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1. 发明申请

US20080035898A1 Manufacturing Method and Usage of Crystallized Metal Oxide Thin Film 有权
标题翻译：结晶金属氧化物薄膜的制造方法和用途
公开(公告)号：US20080035898A1
公开(公告)日：2008-02-14
申请号：US11836387
申请日：2007-08-09
申请人： Tetsuo Tsuchiya , Tomohiko Nakajima , Akio Watanabe , Toshiya Kumagai
发明人： Tetsuo Tsuchiya , Tomohiko Nakajima , Akio Watanabe , Toshiya Kumagai
IPC分类号： B05D3/06 , C01B13/00
CPC分类号： H01G4/10 , C09K11/7787 , C23C18/14 , C30B23/06 , C30B25/105 , C30B29/16 , H01L39/2461
摘要： Provided is a manufacturing method of a crystallized rare-earth thin films on a glass or a silicon substrate. This manufacturing method of a crystallized metal oxide thin film includes a step of retaining an metal organic thin film or a metal oxide film containing at least one type of rare-earth metal element selected from a group comprised of Y, Dy, Sm, Gd, Ho, Eu, Tm, Tb, Er, Ce, Pr, Yb, La, Nd and Lu formed on a substrate at a temperature of 250 to 600° C., and a step of crystallizing the organic metal thin film or the metal oxide film while irradiating ultraviolet radiation having a wavelength of 200 nm or less.
摘要翻译：提供了在玻璃或硅基板上的结晶化稀土类薄膜的制造方法。该结晶化金属氧化物薄膜的制造方法包括：保持金属有机薄膜或金属氧化物膜的工序，所述金属有机薄膜或金属氧化物膜含有选自Y，Dy，Sm，Gd中的至少一种稀土金属元素，在250〜600℃的温度下在基板上形成的Ho，Eu，Tm，Tb，Er，Ce，Pr，Yb，La，Nd和Lu，以及将有机金属薄膜或金属氧化物同时照射波长为200nm以下的紫外线。

2. 发明授权

US06774088B2 Rare earth-Ba-Cu complex composition and method of producing superconductor using same 失效
标题翻译：稀土 - Ba-Cu络合物的组成及使用其制造超导体的方法
公开(公告)号：US06774088B2
公开(公告)日：2004-08-10
申请号：US10086377
申请日：2002-03-04
申请人： Takaaki Manabe , Iwao Yamaguchi , Tetsuo Tsuchiya , Toshiya Kumagai , Susumu Mizuta , Susumu Nakamura
发明人： Takaaki Manabe , Iwao Yamaguchi , Tetsuo Tsuchiya , Toshiya Kumagai , Susumu Mizuta , Susumu Nakamura
IPC分类号： H01B100
CPC分类号： H01L39/2425 , C23C18/1216 , C23C18/1295 , Y10S505/70 , Y10S505/734 , Y10S505/741
摘要： A metal complex composition containing complexes having metal species of a rare earth element, barium and copper and ligands of a trifluoroacetic acid or pentafluoropropionic acid ligand, a pyridine ligand and an acetylacetone ligand. A superconductive film may be obtained by applying an organic solvent solution of the above metal complex composition to a substrate and by heat treating the coating.
摘要翻译：含有具有稀土元素金属物质，钡和铜以及三氟乙酸或五氟丙酸配体配体，吡啶配体和乙酰丙酮配体的配合物的金属络合物组合物。可以通过将上述金属络合物组合物的有机溶剂溶液涂布到基材上并通过热处理涂层来获得超导膜。

3. 发明授权

US5624889A Lubricating grease composition 失效
标题翻译：润滑脂组合物
公开(公告)号：US5624889A
公开(公告)日：1997-04-29
申请号：US565017
申请日：1995-11-30
申请人： Takahiro Ozaki , Tomoo Munakata , Yasushi Kawamura , Kazunori Takase , Tetsuo Tsuchiya
发明人： Takahiro Ozaki , Tomoo Munakata , Yasushi Kawamura , Kazunori Takase , Tetsuo Tsuchiya
IPC分类号： C10M169/06 , C10N10/12 , C10N30/06 , C10N30/08 , C10N40/02 , C10N50/10 , C10M141/06
CPC分类号： C10M169/06 , C10M2201/0606 , C10M2201/0616 , C10M2201/0626 , C10M2201/0656 , C10M2201/0666 , C10M2201/0806 , C10M2201/085 , C10M2201/0856 , C10M2201/0866 , C10M2201/0876 , C10M2201/1013 , C10M2201/1026 , C10M2207/281 , C10M2207/282 , C10M2207/283 , C10M2207/286 , C10M2215/006 , C10M2215/026 , C10M2215/0813 , C10M2215/1013 , C10M2215/102 , C10M2215/1026 , C10M2215/121 , C10M2215/2206 , C10M2215/2275 , C10M2217/044 , C10M2217/045 , C10M2219/066 , C10M2219/068 , C10M2223/045 , C10M2223/047 , C10N2210/06 , C10N2240/00 , C10N2240/02 , C10N2240/22 , C10N2240/30 , C10N2240/50 , C10N2240/52 , C10N2240/54 , C10N2240/56 , C10N2240/58 , C10N2240/60 , C10N2240/66
摘要： A lubricating grease composition includes a grease containing a base oil and a thickening agent consisting of a mixture of tricalcium phosphate represented by the formulaCa.sub.3 (PO.sub.4).sub.2and a urea compound and, incorporated as additives in the grease, (A) a sulfurized molybdenum dialkyldithiocarbamate represented by the formula ##STR1## wherein R.sup.1 and R.sup.2 each independently represents a group selected from the group consisting of alkyl groups having from 1 to 24 carbon atoms; m is 0 or an integer of from 1 to 3; and n is an integer of from 1 to 4; provided that m+n=4, and (B) triphenyl phosphorothionate represented by the formula ##STR2##
摘要翻译：润滑脂组合物包括含有基础油的润滑脂和由式Ca 3（PO 4）2表示的磷酸三钙和尿素化合物的混合物组成的增稠剂，并且作为添加剂掺入润滑脂中，（A）表示为二烷基二硫代氨基甲酸硫化的硫化钼其中R 1和R 2各自独立地表示选自具有1至24个碳原子的烷基的基团; m为0或1〜3的整数; n为1〜4的整数，条件是m + n = 4，和（B）由式“IMAGE”表示的磷酸三苯酯

4. 发明授权

US09187842B2 Oriented perovskite oxide thin film 有权
标题翻译：取向的钙钛矿氧化物薄膜
公开(公告)号：US09187842B2
公开(公告)日：2015-11-17
申请号：US13640760
申请日：2011-04-12
申请人： Tomohiko Nakajima , Tetsuo Tsuchiya , Takaaki Manabe
发明人： Tomohiko Nakajima , Tetsuo Tsuchiya , Takaaki Manabe
IPC分类号： C30B29/24 , C30B1/02 , C03C17/00 , C03C17/23 , C04B35/465 , C04B35/468 , C04B35/495 , C30B7/06 , C30B29/30 , H01L41/187 , C30B1/04 , C30B1/10
CPC分类号： C30B1/023 , C03C17/001 , C03C17/23 , C03C2217/23 , C04B35/465 , C04B35/4682 , C04B35/495 , C04B2235/3201 , C04B2235/3205 , C04B2235/3208 , C04B2235/3213 , C04B2235/3224 , C04B2235/3227 , C04B2235/3232 , C04B2235/3244 , C04B2235/3251 , C04B2235/3258 , C04B2235/3291 , C04B2235/3298 , C04B2235/441 , C04B2235/665 , C04B2235/768 , C04B2235/787 , C30B1/04 , C30B1/10 , C30B7/06 , C30B29/30 , H01L41/1871 , H01L41/1873
摘要： A thin film which comprises an organic metal salt or an alkoxide salt or an amorphous thin film is formed on a substrate, wherein each of the thin films enables the formation of a Dion-Jacobson perovskite-type metal oxide represented by the composition formula A(Bn−1MnO3n+1) (wherein n is a natural number of 2 or greater; A represents one or more monovalent cations selected from Na, K, Rb and Cs; B comprises one or more components selected from a trivalent rare earth ion, Bi, a divalent alkaline earth metal ion and a monovalent alkali metal ion; and M comprises one or more of Nb and Ta; wherein a solid solution may be formed with Ti and Zr) on a non-oriented substrate. The resulting product is maintained at the temperature between room temperature and 600° C.; and crystallization is achieved while irradiating the amorphous thin film or the thin film comprising the organic metal salt or the alkoxide salt on the substrate with ultraviolet light such as ultraviolet laser. In this manner, it becomes possible to produce an oriented Dion-Jacobson perovskite-type oxide thin film characterized in that thin film can be oriented on the substrate in a (001) direction.
摘要翻译：在基材上形成包含有机金属盐或醇盐或非晶态薄膜的薄膜，其中每个薄膜能够形成由组成式A表示的Dion-Jacobson钙钛矿型金属氧化物（ Bn-1MnO3n + 1）（其中n为2或更大的自然数; A表示选自Na，K，Rb和Cs中的一种或多种一价阳离子; B包含一种或多种选自三价稀土离子，Bi ，二价碱土金属离子和一价碱金属离子; M包括Nb和Ta中的一种或多种;其中在非取向基底上可以用Ti和Zr形成固溶体）。所得产物保持在室温至600℃之间的温度。并且在用紫外线激光等紫外线照射基板上的非晶质薄膜或由有机金属盐或醇盐构成的薄膜的同时进行结晶化。以这种方式，可以制备定向的Dion-Jacobson钙钛矿型氧化物薄膜，其特征在于薄膜可以在（001）方向上在基板上取向。

5. 发明授权

US08557352B2 Method of making a metal oxide film, laminates and electronic devices 有权
标题翻译：制造金属氧化物膜，层压板和电子器件的方法
公开(公告)号：US08557352B2
公开(公告)日：2013-10-15
申请号：US11812506
申请日：2007-06-19
申请人： Yuki Miyamoto , Tetsuo Tsuchiya
发明人： Yuki Miyamoto , Tetsuo Tsuchiya
IPC分类号： B05D3/00 , B05D3/06 , B05D3/02 , C08J7/18 , C23C14/28
CPC分类号： C23C18/14 , C23C18/1216 , C23C18/1241 , C23C18/1283 , C23C18/1295 , H01G4/1209 , H01G4/1227 , H01G4/33
摘要： An object is to provide a method of making a metal oxide film with a sufficiently high degree of crystal orientation, without difficulties, at low cost, and with little damage to a base material and the metal oxide film, and to provide laminates and electronic devices using the same. A method includes a step of forming a metal film having a (111) plane, on a base material; a step of forming a metal oxide film on the (111) plane of the metal film; and a step of maintaining a temperature of the metal oxide film formed on the (111) plane of the metal film, at 25-600° C. and irradiating the metal oxide film with UV light.
摘要翻译：本发明的目的是提供一种以低成本制造具有足够高的晶体取向度的金属氧化物膜的方法，并且对基材和金属氧化物膜几乎没有损伤，并且提供层压板和电子器件使用相同一种方法包括在基材上形成具有（111）面的金属膜的步骤; 在金属膜的（111）面上形成金属氧化物膜的工序; 以及在金属膜的（111）面上形成的金属氧化物膜的温度保持在25〜600℃的步骤，并用紫外线照射金属氧化物膜。

6. 发明申请

US20090318296A1 Method of Producing Superconductive Oxide Material 有权
公开(公告)号：US20090318296A1
公开(公告)日：2009-12-24
申请号：US12227840
申请日：2008-02-05
申请人： Mitsugu Sohma , Tetsuo Tsuchiya , Toshiya Kumagai , Kenichi Tsukada , Kunihiko Koyanagi , Takashi Ebisawa , Hidehiko Ohtu
发明人： Mitsugu Sohma , Tetsuo Tsuchiya , Toshiya Kumagai , Kenichi Tsukada , Kunihiko Koyanagi , Takashi Ebisawa , Hidehiko Ohtu
IPC分类号： H01L39/24
CPC分类号： H01L39/2425 , C23C18/1216 , C23C18/1245 , C23C18/1295 , C23C18/14 , H01L39/2451
摘要： The invention provides a method of efficiently producing a superconductive material more excellent in properties without the occurrence of ablation and so forth, and large in area when executing thermal decomposition of an organic compound of metals, and formation of a superconductive material with heat treatment. The method of producing a superconductive material comprising the step (1) of applying a solution of an organic compound of metals, oxides of the metals forming a superconductive material, onto a support body to be subsequently dried, the provisional baking step (2) of causing organic components of the organic compound of the metals to undergo thermal decomposition, and the main baking process step (3) of causing transformation of the oxides of the metals into the superconductive material, thereby producing an epitaxially-grown superconductive coating material, wherein at the time of irradiation of a surface of the support body coated with the solution of the organic compound of the metals for forming the superconductive material, and/or of a surface of the support body, opposite to the surface coated with the solution of the organic compound of the metals, with the laser light, during a period between the steps (1) and (2), it is executed under the conditions adopting the following range. intensity and the number of pulses of the laser light; 5 mJ/cm2≦intensity of the laser light F≦200 mJ/cm2 1≦the number of pulses P≦198000000 total energy of the laser light; (0.03 J/cm2×a substrate constant)≦total energy≦(89000 J/cm2×a substrate constant) (in the expression, the substrate constant is defined as a number not less than 1 in value, dependent on nature and thickness of the support body) an irradiation condition area surrounded by the straight lines having the following equations; log10 P=K1F+K2 log10 P=K1F+K3 (in the equations, K1 represents a slant connecting between a point F corresponding to an arbitrary point P where transformation into the superconductive material occurs first and a point P corresponding to an arbitrary point F where transformation into the superconductive material occurs first, K2 is a logarithmic value at the point P in F=0 where a value at the point P in F=5 where transformation into the superconductive material occurs first is outwardly inserted along the slant K1, and K3 is a logarithmic value at the point P in F=0 where a value at the point P in F=5 where ablation occurs first is outwardly inserted along the slant K1, where K3>K2 is established).

7. 发明申请

US20090246405A1 METHOD FOR PRODUCING PEROVSKITE-STRUCTURE OXIDE 有权
标题翻译：生产氧化钇结构氧化物的方法
公开(公告)号：US20090246405A1
公开(公告)日：2009-10-01
申请号：US12410029
申请日：2009-03-24
申请人： Tetsuo TSUCHIYA , Yuki YAMASHITA , Masato SUSUKIDA
发明人： Tetsuo TSUCHIYA , Yuki YAMASHITA , Masato SUSUKIDA
IPC分类号： C08J7/18
CPC分类号： C01G23/006 , C01G23/002 , C01P2002/34 , C01P2002/72
摘要： The present invention provides a method for producing a perovskite-structure oxide, with which a highly crystalline oxide layer is formed on a base layer that is metal or the like. The method comprises the steps of: forming, on a base layer, a buffer layer having thermal conductivity lower than thermal conductivity of the base layer; forming a precursor layer of an ABO3-type perovskite-structure oxide comprising Ba at A sites thereof and Ti at B sites thereof on the buffer layer; decomposing the precursor layer, thereby forming an oxide layer comprising Ba and Ti; and annealing the oxide layer by irradiating laser light thereon.
摘要翻译：本发明提供一种钙钛矿结构氧化物的制造方法，在金属等的基底层上形成高结晶性氧化物层。该方法包括以下步骤：在基层上形成导热率低于基层导热率的缓冲层; 在其位置上形成包含Ba的ABO 3型钙钛矿结构氧化物的前体层和其B位的Ti在缓冲层上; 分解前体层，从而形成包含Ba和Ti的氧化物层; 以及通过在其上照射激光来对氧化物层进行退火。

8. 发明授权

US06624384B2 Method for manufacturing infrared ray sensor 有权
公开(公告)号：US06624384B2
公开(公告)日：2003-09-23
申请号：US09984853
申请日：2001-10-31
申请人： Tetsuo Tsuchiya , Susumu Mizuta , Toshiya Kumagai , Tsutomu Yoshitake , Yuichi Shimakawa , Yoshimi Kubo
发明人： Tetsuo Tsuchiya , Susumu Mizuta , Toshiya Kumagai , Tsutomu Yoshitake , Yuichi Shimakawa , Yoshimi Kubo
IPC分类号： B23K2600
CPC分类号： C23C26/02 , G01J5/20
摘要： In an infrared ray sensor for a bolometer, a bridge structure body, a resistive element film for the bolometer, and a protection film is formed via a space on a substrate, and is formed into a solution form by dissolving metal organic compound into solvent. The solution is applied and dried. A laser ray is irradiated for the solution with wavelength of 400 nm or less. A bond between carbon and oxygen is decomposed and cut to thereby form an oxide thin-film.

9. 发明授权

US5449471A Urea grease compostition 失效
标题翻译：尿素油脂组合物
公开(公告)号：US5449471A
公开(公告)日：1995-09-12
申请号：US249033
申请日：1994-05-25
申请人： Takahiro Ozaki , Yasushi Kawamura , Tetsuo Tsuchiya , Fumio Goto , Hideaki Tsuyuki , Kazuhiro Miyajima , Takashi Matsuda , Nobuhiko Okano , Hirofumi Mochizuki
发明人： Takahiro Ozaki , Yasushi Kawamura , Tetsuo Tsuchiya , Fumio Goto , Hideaki Tsuyuki , Kazuhiro Miyajima , Takashi Matsuda , Nobuhiko Okano , Hirofumi Mochizuki
IPC分类号： C10M169/02 , C10M169/06 , C10N10/12 , C10N30/02 , C10N30/06 , C10N40/02 , C10N40/04 , C10N50/10 , C10M115/08 , C10M135/18
CPC分类号： C10M169/06 , C10M2215/006 , C10M2215/026 , C10M2215/0813 , C10M2215/1013 , C10M2215/102 , C10M2215/1026 , C10M2215/121 , C10M2215/2206 , C10M2215/2275 , C10M2217/044 , C10M2217/045 , C10M2219/066 , C10M2219/068 , C10M2223/045 , C10M2223/047 , C10N2240/02
摘要： A urea grease composition is disclosed, which comprises a urea grease and, incorporated therein as additives, a sulfurized molybdenum dialkyldithiocarbamate represented by formula (A): ##STR1## wherein R.sub.1 and R.sub.2 each independently represent an alkyl group having from 1 to 24 carbon atoms, m+n=4, m is 0 to 3, and n is 4 to 1 and triphenyl phosphorothionate represented by formula (B): ##STR2##
摘要翻译：公开了一种尿素润滑脂组合物，其包含尿素润滑脂，并且作为添加剂掺入由式（A）表示的硫化二烷基二硫代氨基甲酸钼：其中R 1和R 2各自独立地表示具有1至24个碳原子的烷基，m + n = 4，m为0〜3，n为4〜1，式（B）表示的磷酸三苯酯：

10. 发明授权

US08871363B2 Resistor film for bolometer 有权
标题翻译：测辐射热敏电阻膜
公开(公告)号：US08871363B2
公开(公告)日：2014-10-28
申请号：US13393556
申请日：2010-09-01
申请人： Tetsuo Tsuchiya , Masami Nishikawa , Tomohiko Nakajima , Toshiya Kumagai , Takaaki Manabe
发明人： Tetsuo Tsuchiya , Masami Nishikawa , Tomohiko Nakajima , Toshiya Kumagai , Takaaki Manabe
IPC分类号： B32B5/14 , B32B9/00 , C01G31/02 , G01J5/20 , H01C3/04 , H01C17/065 , H01C7/02 , G01J5/02 , G01J5/04
CPC分类号： H01C17/06533 , C01G31/02 , C01P2002/02 , C01P2002/04 , C01P2002/80 , C01P2006/90 , G01J5/024 , G01J5/046 , G01J5/20 , H01C7/026 , H01L21/02565 , H01L21/02581 , Y10T428/12458 , Y10T428/12493 , Y10T428/12611
摘要： Provided is a resistor film comprising vanadium oxide as a main component, wherein metal-to-insulator transition is indicated in the vicinity of room temperature in temperature variations of electric resistance, there is no hysteresis in a resistance change in response to temperature variations or the temperature width is small at less than 1.5K even if there is hysteresis, and highly accurate measurement can be provided when used in a bolometer.Upon producing the resistor film comprising vanadium oxide as a main component by treating a coating film of an organovanadium compound via laser irradiation or the like, a crystalline phase and a noncrystalline (amorphous) phase are caused to coexist in the resistor film.
摘要翻译：提供了包含氧化钒作为主要成分的电阻膜，其中金属 - 绝缘体转变在室温附近在电阻的温度变化中表示，在温度变化或电流变化的电阻变化中没有迟滞温度宽度小于1.5K，即使有迟滞，并且在测辐射热计中使用时可以提供高精度的测量。通过经由激光照射等处理有机体化合物的涂膜而制造包含氧化钒作为主要成分的电阻膜时，结晶相和非结晶（非晶）相共存在电阻膜中。

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