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1. 发明授权

US5008442A Surface-active compounds on the basis of arylated fatty substances and their use 失效
标题翻译：基于芳基化脂肪物质的表面活性化合物及其用途
公开(公告)号：US5008442A
公开(公告)日：1991-04-16
申请号：US854339
申请日：1986-04-21
申请人： Heinz Uhrig , Klaus Ehl , Reinhold Deubel
发明人： Heinz Uhrig , Klaus Ehl , Reinhold Deubel
IPC分类号： C07C69/66 , B01F17/00 , B01F17/42 , C07C41/00 , C07C41/02 , C07C43/178 , C07C43/20 , C07C43/205 , C07C51/00 , C07C59/125 , C07C67/00 , C07C219/04 , C07C227/00 , C07C229/12 , C07C301/00 , C07C305/10 , C07C309/03 , C07C309/62 , C08G65/26 , C09D7/45 , C11D1/72 , D06P1/60 , D06P1/613
CPC分类号： B01F17/0042 , B01F17/0028 , B01F17/0057 , C08G65/2615 , C09D7/02
摘要： A compound of the formulaA[(Y-O).sub.x - Y - Z].sub.min which A is the radical of an arylated fatty alcohol, Y are identical or different groups of the formulae--CH.sub.2 --CH.sub.2 -- or --CH.sub.2 --CH(CH.sub.3)--,Z are identical or different radicals of the formulae --OH, --O--CO--CH.dbd.CH--COOM and --O--CO--CH.sub.2 --CH(SO.sub.3 M)--COOM,in whichM is a cation,x is an integer from 1 to 150, andm is a number from 1 to 7.

2. 发明授权

US4785082A Process for preparing a highly concentrated aqueous press cakes of an azo disperse dye from dilute aqueous suspension thereof wherein surfactant is added before the dye is isolated 失效
标题翻译：从稀的水性悬浮液制备偶氮分散染料的高浓度水性压饼的方法，其中在染料分离之前加入表面活性剂
公开(公告)号：US4785082A
公开(公告)日：1988-11-15
申请号：US795093
申请日：1985-11-05
申请人： Joachim Weide , Erwin Dietz , Reinhold Deubel
发明人： Joachim Weide , Erwin Dietz , Reinhold Deubel
IPC分类号： C09B67/20 , B01D37/03 , B01F17/42 , C09B67/54 , C09B41/00 , C09B67/38 , C09B67/40
CPC分类号： C09B67/0096 , B01D37/03
摘要： According to the invention, addition of one or more surfactants having a cloud point in aqueous solution to an aqueous suspension of an azo disperse dye gives after the isolation of the dye at a temperature above the cloud point aqueous press cakes containing a large amount of this dye.The direct processing of press cakes as obtained for example after the synthesis and isolation of azo disperse dyes to practical dispersions for use requires a minimum dye content in the press cakes. The minimum content is frequently not obtained when conventional methods of isolation are used, so that it is necessary to proceed via the indirect route of drying to obtain powders and redispersing the powders. By using the process according to the invention it is possible to cut out the costly indirect route or, if desired, to reduce the expense of drying to obtain powders by an appreciable margin.
摘要翻译：根据本发明，将一种或多种在水溶液中具有浊点的表面活性剂加入到偶氮分散染料的水性悬浮液中，在染料分离后，在高于含有大量这种染料。将合成和分离偶氮分散染料后获得的压饼直接加工成实用的分散体需要在压饼中具有最小的染料含量。当使用常规的分离方法时，通常不能获得最小含量，因此有必要通过间接干燥途径进行获得粉末并再分散粉末。通过使用根据本发明的方法，可以切出昂贵的间接途径，或者如果需要，可以减少干燥所需的费用，以获得明显的余量。

3. 发明授权

US4474609A Recrystallization-resistant monoazo pigment mixtures of high tinctorial strength, process for their preparation and their use 失效
标题翻译：具有高着色强度的重结晶耐酸单偶氮颜料混合物，其制备方法及其用途
公开(公告)号：US4474609A
公开(公告)日：1984-10-02
申请号：US474517
申请日：1983-03-14
申请人： Klaus Ehl , Reinhold Deubel
发明人： Klaus Ehl , Reinhold Deubel
IPC分类号： C09B44/00 , C09B29/33 , C09B67/20 , C09B67/22 , C09B69/04 , C09D5/00 , C09D11/02 , D06P1/642
CPC分类号： C09B67/0051 , C09B29/33 , C09B69/045 , Y10S534/01
摘要： By coupling diazotized amines of the benzene series onto acetoacetic acid arylides, in which process more than one diazo and/or coupling component is applied and from 0.1 to 20 molar % of the diazo and/or coupling component contain acid groups, and by subsequently reacting the reactive acid groups of the product obtained by coupling with cation-active quaternary compounds, recrystallization-resistant monoazo pigment mixtures are obtained which are suitable for the preparation of varnishes, printing inks, and oily and aqueous compositions.
摘要翻译：通过将苯系的重氮化胺偶联到乙酰乙酸芳基化合物上，其中施加多于一种的重氮和/或偶联组分，并且0.1至20摩尔％的重氮和/或偶合组分含有酸基团，并且随后使通过与阳离子活性季铵化合物偶联获得的产物的反应性酸基，得到适用于制备清漆，印刷油墨和油性和含水组合物的重结晶耐受性单偶氮颜料混合物。

4. 再颁专利

USRE30650E Dispersing and stabilizing agents for dyestuffs 失效
标题翻译：染料分散稳定剂
公开(公告)号：USRE30650E
公开(公告)日：1981-06-16
申请号：US103492
申请日：1979-12-14
申请人： Reinhold Deubel , Helmut Diery , Wolfgang Klinner , Karl-Hermann List , Heinz Uhrig
发明人： Reinhold Deubel , Helmut Diery , Wolfgang Klinner , Karl-Hermann List , Heinz Uhrig
IPC分类号： C08G8/18 , C08G8/28 , C09B67/46 , D06P1/56
CPC分类号： C08G8/28 , C08G8/18 , C09B67/0086 , D06P1/56
摘要： Dispersions of pigments, disperse- or vat-dyestuffs, wherein the dispersing agent is formed either by cocondensation of a phenolic component, formaldehyde and an alkali metal sulfite or of a sulfonated phenolic component and formaldehyde. These dispersions are characterized in that the dispersing agent used shows an improved dispersing effect. Furthermore, they can also be used when being neutralized for the dispersing alkali sensitive dyestuffs and they show no tendency to soil the fabrics so that also clean shades may be dyed.

5. 发明授权

US5493011A Monoazo or disazo pigments based on (benoxazol-2-yl)- or (benzimidazol-2-yl)-arylacetamides 失效
标题翻译：基于（苯恶唑-2-基） - 或（苯并咪唑-2-基） - 芳基乙酰胺的单偶氮或双偶氮颜料
公开(公告)号：US5493011A
公开(公告)日：1996-02-20
申请号：US934479
申请日：1992-11-06
申请人： Rudiger Jung , Reinhold Deubel
发明人： Rudiger Jung , Reinhold Deubel
IPC分类号： C08K5/3447 , C08K5/353 , C09B29/32 , C09B29/36 , C09B29/42 , C09B29/46 , C09B35/03 , C09B35/035 , C09B35/037 , C09B41/00 , C09B63/00 , C09B67/22 , C09D7/00 , C09D11/037 , D06P5/00 , D21H21/28 , C08K5/23 , D06P1/44
CPC分类号： C09D11/037 , C08K5/3447 , C08K5/353 , C09B29/32 , C09B35/035 , C09B41/002 , C09B41/005 , C09B63/005 , C09B67/0046 , C09D7/007 , D06P5/001 , D21H21/285
摘要： Water-insoluble azo colorants, their preparation and use The invention relates to monoazo and disazo compounds of the formula (I) ##STR1## in which D is the radical of a carbocyclic or heterocyclic diazo or bisdiazo component, R.sup.1 and R.sup.2, independently of one another, are each a substituted or unsubstituted aryl or heteroaryl radical, X.sup.1 and X.sup.2, independently of one another, are each ring-forming ether oxygen or a substituted or unsubstituted imide grouping and n has the value 0 or 1, in which rings A and B, independently of one another, can each be additionally substituted and/or carry substituted or unsubstituted fused rings.These new compounds of the formula (I) are obtained by coupling diazotized amines or diamines of the type D--NH.sub.2 or H.sub.2 N--D--NH.sub.2 with (benzoxazol-2-yl)- or (benzimidazol-2-yl)-arylacetamides.Depending on the presence and length of alkyl chains, the compounds of the formula (I) are suitable for use as pigments, disperse dyes or oil-soluble dyes.
摘要翻译：水不溶性偶氮着色剂及其制备和用途本发明涉及式（I）的单偶氮和双偶氮化合物，其中D是碳环或杂环重氮或双重重氮组分的基团，R1和R2，彼此独立地为取代或未取代的芳基或杂芳基，X 1和X 2彼此独立地为成环醚氧或取代或未取代的酰亚胺基，n为0或1，其中环A和B彼此独立地可以各自另外被取代和/或携带取代或未取代的稠合环。式（I）的这些新化合物是通过将（重氮化的胺或D-NH 2或H 2 N-D-NH 2的二胺与（苯并恶唑-2-基） - 或（苯并咪唑-2-基） - 芳基乙酰胺偶合而获得的。根据烷基链的存在和长度，式（I）的化合物适合用作颜料，分散染料或油溶性染料。

6. 发明授权

US4597906A Surface-active compounds on the basis of arylated fatty substances and their use 失效
标题翻译：基于芳基化脂肪物质的表面活性化合物及其用途
公开(公告)号：US4597906A
公开(公告)日：1986-07-01
申请号：US565906
申请日：1983-12-27
申请人： Heinz Uhrig , Klaus Ehl , Reinhold Deubel
发明人： Heinz Uhrig , Klaus Ehl , Reinhold Deubel
IPC分类号： C07C69/66 , B01F17/00 , B01F17/42 , C07C41/00 , C07C41/02 , C07C43/178 , C07C43/20 , C07C43/205 , C07C51/00 , C07C59/125 , C07C67/00 , C07C219/04 , C07C227/00 , C07C229/12 , C07C301/00 , C07C305/10 , C07C309/03 , C07C309/62 , C08G65/26 , C09D7/45 , C11D1/72 , D06P1/60 , D06P1/613 , C08H3/00
CPC分类号： B01F17/0042 , B01F17/0028 , B01F17/0057 , C08G65/2615 , C09D7/02
摘要： Compounds of the formulaA[(Y--O).sub.x --Y--Z].sub.min which A is the radical of an oxaryl-modified (modified with an aryl group containing a hydroxyl group) fatty alcohol, i.e., the radical of an arylated fatty alcohol, or is the radical of an oxaryl-modified (again, modified with an aryl group containing a hydroxyl group) fatty acid or esterification product thereof, i.e., the radical of an arylated fatty acid or esterification product thereof, Y denotes identical or different groups of the formula--CH.sub.2 --CH.sub.2 -- or --CH.sub.2 --CH(CH.sub.3)--,Z denotes identical or different radicals of the formulae --OH, --O--CO--CH.dbd.CH--COOM and --O--CO--CH.sub.2 --CH(SO.sub.3 M)--COOM, in whichM is a cation,x is an integer of from 1 to 150 andm is a number of from 1 to 7,are suitable as interfacially active agents, in particular as dispersing agents, wetting agents, emulsifiers and dyeing auxiliaries.
摘要翻译：式（A）（YO）xYZ] m的化合物，其中A是被氧杂芳基改性（含有羟基的芳基改性）脂肪醇的基团，即芳基化脂肪醇的基团，或者是氧杂芳基改性（再次用含羟基的芳基改性）脂肪酸或其酯化产物，即芳基化脂肪酸或其酯化产物的基团，Y表示相同或不同的式 - CH 2 -CH 2 - 或-CH 2 -CH（CH 3） - ，Z表示式-OH，-O-CO-CH = CH-COOM和-O-CO-CH 2 -CH（SO 3 M）-COOM的相同或不同的基团，其中M为阳离子，x为1至150的整数，m为1至7的数，适用作界面活性剂，特别是作为分散剂，润湿剂，乳化剂和染色助剂。

7. 发明授权

US4469516A Pigment preparations; process for their manufacture and their use 失效
标题翻译：颜料制剂; 其制造及其使用过程
公开(公告)号：US4469516A
公开(公告)日：1984-09-04
申请号：US450468
申请日：1982-12-16
申请人： Manfred Schneider , Reinhold Deubel , Rainer Schunck
发明人： Manfred Schneider , Reinhold Deubel , Rainer Schunck
IPC分类号： C09B11/00 , B41M5/10 , C09B11/10 , C09B67/20 , C09B67/32 , C09D11/02
CPC分类号： C09B67/0075 , B41M5/10 , C09B11/10 , C09B67/0061 , Y10T428/31964
摘要： Aryl-pararosaniline sulfonic acid pigments can be transformed into a pigment preparation having high tinctorial strength and being easily dispersible by dissolving them in aqueous alkali, adding a water-soluble synthetic resin (being a reaction product or mixture of (I) maleic anhydride addition product of an unsaturated fatty acid or fatty acid polyol ester, said addition product being partially esterified with a polyol, and (II) a low-molecular curable and partially etherified aminoplast and optionally an anionic or nonionic surfactant and precipitating the preparation with a mineral acid. These preparations are especially useful for pigmenting printing inks, carbon paper, duplicating papers and typewriter ribbons.
摘要翻译：芳基 - 对 - 间苯磺酸颜料可以转化成具有高着色强度的颜料制剂，并且通过将它们溶于碱水溶液中容易地分散，加入水溶性合成树脂（作为（I）马来酸酐加成产物的反应产物或混合物的不饱和脂肪酸或脂肪酸多元醇酯，所述加成产物用多元醇部分酯化，和（II）低分子固化和部分醚化的氨基塑料和任选的阴离子或非离子表面活性剂，并用无机酸沉淀该制剂。这些制剂对于着色印刷油墨，碳纸，复印纸和打字机色带特别有用。

8. 发明授权

US3960591A Process for the preparation of pigment compositions for the dope dyeing of polyacrylonitrile 失效
标题翻译：制备用于聚丙烯腈染色的颜料组合物的方法
公开(公告)号：US3960591A
公开(公告)日：1976-06-01
申请号：US441936
申请日：1974-02-13
申请人： Reinhold Deubel , Volker Hemmerling , Werner Reitz , Wolfgang Teige
发明人： Reinhold Deubel , Volker Hemmerling , Werner Reitz , Wolfgang Teige
IPC分类号： C08J3/22 , C09B41/00 , C09B67/20 , C09C3/10
CPC分类号： C08J3/226 , C09B41/001 , C09B41/003 , C09B67/006 , C08J2333/20 , C08J2433/00
摘要： A pigment composition for the dyeing of polyacrylonitrile polymers and copolymers prepared by adding a polyacrylonitrile polymer or copolymer as a support in the preparation of formation of the pigment and working up the pigment in usual manner.As support material there are suitable as well pure polyacrylonitrile as copolymers containing, in addition to acrylonitrile, one or more other copolymerizable monoolefinic monomers.The amount of support material to be added ranges from 20 to 80, preferably from 30 to 60% by weight, calculated on the finished composition. As pigments there may be used those which are prepared or formed in purely aqueous systems or in aqueous systems containing organic solvents, for example azo pigments or pigments of perylene tetracarboxylic acid or naphthalene tetracarboxylic acid, dioxazines, phthalocyanines, quinacridones, indigoids, anthraquinone dyestuffs, iron oxide and titanium dioxide.The pulverulent compositions thus obtained are especially suitable for the dyeing of spinning solutions of polyacrylonitrile fibers and the modifications thereof. They may be dispersed by simply stirring them into an appropriate spinning solvent.
摘要翻译：用于染色聚丙烯腈聚合物和共聚物的颜料组合物通过将聚丙烯腈聚合物或共聚物作为载体加入到制备颜料的制备中并以常规方式处理颜料而制备。

9. 发明授权

US4828622A Process for preparing highly concentrated aqueous press cakes of solids 失效
标题翻译：制备高浓缩水性固体的压饼的方法
公开(公告)号：US4828622A
公开(公告)日：1989-05-09
申请号：US191808
申请日：1988-05-05
申请人： Joachim Weide , Erwin Dietz , Reinhold Deubel
发明人： Joachim Weide , Erwin Dietz , Reinhold Deubel
IPC分类号： C09B67/38 , B01D37/03 , B01J13/00 , C09B67/02 , C09B67/42 , C09B67/54
CPC分类号： B01D37/03 , C09B67/0096
摘要： According to the invention, addition of one or more surfactants having a cloud point in aqueous solution to an aqueous suspension of a solid gives after the isolation of the solid at a temperature above the cloud point aqueous press cakes containing a large amount of this solid. The direct processing of press cakes as obtained for example after the synthesis and isolation of dyes or pigments to give practical aqueous pastes or dispersions requires a minimum solids content in the press cakes. The minimum content is frequently not obtained when conventional methods of isolation are used, so that it is necessary to proceed via the indirect route of drying to obtain the powders and redispersing the powders. By using the process according to the invention it is possible to cut out the costly indirect route or, if desired, to reduce the expense of drying to obtain powders by an appreciable margin.
摘要翻译：根据本发明，将一种或多种在水溶液中具有浊点的表面活性剂加入到固体的水悬浮液中，在高于含有大量该固体的浊点水性压饼的温度下分离固体后，得到固体。在合成和分离染料或颜料之后获得的压榨蛋糕的直接加工以产生实用的水性糊剂或分散体，需要在压榨蛋糕中具有最小的固体含量。当使用常规的隔离方法时，通常不能获得最小含量，因此需要通过间接的干燥途径进行获得粉末并再分散粉末。通过使用根据本发明的方法，可以切出昂贵的间接途径，或者如果需要，可以减少干燥所需的费用，以获得明显的余量。

10. 发明授权

US4719292A .beta.-modified crystalline red pigment 失效
标题翻译： β-改性结晶红色素
公开(公告)号：US4719292A
公开(公告)日：1988-01-12
申请号：US507720
申请日：1983-06-23
申请人： Franz Schui , Reinhold Deubel , Norbert Wester
发明人： Franz Schui , Reinhold Deubel , Norbert Wester
IPC分类号： C09B29/15 , C09B63/00 , C09B67/00 , C09B67/20 , C09B67/26 , C09B67/48 , C09D7/12 , C09D11/02 , C09B67/24 , C09B11/02 , D06P1/44
CPC分类号： C09B67/0029 , C09B63/00
摘要： A novel crystallographic modification (.beta.-modification) of the pigment C. I. Pigment Red 53:1 is described and claimed which has characteristic reflection values in its X-ray diffraction pattern obtained by means of Cu-K.sub..alpha. radiation. This novel pigment form is obtained by reacting an aqueous solution of an alkali metal or ammonium salt of the formula 1 ##STR1## with the equivalent amount of a water-soluble barium salt in the presence of a compound of the formula 2 ##STR2## The modification is distinguished by a more yellowish-red shade as compared to the known .alpha.-modification.
摘要翻译：描述和要求保护颜料C.I.颜料红53:1的新型晶体学修饰（β-改性），其在其通过Cu-Kαα辐射获得的X射线衍射图中具有特征反射值。该新型颜料形式是通过使式1的碱金属盐或铵盐的水溶液与等量的水溶性钡盐在式2化合物（2）与已知的α-修饰相比，修饰的区别在于更淡黄色的阴影。

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