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1. 发明授权

US5637705A Bisazo compounds and use thereof as fiber reactive dyes 失效
标题翻译：双偶氮化合物及其作为纤维活性染料的用途
公开(公告)号：US5637705A
公开(公告)日：1997-06-10
申请号：US532510
申请日：1995-09-22
申请人： Sigeru Sasaki , Kingo Akahori , Takeshi Washimi , Takashi Omura , Toshiyuki Araki , Atsushi Inoue
发明人： Sigeru Sasaki , Kingo Akahori , Takeshi Washimi , Takashi Omura , Toshiyuki Araki , Atsushi Inoue
IPC分类号： C09B62/513 , C07D251/52 , C07D251/54
CPC分类号： C09B62/513
摘要： A bisazo compound of the following formula: ##STR1## wherein R.sup.1 and R.sup.3 are each hydrogen or alkyl; D is phenylene or naphthylene; one of X.sup.1 and X.sup.2 is NH.sub.2 and the other is OH; Z.sup.1 and Z.sup.2 are each --CH.dbd.CH.sub.2 or --CH.dbd.CH.sub.2 Z' in which Z' is a splittable group; B is monosulfophenylene, monosulfophenylene-methylene or mono- or di-sulfonaphthylene-methylene; U is phenylene or an aliphatic bridging group; and J is an amono-derivative group or, J may be alkoxy when X.sup.1 is OH and U is phenylene, and J may be alkoxy or phenoxy when X.sup.1 is OH and U is the aliphatic bridging group. This compound is useful for dyeing or printing fiber materials and gives a dyed or printed product having a color superior in various fastness properties with superior build-up property.
摘要翻译：下式的双偶氮化合物：其中R 1和R 3各自为氢或烷基; D是亚苯基或亚萘基; X1和X2之一是NH2，另一个是OH; Z 1和Z 2各自为-CH = CH 2或-CH = CH 2 Z'，其中Z'为可裂组; B是单磺酰亚砜，单磺酰亚苯基 - 亚甲基或单 - 或二 - 磺基亚乙基 - 亚甲基; U是亚苯基或脂族桥基; 并且J是氨基衍生基团，或者当X1是OH且U是亚苯基时，J可以是烷氧基，当X 1是OH且U是脂族桥基时，J可以是烷氧基或苯氧基。该化合物可用于染色或印刷纤维材料，并提供具有优异的各种牢度性能的优异的成色性能的染色或印刷产品。

2. 发明授权

US5324329A Reactive dye composition and dyeing or printing process using the same 失效
标题翻译：活性染料组合物和染色或印刷方法使用相同
公开(公告)号：US5324329A
公开(公告)日：1994-06-28
申请号：US76962
申请日：1993-06-16
申请人： Takeshi Washimi , Naoki Harada , Shuhei Hashizume , Takashi Omura
发明人： Takeshi Washimi , Naoki Harada , Shuhei Hashizume , Takashi Omura
IPC分类号： C09B67/24 , C09B62/44 , C09B67/22 , D06P1/384 , D06P3/66 , C09B62/00
CPC分类号： C09B67/0052 , C09B62/4413 , Y10S8/918
摘要： A reactive dye composition containing at least one dye of the formula (I) in the free acid form: ##STR1## wherein m is zero or 1; R.sub.1 is hydrogen, lower alkyl or lower alkoxy; R.sub.2 and R.sub.3 are independently hydrogen or substituted or unsubstituted lower alkyl; A is substituted or unsubstituted phenylene or naphthylene; X.sub.1 is halogen, --N(R.sub.4)R.sub.5 or --OR.sub.6 in which R.sub.4, R.sub.5 and R.sub.6 are independently hydrogen or substituted or unsubstituted alkyl, phenyl or naphthyl; and Y.sub.1 is the group --SO.sub.2 CH.dbd.CH.sub.2 or the group --SO.sub.2 CH.sub.2 CH.sub.2 Z.sub.1 in which Z.sub.1 is a group splittable by the action of an alkali, and at least one dye of the formula (II) in the free acid form: ##STR2## wherein n is zero, 1 or 2; one of W.sub.1 and W.sub.2 is hydrogen and the other is sulfo; R.sub.7 is hydrogen or substituted or unsubstituted lower alkyl; B is substituted or unsubstituted phenylene or naphthylene; X.sub.2 is --N(R.sub.8)R.sub.9, --OR.sub.10 in which R.sub.8, R.sub.9 and R.sub.10 are independently hydrogen or substituted or unsubstituted alkyl, phenyl, naphthyl, pyridinio, morpholino or piperidino; and Y.sub.2 is the group --SO.sub.2 CH.dbd.CH.sub.2 or the group --SO.sub.2 CH.sub.2 CH.sub.2 Z.sub.2 in which Z.sub.2 is a group splittable by the action of an alkali, dyes or prints cellulose fiber materials or fiber materials containing a cellulose fiber to give a vivid, deep and highly fast red color.
摘要翻译：含有游离酸形式的至少一种式（I）染料的活性染料组合物：其中m为0或1; R1是氢，低级烷基或低级烷氧基; R2和R3独立地为氢或取代或未取代的低级烷基; A是取代或未取代的亚苯基或亚萘基; X 1是卤素，-N（R 4）R 5或-OR 6，其中R 4，R 5和R 6独立地是氢或取代或未取代的烷基，苯基或萘基; Y1是基团-SO2CH = CH2或基团-SO2CH2CH2Z1，其中Z1是可以通过碱作用而分裂的基团，以及至少一种游离酸形式的式（II）染料：II ）其中n为0,1或2; W1和W2之一是氢，另一个是磺基; R7是氢或取代或未取代的低级烷基; B是取代或未取代的亚苯基或亚萘基; X 2是-N（R 8）R 9，-OR 10，其中R 8，R 9和R 10独立地是氢或取代或未取代的烷基，苯基，萘基，吡啶基，吗啉代或哌啶子基; 并且Y2是基团-SO 2 CH = CH 2或基团-SO 2 CH 2 CH 2 Z 2，其中Z 2是可以通过碱的作用而分裂的基团，染料或印刷含纤维素纤维的纤维素纤维材料或纤维材料，以产生生动，深度和高度快速红色。

3. 发明授权

US5235046A Triazine compounds and method for dyeing or printing fiber materials using the same 失效
标题翻译：三氮唑化合物和使用该方法染色或印刷纤维材料的方法
公开(公告)号：US5235046A
公开(公告)日：1993-08-10
申请号：US793096
申请日：1991-11-18
申请人： Kingo Akahori , Masayuki Miki , Yutaka Kayane , Takeshi Washimi
发明人： Kingo Akahori , Masayuki Miki , Yutaka Kayane , Takeshi Washimi
IPC分类号： C09B62/04 , C09B62/085 , C09B62/503 , C09B62/505 , C09B62/51 , C09B62/513 , C09B62/515 , D06P1/38 , D06P1/384 , D06P3/66
CPC分类号： C09B62/503
摘要： A triazine compound which is useful for dyeing or printing materials containing hydroxyl group and/or amide group, and which has the following formula (I) or salts thereof ##STR1## wherein R represents hydrogen or unsubstituted or substituted alkyl; R.sub.1 represents hydrogen, an alkyl unsubstituted or substituted by carboxy, sulfo, alkoxy, halogeno, sulfato or hydroxy, or --Y--SO.sub.2 Z.sub.3 ; R.sub.2 represents hydrogen or unsubstituted or substituted alkyl; A represents unsubstituted or substituted phenylene or naphthylene; Y represents a divalent group which is C.sub.2 -C.sub.7 alkylene and so on; Z.sub.1, Z.sub.2 and Z.sub.3 independently of one another are each --CH.dbd.CH.sub.2 or --CH.sub.2 CH.sub.2 Z' wherein Z' is a group capable of being split by the action of an alkali; and F is any one of the dye residue which is anthraquinone, azo, disazo, trisazo or phthalocyanine nucleus and so on, and a process for dyeing or printing fiber materials which comprises using said triazine compounds or salts thereof.

4. 发明授权

US5606092A Monoazo compounds and method for dyeing or printing fiber materials using the same 失效
标题翻译：单偶氮化合物和使用其的纤维材料的染色或印花方法
公开(公告)号：US5606092A
公开(公告)日：1997-02-25
申请号：US546321
申请日：1995-10-20
申请人： Masayuki Miki , Kingo Akahori , Yutaka Kayane , Takeshi Washimi
发明人： Masayuki Miki , Kingo Akahori , Yutaka Kayane , Takeshi Washimi
IPC分类号： C09B62/085 , C09B62/44 , C09B62/51 , D06P1/384 , C07C317/28 , C07C317/34
CPC分类号： C09B62/4413 , C09B62/51
摘要： A monoazo compound of the following formula, ##STR1## wherein D is phenylene or naphthylene; X is halogeno, pyridinio or ##STR2## B is --OR.sub.3, --SR.sub.4, ##STR3## in which R.sub.3, R.sub.4, R.sub.5 and R.sub.6 are each hydrogen, alkyl, phenyl, naphthyl or benzyl, r is 0 or 1, and E is O, SO, SO.sub.2, CH.sub.2 or NR.sub.8, in which R.sub.8 is hydrogen or C.sub.1 -C.sub.4 alkyl; R, R.sub.1, R.sub.2 and R.sub.7 are each hydrogen or alkyl; A.sub.1, A.sub.2 and A.sub.3 are each phenylene, naphthylene or alkylene; Z.sub.1, Z.sub.2 and Z.sub.3 are each --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Y, in which Y is a splittable group; and p is 0 or 1; which compound is useful for dyeing or printing fiber materials to obtain a product dyed or printed in a color superior in various fastness properties with superior build-up property.
摘要翻译：下式的单偶氮化合物，其中D是亚苯基或亚萘基; X是卤素，吡啶鎓或B是-OR 3，-SR 4，其中R 3，R 4，R 5和R 6各自是氢，烷基，苯基，萘基或苄基，r是0或1，E是 O，SO，SO 2，CH 2或NR 8，其中R 8是氢或C 1 -C 4烷基; R，R 1，R 2和R 7各自为氢或烷基; A1，A2和A3各自为亚苯基，亚萘基或亚烷基; Z 1，Z 2和Z 3各自为-SO 2 CH = CH 2或-SO 2 CH 2 CH 2 Y，其中Y为可裂解基团; p为0或1; 该化合物可用于染色或印刷纤维材料以获得染色或印刷成具有优异的各种牢度性能的颜色的产品，具有优异的聚集性能。

5. 发明授权

US5770707A Monoazo compounds and dyeing or printing methods using the same 失效
标题翻译：单偶氮化合物和染色或印刷方法使用相同
公开(公告)号：US5770707A
公开(公告)日：1998-06-23
申请号：US605432
申请日：1996-02-22
申请人： Yoshimi Ebiike , Takeshi Washimi , Yasuyoshi Ueda , Takashi Omura
发明人： Yoshimi Ebiike , Takeshi Washimi , Yasuyoshi Ueda , Takashi Omura
IPC分类号： C09B62/51
CPC分类号： C09B62/51
摘要： A monoazo compound represented by the general formula (I): ##STR1## wherein D is an optionally substituted phenyl or an optionally substituted naphthyl; R and R.sup.1 are hydrogen or an optionally substituted lower alkyl; A is a naphthylene represented by the general formula (A1): ##STR2## m.sub.1 and m.sub.2 are 0 or 1; Y is an aliphatic connecting group Z is --CH.dbd.CH.sub.2 or --CH.sub.2 CH.sub.2 Z.sup.1 in which Z.sup.1 is a group removable by the action of an alkali; X is an aliphatic, aromatic, alicyclic, cyclic amino group, etc; and a method for dyeing or printing fiber materials using the monoazo compound.
摘要翻译：由通式（I）表示的单偶氮化合物：其中D是任选取代的苯基或任选取代的萘基; R和R 1是氢或任选取代的低级烷基; A是由通式（A1）表示的亚萘基：（IMA）（A1）m1和m2是0或1; Y是脂族连接基团Z是-CH = CH 2或-CH 2 CH 2 Z 1，其中Z 1是可以通过碱的作用除去的基团; X是脂肪族，芳香族，脂环族，环状氨基等; 以及使用单偶氮化合物染色或印刷纤维材料的方法。

6. 发明授权

US5720779A Anthraquinone reactive dye compositions and methods for dyeing or printing using the same 失效
标题翻译：蒽醌活性染料组合物和使用其的染色或印花方法
公开(公告)号：US5720779A
公开(公告)日：1998-02-24
申请号：US591267
申请日：1996-01-22
申请人： Yoshimi Ebiike , Takeshi Washimi , Yasuyoshi Ueda , Takashi Omura
发明人： Yoshimi Ebiike , Takeshi Washimi , Yasuyoshi Ueda , Takashi Omura
IPC分类号： C09B62/505 , C09B67/22 , D06P1/384
CPC分类号： C09B67/0038 , C09B62/505
摘要： A reactive dye composition comprising an anthraquinone compound(I) of the following formula: ##STR1## wherein Z represents --CH=CH2 or --CH2CH2Z.sup.1 in which Z.sup.1 represents a group splitable by the action of an alkali other than a carboxypyridinio group and an anthraquinone compound(II) of the following formula: ##STR2## and a method for dyeing or printing cellulose-containing fiber materials using the same.
摘要翻译：一种活性染料组合物，其包含下式的蒽醌化合物（I）：其中Z表示-CH = CH 2或-CH 2 CH 2 Z 1，其中Z 1表示可通过除羧基吡啶基以外的碱而分裂的基团和下式的蒽醌化合物（II）：＆lt; IMAGE＆gt;（II）和使用其的含纤维素纤维材料的染色或印花的方法。

7. 发明授权

US5488098A Monoazo compounds having vinylsulfone type fiber reactive group and method for dyeing or printing fiber materials using the same 失效
标题翻译：具有乙烯基砜型纤维反应性基团的单偶氮化合物和使用其的纤维材料的染色或印花方法
公开(公告)号：US5488098A
公开(公告)日：1996-01-30
申请号：US193646
申请日：1994-02-07
申请人： Masayuki Miki , Kingo Akahori , Yutaka Kayane , Takeshi Washimi
发明人： Masayuki Miki , Kingo Akahori , Yutaka Kayane , Takeshi Washimi
IPC分类号： C09B62/085 , C09B62/44 , C09B62/51 , D06P1/384
CPC分类号： C09B62/4413 , C09B62/51
摘要： A monoazo compound of the following formula, ##STR1## wherein D is phenylene or naphthylene; X is halogeno, pyridinio or ##STR2## B is --OR.sub.3, --SR.sub.4, ##STR3## in which R.sub.3, R.sub.4, R.sub.5 and R.sub.6 are each hydrogen, alkyl, phenyl, naphthyl or benzyl, r is 0 or 1, and E is O, SO, SO.sub.2, CH.sub.2 or NR.sub.8, in which R.sub.8 is hydrogen or C.sub.1 -C.sub.4 alkyl; R, R.sub.1, R.sub.2 and R.sub.7 are each hydrogen or alkyl; A.sub.1, A.sub.2 and A.sub.3 are each phenylene, naphthylene or alkylene; Z.sub.1, Z.sub.2 and Z.sub.3 are each --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Y, in which Y is a splittable group; and p is 0 or 1; which compound is useful for dyeing or printing fiber materials to obtain a product dyed or printed in a color superior in various fastness properties with superior build-up property.
摘要翻译：下式的单偶氮化合物，其中D是亚苯基或亚萘基; X是卤素，吡啶鎓或B是-OR 3，-SR 4，其中R 3，R 4，R 5和R 6各自是氢，烷基，苯基，萘基或苄基，r是0或1，E是 O，SO，SO 2，CH 2或NR 8，其中R 8是氢或C 1 -C 4烷基; R，R 1，R 2和R 7各自为氢或烷基; A1，A2和A3各自为亚苯基，亚萘基或亚烷基; Z 1，Z 2和Z 3各自为-SO 2 CH = CH 2或-SO 2 CH 2 CH 2 Y，其中Y为可裂解基团; p为0或1; 该化合物可用于染色或印刷纤维材料以获得染色或印刷成具有优异的各种牢度性能的颜色的产品，具有优异的聚集性能。

8. 发明授权

US5359040A Monoazo compounds having naphthylazonaphtylamino group and use therefor for dyeing or printing fiber materials 失效
标题翻译：具有萘氮杂萘基氨基的单偶氮化合物，用于染色或印刷纤维材料
公开(公告)号：US5359040A
公开(公告)日：1994-10-25
申请号：US963553
申请日：1992-10-20
申请人： Kingo Akahori , Masayuki Miki , Takeshi Washimi , Yutaka Kayane
发明人： Kingo Akahori , Masayuki Miki , Takeshi Washimi , Yutaka Kayane
IPC分类号： C07D251/54 , C09B62/085 , C09B62/51 , D06P1/384
CPC分类号： C09B62/51
摘要： A monoazo compound represented by the following formula (I) in the free acid form: ##STR1## wherein X is an alkylamino, C.sub.5 -C.sub.7 cycloalkylamino, piperidino, pyrrolidino or morpholino group which is unsubstituted or substituted with a substituent other than sulfo, R is hydrogen or unsubstituted or substituted C.sub.1 -C.sub.4 alkyl, R.sub.1 and R.sub.2 independently of one another are each hydrogen, methoxy, ethoxy, methyl, ethyl, chloro, bromo, nitro, carboxy or sulfo, Z is vinyl or -CH.sub.2 CH.sub.2 Y in which Y is a group which is split by the action of an alkali and p is 0 or 1. This compound is a reactive dye suitable for dyeing or printing fiber materials containing hydroxyl group and/or amide group in red color. This compound is high in dissolvability and can give dyed or printed products excellent in dyeability such as build-up property and various fastnesses.
摘要翻译：由游离酸形式的下式（I）表示的单偶氮化合物：其中X是未被取代或被取代基以外的取代基取代的烷基氨基，C 5 -C 7环烷基氨基，哌啶子基，吡咯烷子基或吗啉代基磺基，R为氢或未取代或取代的C 1 -C 4烷基，R 1和R 2各自独立地为氢，甲氧基，乙氧基，甲基，乙基，氯，溴，硝基，羧基或磺基，Z为乙烯基或-CH2CH2Y Y是通过碱的作用而分裂的基团，p是0或1.该化合物是适用于染色或印刷含有红色的羟基和/或酰胺基的纤维材料的活性染料。该化合物的溶解性高，可以赋予染色性，印染性等优异的染色性，例如聚集性和各种坚牢度。

9. 发明授权

US5306814A Bisazo compounds having sulfophenylazonaphtylazophenylamino-s-triazinyl group and use thereof for dyeing or printing fiber materials 失效
标题翻译：具有磺基苯基偶氮萘基偶氮苯基氨基-s-三嗪基的双偶氮化合物及其用于染色或印刷纤维材料的用途
公开(公告)号：US5306814A
公开(公告)日：1994-04-26
申请号：US993713
申请日：1992-12-17
申请人： Kingo Akahori , Takeshi Washimi , Takashi Omura , Mahito Fujita
发明人： Kingo Akahori , Takeshi Washimi , Takashi Omura , Mahito Fujita
IPC分类号： C09B62/09 , C09B62/513 , D06P1/384
CPC分类号： C09B62/513 , C09B62/09
摘要： A bisazo compound represented by the following formula (I) in the free acid form: ##STR1## wherein R is hydrogen or unsubstituted or substituted C.sub.1 -C.sub.4 alkyl; A is an unsubstituted or substituted phenylene or naphthylene group; Z is --SO.sub.2 CH.dbd.CH.sub.2 or --SO.sub.2 CH.sub.2 CH.sub.2 Y, in which Y is a group capable of being split by the action of an alkali; X is --NR.sub.1 R.sub.2, C.sub.5 -C.sub.7 cycloalkylamino or ##STR2## in which Q is --CH.sub.2 --, --O--, --SO.sub.2 --, --SO-- or --NR.sub.3 -- in which R.sub.3 is hydrogen or C.sub.1 -C.sub.4 alkyl; and n is 1 or 2; R.sub.1 is hydrogen or unsubstituted or substituted alkyl; R.sub.2 is hydrogen or an unsubstituted or substituted alkyl or phenyl group; and m is 1 or 2, provided that when m is 2, X is ##STR3## This compound is suitable for dyeing and printing cellulose fiber, natural and synthetic polyamide fibers, polyurethane fiber, leather and mixed yarns thereof, to obtain dyed or printed products of a color fast to light and wetness with superior build-up property.
摘要翻译：由游离酸形式的下式（I）表示的双偶氮化合物：（*化学结构*）（I）（*化学结构*）其中R为氢或未取代或取代的C 1 -C 4烷基; A是未取代或取代的亚苯基或亚萘基; Z是-SO 2 CH = CH 2或-SO 2 CH 2 CH 2 Y，其中Y是能够通过碱的作用而分裂的基团; X是-NR 1 R 2，C 5 -C 7环烷基氨基或（*化学结构*）其中Q是-CH 2 - ， - O - ， - SO 2 - ， - SO-或-NR 3 - ，其中R 3是氢或C 1 -C 4烷基; n为1或2; R1是氢或未取代或取代的烷基; R2是氢或未取代或取代的烷基或苯基; m为1或2，条件是当m为2时，X为（*化学结构*）该化合物适用于染色和印刷纤维素纤维，天然和合成聚酰胺纤维，聚氨酯纤维，皮革及其混纺纱线，以获得染色或印刷的产品，颜色快速，轻盈，具有优异的积聚性能。

10. 发明授权

US5478927A Bisazo compounds and use thereof as fiber reactive dyes 失效
标题翻译：双偶氮化合物及其作为纤维活性染料的用途
公开(公告)号：US5478927A
公开(公告)日：1995-12-26
申请号：US188755
申请日：1994-01-31
申请人： Sigeru Sasaki , Kingo Akahori , Takeshi Washimi , Takashi Omura , Toshiyuki Araki , Atsushi Inoue
发明人： Sigeru Sasaki , Kingo Akahori , Takeshi Washimi , Takashi Omura , Toshiyuki Araki , Atsushi Inoue
IPC分类号： C09B62/513 , D06P1/384
CPC分类号： C09B62/513
摘要： A bisazo compound of the following formula: ##STR1## wherein R.sup.1 and R.sup.3 are each hydrogen or alkyl; D is phenylene or naphthylene; one of X.sup.1 and X.sup.2 is NH.sub.2 and the other is OH; Z.sup.1 and Z.sup.2 are each --CH.dbd.CH.sub.2 or --CH.dbd.CH.sub.2 Z' in which Z' is a splittable group; B is monosulfophenylene, monosulfophenylene-methylene or mono- or di-sulfonaphthylene-methylene; U is phenylene or an aliphatic bridging group; and J is an amono-derivative group or, J may be alkoxy when X.sup.1 is OH and U is phenylene, and J may be alkoxy or phenoxy when X.sup.1 is OH and U is the aliphatic bridging group. This compound is useful for dyeing or printing fiber materials and gives a dyed or printed product having a color superior in various fastness properties with superior build-up property.
摘要翻译：下式的双偶氮化合物：其中R 1和R 3各自为氢或烷基; D是亚苯基或亚萘基; X1和X2之一是NH2，另一个是OH; Z 1和Z 2各自为-CH = CH 2或-CH = CH 2 Z'，其中Z'为可裂组; B是单磺酰亚砜，单磺酰亚苯基 - 亚甲基或单 - 或二 - 磺基亚乙基 - 亚甲基; U是亚苯基或脂族桥基; 并且J是氨基衍生基团，或者当X1是OH且U是亚苯基时，J可以是烷氧基，当X 1是OH且U是脂族桥基时，J可以是烷氧基或苯氧基。该化合物可用于染色或印刷纤维材料，并提供具有优异的各种牢度性能的优异的成色性能的染色或印刷产品。

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