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1. 发明申请

US20100036180A1 METHOD OF OBTAINING 1,2-DICHLOROETHANE BY DIRECT CHLORINATION WITH A STEP OF SEPARATION FROM THE CATALYST BY DIRECT EVAPORATION, AND FACILITY FOR THE IMPLEMENTATION THEREOF 审中-公开
标题翻译：通过直接氯化法从催化剂中分离直接氯化获得1,2-二氯乙烷的方法及其实施方法
公开(公告)号：US20100036180A1
公开(公告)日：2010-02-11
申请号：US12373388
申请日：2007-07-10
申请人： Philippe Leduc , Francois Vanney , Remy Teissier
发明人： Philippe Leduc , Francois Vanney , Remy Teissier
IPC分类号： C07C21/04 , B01J10/00
CPC分类号： C07C17/02 , C07C17/25 , C07C19/045 , C07C21/06
摘要： The present invention relates to a method of producing liquid 1,2-dichloroethane (DCE), obtained by low-temperature direct chlorination of ethylene, in the presence of a Lewis acid-type catalyst, that makes it possible to obtain, after separation of the catalyst, DCE of sufficient purity to give, via cracking, vinyl chloride monomer (VCM); characterized in that it comprises a step of dechlorination (5) of the liquid DCE stream (4) exiting the chlorination reactor (1), that makes it possible to remove the excess dissolved chlorine, followed by a step of direct evaporation (9) of the whole of the liquid DCE stream (8) exiting said reactor, that makes it possible to separate the catalyst from the evaporated fraction (10) of the stream of DCE good for cracking.The invention also relates to the plant for the implementation of such a method.
摘要翻译：本发明涉及一种在路易斯酸型催化剂存在下，通过乙烯的低温直接氯化得到的液体1,2-二氯乙烷（DCE）的制备方法，其可以在分离后催化剂，DCE具有足够的纯度，通过裂化得到氯乙烯单体（VCM）; 其特征在于它包括离开氯化反应器（1）的液体DCE流（4）的脱氯（5）的步骤，这使得可以除去过量的溶解氯，然后直接蒸发（9）离开所述反应器的整个液体DCE流（8），这使得可以将催化剂与DCE流的蒸发馏分（10）分离，以使其破裂。本发明还涉及用于实施这种方法的设备。

2. 发明申请

US20060014976A1 Continuous method for preparing ethyl lactate 失效
标题翻译：连续制备乳酸乙酯的方法
公开(公告)号：US20060014976A1
公开(公告)日：2006-01-19
申请号：US10537150
申请日：2003-12-05
申请人： Georges Martino-Gauchi , Remy Teissier
发明人： Georges Martino-Gauchi , Remy Teissier
IPC分类号： C07C67/08
CPC分类号： C07C67/08 , C07C69/68
摘要： The invention concerns a continuous method for preparing ethyl lactate by esterifying lactic acid with ethanol, in the presence of a catalyst which consists in reacting said lactic acid with ethanol in an initial ethanol/lactic acid mol ratio not less than 2.5, in the presence of a catalyst, at a reflux of the reaction medium of about 100° C. under absolute pressure ranging between 1.5 to 3 bars. Said method is characterized in that it consists in continuously extracting from the esterification reaction medium a near-azeotropic water/ethanol gas mixture; then in dehydrating said gas mixture directly using molecular sieves, then recuperating from said dehydration an ethanol gas stream capable of being recycled to the esterification reaction medium and a flow consisting of water and ethanol which is subjected to distillation wherefrom is obtained water and an azeotropic water/ethanol mixture which is injected into the distillation column head of the gas mixture extracted from the esterification reaction medium; then in continuously extracting crude ethyl lactate which is subjected to purification wherefrom are obtained high purity ethyl lactate and heavy products.
摘要翻译：本发明涉及通过在乙醇中酯化乳酸，在催化剂存在下制备乳酸乙酯的连续方法，所述催化剂包括在初始乙醇/乳酸摩尔比不小于2.5时使所述乳酸与乙醇反应，催化剂，在反应介质的回流下，在绝对压力范围为1.5至3巴之间约100℃。所述方法的特征在于其从酯化反应介质中连续提取近共沸水/乙醇气体混合物; 然后使用分子筛直接使所述气体混合物脱水，然后从所述脱水中回收能够再循环到酯化反应介质的乙醇气流和由水和乙醇组成的流，其中得到水和共沸水 /乙醇混合物，其被注入从酯化反应介质中提取的气体混合物的蒸馏塔头中; 然后连续提取经过纯化的粗乳酸乙酯，得到高纯度乳酸乙酯和重质产物。

3. 发明申请

US20050080201A1 Method for lactic acid oligomerization 审中-公开
标题翻译：乳酸低聚方法
公开(公告)号：US20050080201A1
公开(公告)日：2005-04-14
申请号：US10503375
申请日：2003-01-31
申请人： Remy Teissier , Serge Tretjak , Elie Burtin
发明人： Remy Teissier , Serge Tretjak , Elie Burtin
IPC分类号： B01D3/00 , B01D3/10 , B01J19/24 , C07C67/08 , C07C69/68 , C08L67/00
CPC分类号： B01J19/2465 , B01D3/009 , B01J19/24 , B01J2219/00094 , B01J2219/00182 , C07C67/08 , Y02P20/127 , C07C69/68
摘要： The invention concerns a method for continuously producing a dimmer-rich and tri-mer rich oligomeric lactic acid composition, starting with a lactic composition by eliminating water from said lactic acid composition. The invention is characterized in that it consists in: carrying out said elimination in an adiabatic reactor provided with a recycling loop, continuously introducing a lactic acid composition in a circulating starter reaction medium being brought to a temperature ranging between 120° C. and 180° C. and in eliminating the water vapour form.
摘要翻译：本发明涉及连续生产富二醇和三聚体低聚乳酸组合物的方法，其通过从所述乳酸组合物中除去水由乳酸组合物开始。本发明的特征在于：在具有循环回路的绝热反应器中进行所述消除，将循环起始反应介质中的乳酸组合物连续引入温度范围为120℃至180℃ 并消除水蒸气形式。

4. 发明授权

US06063944A Method for preparing lattice-inserted titanium zeolites, and use thereof 失效
标题翻译：晶格插入钛沸石的制备方法及其用途
公开(公告)号：US06063944A
公开(公告)日：2000-05-16
申请号：US195
申请日：1998-05-04
申请人： Francesco Di Renzo , Sylvie Gomez , Francois Fajula , Remy Teissier
发明人： Francesco Di Renzo , Sylvie Gomez , Francois Fajula , Remy Teissier
IPC分类号： B01J29/89 , C01B39/06 , C01B39/08 , C01B39/12 , C01B39/20 , C01B39/26 , C01B39/46 , C07D301/12
CPC分类号： C01B39/085 , B01J29/89 , C01B39/065 , C01B39/12
摘要： A method is provided for preparing fully lattice-inserted titanium zeolites by post-synthesis processing of the synthetic zeolite optionally containing titanium with an inorganic acid, wherein the post-synthesis processing comprises processing the zeolite in the presence of at least one titanium source with a solution containing at least one oxidizing inorganic acid having a higher redox potential than an acidic tetravalent titanium solution. The invention is also directed to the use of the zeolites.
摘要翻译： PCT No.PCT / FR96 / 01209 Sec。 371日期：1998年5月4日 102（e）日期1998年5月4日PCT提交1996年7月31日PCT公布。出版物WO97 / 05060 日期1997年2月13日提供了一种用于通过后处理合成沸石制备完全晶格插入的钛沸石的方法，所述合成沸石任选地含有钛与无机酸，其中后合成工艺包括在至少存在下处理沸石一种钛源与含有至少一种具有比酸性四价钛溶液更高的氧化还原电位的氧化性无机酸的溶液。本发明还涉及沸石的用途。

5. 发明授权

US06046366A Preparation of .beta.-hydroxycarbonyl and/or .alpha.,.beta.-unsaturated carbonyl compounds 失效
标题翻译： β-羟基羰基和/或α，β-不饱和羰基化合物的制备
公开(公告)号：US06046366A
公开(公告)日：2000-04-04
申请号：US206296
申请日：1998-12-07
申请人： Remy Teissier , Didier Tichit
发明人： Remy Teissier , Didier Tichit
IPC分类号： B01J23/76 , B01J23/00 , B01J23/06 , B01J23/08 , B01J23/755 , B01J23/825 , B01J23/835 , C07B61/00 , C07C45/72 , C07C45/74 , C07C49/17 , C07C49/203 , C07C45/45
CPC分类号： C07C45/74 , B01J23/002 , B01J23/007 , C07C45/72 , B01J2523/00
摘要： The invention relates to the use of compounds of formula:[M(II).sub.1-x M*(III).sub.x (OH).sub.2+x ].mH.sub.2 O (I)in which M(II) represents a divalent cation chosen from the group consisting of nickel, zinc, cobalt, magnesium or the mixture of two or more of the abovementioned metals; M(III) represents a trivalent cation, such as aluminum, gallium, iron or chromium, with the exception of the compound of formula (I) in which M(II) is magnesium and M(III) is aluminum, x is between 0.20 and 0.33 and m.ltoreq.1; in the preparation of .beta.-hydroxycarbonyl and/or .alpha.,.beta.-unsaturated carbonyl compounds.
摘要翻译：本发明涉及式[M（II）1-xM *（III）x（OH）2 + x]·mH 2 O（I）的化合物的用途，其中M（II）代表选自下组的二价阳离子由镍，锌，钴，镁或两种或更多种上述金属的混合物组成; M（III）表示三价阳离子，例如铝，镓，铁或铬，除了其中M（II）是镁和M（III）是铝的式（I）化合物之外，x在0.20 和0.33和m <1; 在β-羟基羰基和/或α，β-不饱和羰基化合物的制备中。

6. 发明授权

US5849957A Process for obtaining isophorone 失效
标题翻译：获得异佛尔酮的方法
公开(公告)号：US5849957A
公开(公告)日：1998-12-15
申请号：US808117
申请日：1997-02-28
申请人： Remy Teissier , Jacques Kervennal
发明人： Remy Teissier , Jacques Kervennal
IPC分类号： B01J21/10 , C07B61/00 , C07C45/74 , C07C49/603 , C07C45/45
CPC分类号： B01J21/10 , C07C45/74
摘要： The present invention relates to a process for obtaining isophorone from acetone, characterized in that the operation is carried out (i) in liquid phase in the presence of a magnesium aluminum double oxide of formula Mg.sub.1-x Al.sub.x O.sub.1+x or (ii) either in gaseous or liquid phase in the presence of a catalyst of general formula (I): �(Mg.sup.2+).sub.1-x (Al.sup.3+).sub.x (OH.sup.-).sub.2 !.sup.x+ �(OH.sup.-).sub.x !.sup.x- (H.sub.2 O).sub.n (I) with 0.20.ltoreq.x.ltoreq.0.33 and n
摘要翻译：本发明涉及一种从丙酮获得异佛尔酮的方法，其特征在于：（i）在式Mg1-xAlxO1 + x的镁铝双氧化物存在下，在液相中进行操作，或（ii）气态（I）：[（Mg2 +）1-x（Al3 +）x（OH-）2] x + [（OH-）x] x-（H2O）n（I））的催化剂存在下，其中0.20≤x≤0.33且n <1。

7. 发明授权

US4874859A Di-bishydroxypropyl cyanuric acid, trisubstituted derivatives thereof and a process for their preparation 失效
标题翻译：二羟基丙二酸二羟丙酯，三取代衍生物及其制备方法
公开(公告)号：US4874859A
公开(公告)日：1989-10-17
申请号：US131793
申请日：1987-12-11
申请人： Remy Teissier , Serge Clamens
发明人： Remy Teissier , Serge Clamens
IPC分类号： C07D251/34 , C08K5/34 , C08K5/3477
CPC分类号： C07D251/34 , C08K5/3477
摘要： The subject of the invention is new derivatives (I) and (II) of cyanuric acid which have the formula, respectively, ##STR1## in which: R' and R" are --CH.sub.2 --CH(OH)--CH.sub.2 OH andR is an alkyl containing a polymerizable ethylenic functional group such as an acrylic, methacrylic or allyl group.The derivatives (I) and (II) according to the invention may be employed as crosslinking agents in polymers.
摘要翻译：本发明的主题是具有下式的分别具有式（I）和（II）的氰尿酸的新衍生物（I）和（II），其中：R'和R“是-CH 2 -CH（OH）-CH 2 OH，R为含有可聚合的烯属官能团如丙烯酸，甲基丙烯酸或烯丙基的烷基。根据本发明的衍生物（I）和（II）可以用作聚合物中的交联剂。

8. 发明申请

US20060041165A1 Continuous ethyl lactate preparation method 审中-公开
标题翻译：连续乳酸乙酯制备方法
公开(公告)号：US20060041165A1
公开(公告)日：2006-02-23
申请号：US10537422
申请日：2003-12-05
申请人： Serge Tretjak , Elie Burtin , Remy Teissier
发明人： Serge Tretjak , Elie Burtin , Remy Teissier
IPC分类号： C07C69/68
CPC分类号： C07C67/08 , C07C67/54 , C07C69/68
摘要： The invention relates to a continuous method of preparing ethyl lactate by means of lactic acid esterification using ethanol in the presence of a catalyst. The inventive method consists in continuously extracting a mixture comprising ethyl lactate, ethanol, water and different heavy products from an esterification reaction medium at partial lactic acid conversion rate and, subsequently, subjecting said mixture to a reduced-pressure flash separation, thereby producing an overhead stream containing a mixture of ethyl lactate, ethanol and water, the lower part of said mixture supplying a fractional distillation column.
摘要翻译：本发明涉及通过在催化剂存在下使用乙醇进行乳酸酯化制备乳酸乙酯的连续方法。本发明的方法包括以部分乳酸转化率从酯化反应介质连续提取包含乳酸乙酯，乙醇，水和不同重质产物的混合物，随后将所述混合物进行减压闪蒸分离，由此产生塔顶含有乳酸乙酯，乙醇和水的混合物，所述混合物的下部供应分馏塔。

9. 发明授权

US5936131A Process for obtaining .beta.-hydroxy and/or .alpha.,.beta.-unsaturated carbonyl compounds 失效
标题翻译：获得β-羟基和/或α，β-不饱和羰基化合物的方法
公开(公告)号：US5936131A
公开(公告)日：1999-08-10
申请号：US808118
申请日：1997-02-28
申请人： Remy Teissier , Maurice Fournier
发明人： Remy Teissier , Maurice Fournier
IPC分类号： B01J23/02 , B01J21/10 , C07B61/00 , C07C45/72 , C07C45/74 , C07C47/19 , C07C47/21 , C07C49/17 , C07C49/203
CPC分类号： C07C45/72 , B01J21/10 , C07C45/74
摘要： The present invention relates to a process for obtaining .beta.-hydroxy carbonyl compounds and/or .alpha.,.beta.-unsaturated carbonyl compounds, characterized in that at least one aldehyde or one ketone is brought into contact with a solid catalyst of general formula (I):�(Mg.sup.2+).sub.1-x (Al.sup.3+).sub.x (OH.sup.-).sub.2 !.sup.x+ �(OH.sup.-).sub.x !.sup.x- (H.sub.2 O).sub.n (I)with 0.20.ltoreq.x.ltoreq.0.33 and n
摘要翻译：本发明涉及一种获得β-羟基羰基化合物和/或α，β-不饱和羰基化合物的方法，其特征在于使至少一种醛或一种酮与通式（I）的固体催化剂接触： [（Mg2 +）1-x（Al3 +）x（OH-）2] x + [（OH-）x] x-（H2O）n（I），其中0.20≤x≤0.33且n <1。

10. 发明授权

US5672764A Selective aldolization of acetone to diacetone alcohol by a solid basic catalyst 失效
标题翻译：通过固体碱性催化剂选择性地将丙酮醛化成双丙酮醇
公开(公告)号：US5672764A
公开(公告)日：1997-09-30
申请号：US584900
申请日：1996-01-05
申请人： Remy Teissier , Didier Tichit , Fran.cedilla.ois Figueras , Jacques Kervennal
发明人： Remy Teissier , Didier Tichit , Fran.cedilla.ois Figueras , Jacques Kervennal
IPC分类号： B01J21/10 , B01J23/00 , C07B61/00 , C07C45/72 , C07C49/17 , C07C45/45
CPC分类号： B01J21/10 , B01J23/007 , C07C45/72
摘要： The aldolization is characterized by the use of a solid basic catalyst which has the following general formula �(Mg.sup.2+).sub.1-x (Al.sup.3+).sub.x (OH.sup.-).sub.2 !.sup.+x �(OH.sup.-).sub.x (H.sub.2 O).sub.n !.sup.-x (II) wherein 0.20.ltoreq.x.ltoreq.0.33 and n has a value of less than 1. This catalyst has a defined crystal structure similar to that of hydrotalcite or, alternatively, of meixnerite. Also disclosed are processes for the preparation of the catalyst.
摘要翻译：醛固化的特征在于使用具有以下通式[（Mg2 +）1-x（Al3 +）x（OH-）2] + x [（OH-）x（H2O）n] -x的固体碱性催化剂（II），其中0.20≤x≤0.33且n的值小于1.该催化剂具有与水滑石相似的限定的晶体结构，或者替代地，镁石。还公开了制备催化剂的方法。

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