月7日 102（e）日期1992年4月7日PCT 1991年8月17日PCT PCT。出版物WO92 / 04005 头发氧化染色的组合物含有至少一种式（I）的成色剂物质，其中R是直链或支链的C 1〜C 4 - 烷基，X是氟或溴，以及新的5-卤代-2,4-二氨基烷基苯。式（I）的成色剂物质可以通过简单的化学反应获得，易溶于水并且具有良好的贮存稳定性，特别是作为本文所述的染发组合物的成分。除了多种色调之外，根据本发明的染发组合物可以实现的染色结果特别地由红色调的颜色强度和蓝色色调的良好均匀性区分开来。

4. 发明授权

US4900869A Process for the production of 4-[ethyl-(2'-hydroxyethyl)-amino]-1-[(2'-hydroxyethyl)-amino]-2-nitroben zene 失效
标题翻译：制备4- [乙基 - （2'-羟乙基） - 氨基] -1 - [（2'-羟乙基） - 氨基] -2-硝基苯
公开(公告)号：US4900869A
公开(公告)日：1990-02-13
申请号：US120213
申请日：1987-11-06
申请人： Thomas Clausen , Isolde Lowe
发明人： Thomas Clausen , Isolde Lowe
IPC分类号： C09B51/00
CPC分类号： C09B51/00
摘要： A process is disclosed for the production of 4-[ethyl-(2'-hydroxyethyl)-amino]-1-[(2'-hydroxyethyl)-amino]-2-nitrobenzene, by means of a two-stage technique proceeding from the reaction product of 1,4-diamino-2-nitrobenzene with chloroformic acid chloroethyl ester, or by means of a multiple-stage technique which is based upon an improved process for the production of the pre-stage 4-ethylamino-1-[(2'-hydroxyethyl)-amino]-2-nitrobenzene through sulfuric acid splitting off of 4-(N-ethylarylsulfonamido)-1-[(2'-hydroxyethyl)-amino]-2-nitrobenzene.
摘要翻译：公开了通过两步技术方法制备4- [乙基 - （2'-羟乙基） - 氨基] -1 - [（2'-羟乙基） - 氨基] -2-硝基苯的方法从1,4-二氨基-2-硝基苯与氯甲酸氯乙酯的反应产物，或通过多阶段技术，其基于改进的制备前段4-乙基氨基-1- 通过硫酸分离4-（N-乙基芳基亚磺酰氨基）-1 - [（2'-羟乙基） - 氨基] -2-硝基苯，得到[（2'-羟乙基） - 氨基] -2-硝基苯。

5. 发明授权

US4854935A 5-alkoxy-2,4-diamino-alkyl-benzenes and hairdye compositions based on 5-alkoxy-2,4-diamino-alkyl-benzenes 失效
标题翻译：基于5-烷氧基-2,4-二氨基 - 烷基苯的5-烷氧基-2,4-二氨基 - 烷基 - 苯和发丝组合物
公开(公告)号：US4854935A
公开(公告)日：1989-08-08
申请号：US165278
申请日：1988-02-26
申请人： Thomas Clausen , Eugen Konrad
发明人： Thomas Clausen , Eugen Konrad
IPC分类号： A61K8/41 , A61K20060101 , A61K8/31 , A61K8/33 , A61Q5/10 , C07C20060101 , C07C205/37 , C07C217/84
CPC分类号： A61Q5/10 , A61K8/411 , C07C205/37
摘要： New 5-alkoxy-2,4-diaminoalkylbenzenes is disclosed having the formula (I) ##STR1## where R.sup.1 is methyl or ethyl and R.sup.2 is an alkyl radical having from 2 to 4 carbon atoms, a monohydroxyalkyl radical having from 2 to 4 carbon atoms or a dihydroxyalkyl radical having from 3 to 4 carbon atoms, as well as their acid addition salts, and oxidative hair dyeing compositions containing compounds of formula (I).
摘要翻译： PCT No.PCT / EP87 / 00320 Sec。 371日期1988年2月26日 102（e）日期1988年2月26日PCT提交1987年6月20日PCT公布。第WO88 / 00042号公报日本公开了新的5-烷氧基-2,4-二氨基烷基苯，其具有式（I）其中R 1是甲基或乙基，R 2是具有2至4个碳原子的烷基，具有2至4个碳原子的单羟基烷基或具有3至4个碳原子的二羟基烷基，以及它们的酸加成盐，和含有式（I）化合物的氧化染发组合物。

6. 发明授权

US4713080A Method and composition for the dyeing of hair with 2,6-diamino-pyridine derivatives 失效
标题翻译：用2,6-二氨基 - 吡啶衍生物染发毛发的方法和组成
公开(公告)号：US4713080A
公开(公告)日：1987-12-15
申请号：US882634
申请日：1986-07-07
申请人： Eugen Konrad , Thomas Clausen
发明人： Eugen Konrad , Thomas Clausen
IPC分类号： A61K8/49 , A61Q5/10 , C07D213/73 , C07D213/74 , D06P1/32 , D06P3/08 , A61K7/13
CPC分类号： C07D213/74 , A61K8/4926 , A61Q5/10 , C07D213/73
摘要： A method and composition are disclosed for the oxidative coloration of hair, based upon a developer substance-coupler substance combination, employing as coupler substance at least one 2,6-diamino-pyridine derivative according to Formula I ##STR1## in which R.sup.1 and R.sup.2 are the same or different and are each CH.sub.3 or C.sub.2 H.sub.5 and R.sup.3 is hydrogen, C.sub.1 -C.sub.4 -alkyl or C.sub.1 -C.sub.4 -hydroxyalkyl, also in the form of the physiologically compatible salts. The coupler substance, preferably 2,6-diamino-3,5-dimethoxy-pyridine, 2,6-diamino-3,5-diethoxy-pyridine and 2-amino-6-(2'-hydroxyethyl)amino-3,5-dimetnoxy-pyridine, should be present in the composition in a concentration from 0.01 to 3.0% by weight, preferably from 0.1 to 2.0% by weight. The coupler substance according to Formula I is storage resistant, well soluble in water and possesses favorable toxicological as well as dermatological characteristics. The coupler substance of Formula I provides, in combination with 1,4-diamino benzene or its derivatives, very intense cold blue tones without red portions, and in combination with 4-aminophenol, strongly lustrous gold-orange tones.
摘要翻译：公开了基于显影剂物质 - 成色剂物质组合的头发的氧化着色的方法和组合物，其用作成色剂物质至少一种根据式I的（I）的2,6-二氨基 - 吡啶衍生物，其中 R 1和R 2相同或不同，并且各自为CH 3或C 2 H 5，且R 3为氢，C 1 -C 4 - 烷基或C 1 -C 4 - 羟烷基，也为生理上相容的盐形式。成色剂物质，优选2,6-二氨基-3,5-二甲氧基 - 吡啶，2,6-二氨基-3,5-二乙氧基 - 吡啶和2-氨基-6-（2'-羟乙基）氨基-3,5 二甲氧基 - 吡啶应以0.01至3.0重量％，优选0.1至2.0重量％的浓度存在于组合物中。根据式I的成色剂物质是耐贮存的，易溶于水，具有良好的毒理学和皮肤病学特性。式I的成色剂物质与1,4-二氨基苯或其衍生物组合提供非常强烈的冷蓝色色调而没有红色部分，并与4-氨基苯酚组合，具有强光泽的金橙色调。

7. 发明授权

US4704474A 1,4-diamino-5-chloro-2-nitrobenzene derivatives, processes for their production and compositions containing the same for the coloration of hair 失效
标题翻译： 1,4-二氨基-5-氯-2-硝基苯衍生物，它们的生产方法和含有它们的组合物用于着色头发
公开(公告)号：US4704474A
公开(公告)日：1987-11-03
申请号：US834644
申请日：1986-02-26
申请人： Eugen Konrad , Thomas Clausen
发明人： Eugen Konrad , Thomas Clausen
IPC分类号： A61K8/00 , A61K8/41 , A61Q5/06 , A61Q5/10 , C07C67/00 , C07C209/00 , C07C209/08 , C07C211/52 , C07C215/16 , C09B51/00 , C07C87/60 , A61K7/13
CPC分类号： A61K8/418 , A61Q5/065 , C09B51/00
摘要： New 1,4-diamino-5-chloro-2-nitrobenzene derivatives are disclosed of the formula I ##STR1## Wherein R.sup.1 and R.sup.2 are the same or different and are each hydrogen, 2-hydroxyethyl or 2,3-dihydroxypropyl, with the proviso, that at least one of said R.sup.1 and R.sup.2 is 2,3-dihydroxypropyl, along with processes for their production, as well as hair coloring compositions containing the same and methods of coloring hair. The compounds are red- to violet-coloring direct dyes, and are readily soluble in water, with favorable toxicological characteristics.
摘要翻译：新的1,4-二氨基-5-氯-2-硝基苯衍生物公开了式I（I），其中R1和R2相同或不同，各自为氢，2-羟乙基或2,3-二羟丙基条件是所述R 1和R 2中的至少一个是2,3-二羟基丙基，以及它们的制备方法，以及含有该染色组合物的毛发着色组合物和染发剂的方法。这些化合物是红色至紫色着色的直接染料，易溶于水，具有良好的毒理特性。

8. 发明授权

US4661114A 3-Amino-5-hydroxypyridine derivatives and hair coloring compositions containing the same 失效
标题翻译： 3-氨基-5-羟基吡啶衍生物和含有它们的头发着色组合物
公开(公告)号：US4661114A
公开(公告)日：1987-04-28
申请号：US798018
申请日：1985-11-14
申请人： Eugen Konrad , Thomas Clausen
发明人： Eugen Konrad , Thomas Clausen
IPC分类号： A61K8/00 , A61K8/33 , A61K8/35 , A61K8/40 , A61K8/41 , A61K8/49 , A61K31/44 , A61Q5/10 , C07D213/73 , C07D213/75 , A61K31/40 , C07D213/72
CPC分类号： C07D213/73 , A61K8/4926 , A61Q5/10
摘要： New 3-amino-5-hydroxypyridine derivatives are disclosed, of the formula I ##STR1## wherein R.sup.1 and R.sup.2 are independently CH.sub.3, C.sub.2 H.sub.5 or C.sub.2 H.sub.4 OH, and its physiologically compatible salts, as well as oxidation hair coloring compositions based upon the compounds of general formula I as coupler substance. The oxidation hair coloring compositions based upon the new couplers, of which the 3-amino-5-hydroxy-2,6-dimethoxypyridine is preferred, are particularly suitable in combination with known developer substances to obtaining red, red-brown, bond and orange colored tones. The new coupler substances of formula I prove to have favorable toxicological and dermatological characteristics.
摘要翻译：公开了新的3-氨基-5-羟基吡啶衍生物，其具有式I（I）其中R 1和R 2独立地是CH 3，C 2 H 5或C 2 H 4 OH，及其生理上相容的盐，以及基于通式I的化合物作为成色剂物质。基于其中优选3-氨基-5-羟基-2,6-二甲氧基吡啶的新成色剂的氧化毛发着色组合物特别适合与已知的显影剂物质组合以获得红色，红棕色，结合和橙色彩色色调。式I的新成色剂物质证明具有有利的毒理学和皮肤病学特征。

9. 发明申请

US20120327957A1 DATA PACKET SYNCHRONIZATION AND RETURN-TO-ZERO CONVERSION 审中-公开
标题翻译：数据包同步和返回到零转换
公开(公告)号：US20120327957A1
公开(公告)日：2012-12-27
申请号：US13576148
申请日：2011-02-01
申请人： Leif Katsuo Oxenlowe , Michael Galili , Anders Thomas Clausen
发明人： Leif Katsuo Oxenlowe , Michael Galili , Anders Thomas Clausen
IPC分类号： H04J3/06 , H04B10/00 , H04L7/06
CPC分类号： H04L7/0075 , H04J3/0685 , H04J14/08 , H04J14/086 , H04L7/0091
摘要： The present invention relates to a system and method that enable transmission of multiple data packet lines as an optical time-division multiplexed signal. The invention provides a method and system that can synchronize data packet signals to a clock and convert them into return-to-zero signals. When multiple data packet lines are converted, they can be multiplexed together and transmitted according to well-known methods.
摘要翻译：本发明涉及能够将多条数据包线路作为光时分复用信号传输的系统和方法。本发明提供了一种方法和系统，其可以将数据分组信号同步到时钟并将其转换成归零信号。当多个数据分组线被转换时，它们可以被多路复用在一起并按照众所周知的方法发送。

10. 发明授权

US5674476A Process for making a persulfate-containing granulate for decolorizing or bleaching hair 失效
标题翻译：制造含过硫酸盐的颗粒以脱色或漂白毛发的方法
公开(公告)号：US5674476A
公开(公告)日：1997-10-07
申请号：US612533
申请日：1996-03-08
申请人： Thomas Clausen , Wolfgang R. Balzer , Volker Port , Jolanthe Kujawa
发明人： Thomas Clausen , Wolfgang R. Balzer , Volker Port , Jolanthe Kujawa
IPC分类号： A61K8/00 , A45D19/00 , A61K8/04 , A61K8/21 , A61K8/34 , A61K8/86 , A61Q5/08 , B01J2/10 , C08L39/06 , C08L71/02 , A61K7/135
CPC分类号： A61Q5/08 , A61K8/0275 , A61K2800/51
摘要： The method of making a granulate composition for decolorizing or bleaching hair consists of preparing a powdery mixture consisting of from 30 to 65% by weight of one or more inorganic persulfates, from 1 to 20% by weight of a binding agent selected from the group consisting of polyvinylpyrrolidone and polyethylene glycols having molecular weights of 200 to 10,000; of 15 to 45% by weight of at least one salt selected from the group consisting of alkali metal carbonates, alkaline earth metal carbonates, alkali metal hydrogen carbonates, alkali metal silicates and from 0.1 to 3 percent by weight of a chelating agent, and one or more auxiliary and additive substance selected from the group consisting of perfume oils, hair dyes, amphoteric, anionic, cationic and nonionic surface-active substances and water-soluble thickeners; after making this powdery mixture, spraying ethanol and/or isopropanol in a weight ratio from 13:1 to 4:1 (powdery mixture to alcohol) into the powdery mixture to form a moistened mixture; granulating the moistened mixture formed during the spraying in a granulating apparatus to form a moist granulate; and after the granulating, drying the moist granulate to remove the alcohol or alcohols and to form the granulate composition.
摘要翻译：制备用于脱色或漂白毛发的颗粒组合物的方法包括制备由30至65重量％的一种或多种无机过硫酸盐，1至20重量％的选自以下的粘合剂组成的粉末混合物：的聚乙烯吡咯烷酮和分子量为200至10,000的聚乙二醇; 15至45重量％的至少一种选自碱金属碳酸盐，碱土金属碳酸盐，碱金属碳酸氢盐，碱金属硅酸盐和0.1至3重量％螯合剂的盐，以及一种或更多选自香水油，染发剂，两性，阴离子，阳离子和非离子表面活性物质和水溶性增稠剂的辅助和添加剂物质; 在制备该粉末混合物之后，将重量比为13:1至4:1的乙醇和/或异丙醇（粉末混合物至醇）喷入粉末混合物中以形成润湿的混合物; 将在喷雾期间形成的润湿混合物造粒在造粒设备中以形成湿颗粒; 在造粒后，干燥湿颗粒以除去醇或醇并形成颗粒组合物。

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