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1. 发明申请

US20130045989A1 STABILIZED CRYSTAL OF 2-ETHYL-3,7-DIMETHYL-6-(4-(TRIFLUOROMETHOXY)PHENOXY)QUINOLINE-4-YL METHYL CARBONATE, PROCESS FOR PRODUCING THE CRYSTAL, AND AGRICULTURAL CHEMICAL COMPOSITION COMPRISING THE CRYSTAL 有权
标题翻译： 2-乙基-3,7-二甲基-6-（4-（三氟甲氧基）苯氧基）喹啉-4-基甲基碳酸酯的稳定晶体，生产水晶的方法和包含晶体的农业化学组合物
公开(公告)号：US20130045989A1
公开(公告)日：2013-02-21
申请号：US13580550
申请日：2011-02-22
申请人： Kouki Tanigakiuchi , Mikio Sekiguchi , Hiroki Hotta , Shizuo Shimano , Akinori Morikawa , Kazumi Yamamoto , Nozomu Nakanishi , Nobuto Minowa , Takashi Watanabe
发明人： Kouki Tanigakiuchi , Mikio Sekiguchi , Hiroki Hotta , Shizuo Shimano , Akinori Morikawa , Kazumi Yamamoto , Nozomu Nakanishi , Nobuto Minowa , Takashi Watanabe
IPC分类号： C07D215/22 , A01P7/04 , A01N43/40
CPC分类号： C07D215/233 , A01N43/42 , A01N47/06 , C07D215/20 , A01N25/12
摘要： An objective of the present invention is to provide a crystal of 2-ethyl-3,7-dimethyl-6-(4-(trifluoromethoxy)phenoxy)quinoline-4-yl methyl carbonate having stable physicochemical properties.The objective is attained by a crystal of 2-ethyl-3,7-dimethyl-6-(4-(trifluoromethoxy)phenoxy)quinoline-4-yl methyl carbonate that exhibits a diffraction peak pattern shown in FIG. 1 as determined by powder X-ray diffractometry.
摘要翻译：本发明的目的是提供具有稳定物理化学性质的2-乙基-3,7-二甲基-6-（4-（三氟甲氧基）苯氧基）喹啉-4-基甲基碳酸酯的结晶。目的是通过图2所示的衍射峰图案的2-乙基-3,7-二甲基-6-（4-（三氟甲氧基）苯氧基）喹啉-4-基甲基碳酸酯的晶体得到。 1，通过粉末X射线衍射测定。

2. 发明授权

US08367833B2 Process for producing 6-aryloxyquinoline derivative and intermediate therefor 有权
标题翻译： 6-芳氧基喹啉衍生物及其中间体的制备方法
公开(公告)号：US08367833B2
公开(公告)日：2013-02-05
申请号：US13054240
申请日：2009-07-13
申请人： Yasuhito Kato , Shizuo Shimano , Akinori Morikawa , Hiroki Hotta , Kazumi Yamamoto , Nozomu Nakanishi , Nobuto Minowa , Hiroshi Kurihara
发明人： Yasuhito Kato , Shizuo Shimano , Akinori Morikawa , Hiroki Hotta , Kazumi Yamamoto , Nozomu Nakanishi , Nobuto Minowa , Hiroshi Kurihara
IPC分类号： C07D215/38
CPC分类号： C07D215/22 , C07C227/04 , C07C229/64 , C07D215/20
摘要： Disclosed is a process for producing 6-aryloxyquinoline derivatives useful as insecticides or fungicides for agricultural and horticultural use. The process comprises a cyclization reaction step of reacting an anthranilic acid derivative represented by general formula (1) with a kenone in the presence of an acid to obtain a quinolone derivative and a condensation reaction step of reacting the quinolone derivative with a halogen compound or an acid anhydride to obtain a quinoline derivative.
摘要翻译：公开了用作农业和园艺用途的杀虫剂或杀真菌剂的6-芳氧基喹啉衍生物的方法。该方法包括在酸存在下使通式（1）表示的邻氨基苯甲酸衍生物与酮酮反应以获得喹诺酮衍生物的环化反应步骤和使喹诺酮衍生物与卤素化合物或酸酐，得到喹啉衍生物。

3. 发明申请

US20120046470A1 PROCESS FOR PRODUCING PYRIPYROPENE DERIVATIVES 有权
标题翻译：生产吡啶衍生物的方法
公开(公告)号：US20120046470A1
公开(公告)日：2012-02-23
申请号：US13266671
申请日：2010-05-12
申请人： Yoshimasa Fukuda , Takashi Ando , Kimihiko Goto , Nozomu Nakanishi , Takashi Watanabe , Kenichi Kurihara , Nobuto Minowa , Masaaki Mitomi
发明人： Yoshimasa Fukuda , Takashi Ando , Kimihiko Goto , Nozomu Nakanishi , Takashi Watanabe , Kenichi Kurihara , Nobuto Minowa , Masaaki Mitomi
IPC分类号： C07D493/04
CPC分类号： C07D493/04
摘要： Disclosed is a process for efficiently producing pyripyropene derivatives having acyloxy at the 1-position and 11-position and hydroxyl at the 7-position. The process comprises selectively acylating hydroxyl at the 1-position and 11-position of a compound represented by formula B1 through one to three steps with an acylating agent in the presence or absence of a base.
摘要翻译：公开了一种有效生产在1-位和11位上具有酰氧基并在7-位具有羟基的吡啶并苯衍生物的方法。该方法包括在存在或不存在碱的情况下用酰化剂选择性地将式B1化合物的1位和11位羟基选择性酰化1-3步。

4. 发明授权

US08076503B2 Process for production of optically active aminophosphinylbutanoic acids 有权
标题翻译：光学活性氨基氧膦基丁酸生产方法
公开(公告)号：US08076503B2
公开(公告)日：2011-12-13
申请号：US12298067
申请日：2007-09-03
申请人： Nobuto Minowa , Nozomu Nakanishi , Masaaki Mitomi , Hideki Nara , Tohru Yokozawa
发明人： Nobuto Minowa , Nozomu Nakanishi , Masaaki Mitomi , Hideki Nara , Tohru Yokozawa
IPC分类号： C07C229/04 , C07F9/28
CPC分类号： C07B53/00 , C07F9/301 , C07F9/3211
摘要： The present invention is a process for producing optically active aminophosphinylbutanoic acids represented by the formula (2), comprising asymmetrically hydrogenating a compound represented by the formula (1) in the presence of a ruthenium-optically active phosphine complex, a process for the production thereof, and a compound useful in a herbicide such as L-AHPB that can be produced with good efficiency and high asymmetric yield.
摘要翻译：本发明是一种制备由式（2）表示的光学活性氨基氧膦基丁酸的方法，包括在钌 - 光学活性膦配合物的存在下不对称地氢化由式（1）表示的化合物，其制备方法，以及可以以高效率和高不对称产率生产的用于除草剂如L-AHPB的化合物。

5. 发明授权

US07772426B2 Method for producing L-2-amino-4-(hydroxymethylphosphinyl)-butanoic acid 有权
标题翻译：制备L-2-氨基-4-（羟甲基氧膦基） - 丁酸的方法
公开(公告)号：US07772426B2
公开(公告)日：2010-08-10
申请号：US11909839
申请日：2006-03-28
申请人： Nobuto Minowa , Nozomu Nakanishi , Masaaki Mitomi
发明人： Nobuto Minowa , Nozomu Nakanishi , Masaaki Mitomi
IPC分类号： C07C227/32
CPC分类号： C07B53/00 , C07F9/301 , C07F9/65683
摘要： Disclosed is a method for efficiently and highly selectively producing L-2-amino-4-(hydroxymethylphosphinyl)-butanoic acid, which is useful as a herbicide, through a catalytic asymmetric synthesis reaction. Specifically disclosed is a method for producing L-2-amino-4-(hydroxymethylphosphinyl)-butanoic acid which is characterized in that a dehydroamino acid is subjected to an asymmetric hydrogenation by using a rhodium catalyst represented by the formula (2) below and having an optically active cyclic phosphine ligand, and then the resulting product is subjected to hydrolysis: [Rh(R4)(L)]X (2) [where R4 represents 1,5-cyclooctadien or norbornadien; L represents a substance represented by the following formula (6): (wherein R5 and R8 respectively represent a C1-4 alkyl group; R6 and R7 respectively represent hydrogen atom or hydroxyl group; and Y represents a group selected from groups represented by the following formula (7): (where Me represents methyl group)).].
摘要翻译：公开了通过催化不对称合成反应有效和高选择性地生产可用作除草剂的L-2-氨基-4-（羟甲基氧膦基） - 丁酸的方法。具体公开了一种生产L-2-氨基-4-（羟甲基氧膦基） - 丁酸的方法，其特征在于，使用下式（2）表示的铑催化剂对脱氢氨基酸进行不对称氢化，光学活性环膦配体，然后使所得产物水解：[Rh（R 4）（L）] X（2）[其中R 4表示1,5-环辛二烯或降冰片素; L表示由下式（6）表示的物质：（其中，R 5和R 8分别表示C 1-4烷基; R 6和R 7分别表示氢原子或羟基，Y表示选自下述式（7）：（Me表示甲基））。

6. 发明申请

US20090270647A1 METHOD FOR PRODUCING ALPHA - AMINO ACID INCLUDING PHOSPHORUS AND PRODUCTION INTERMEDIATES THEREOF 有权
标题翻译：生产含氨基酸的氨基酸及其生产中间体的方法
公开(公告)号：US20090270647A1
公开(公告)日：2009-10-29
申请号：US12442011
申请日：2007-09-19
申请人： Nobuto Minowa , Nozomu Nakanishi , Masaaki Mitomi
发明人： Nobuto Minowa , Nozomu Nakanishi , Masaaki Mitomi
IPC分类号： C07F9/32
CPC分类号： C07B53/00 , B01J31/0207 , B01J31/0209 , B01J31/0235 , B01J31/0237 , B01J31/0261 , B01J31/0271 , B01J2231/341 , C07F9/3211 , Y02P20/55
摘要： A method for efficiently producing L-2-amino-4-(hydroxymethylphosphinyl)-butanoic acid, useful as a herbicide, by a catalytic asymmetric synthesis reaction with a high asymmetric yield. The method includes a step in which a compound represented by the below formula (1) and a benzylamine are reacted in the presence of dehydrating agent, then the resulting mass is reacted with hydrogen cyanide in the presence of an asymmetric catalyst, followed by acid hydrolysis, further followed by elimination of a protective group. [chemical formula 1] (1) (where, R1 represents a C1-4 alkyl group.)
摘要翻译：通过具有高不对称产率的催化不对称合成反应有效生产可用作除草剂的L-2-氨基-4-（羟甲基氧膦基） - 丁酸的方法。该方法包括在脱水剂的存在下使由下式（1）表示的化合物和苄胺反应的步骤，然后将所得物质与氰化氢在不对称催化剂的存在下反应，随后进行酸水解，然后除去保护基。 [化学式1]（1）（其中，R 1表示C 1-4烷基）

7. 发明授权

US09126934B2 Process for producing 4-carbonyloxyquinoline derivatives 有权
标题翻译： 4-羰基氧基喹啉衍生物的制备方法
公开(公告)号：US09126934B2
公开(公告)日：2015-09-08
申请号：US13885783
申请日：2011-11-16
申请人： Shizuo Shimano , Akinori Morikawa , Kenichi Yamamoto , Hiroki Hotta , Kazumi Yamamoto , Nozomu Nakanishi , Nobuto Minowa
发明人： Shizuo Shimano , Akinori Morikawa , Kenichi Yamamoto , Hiroki Hotta , Kazumi Yamamoto , Nozomu Nakanishi , Nobuto Minowa
IPC分类号： C07D215/38 , C07D215/20 , C07D215/14
CPC分类号： C07D215/20 , C07D215/14 , C07D215/22
摘要： An objective of the present invention is to provide a process for producing 4-carbonyl oxyquinoline derivatives useful as agricultural and horticultural pesticides and fungicides. The objective can be attained by a process for producing 4-carbonyl oxyquinoline derivatives represented by general formula (1), the process including reacting a quinolone derivative with a halogenated compound or an acid anhydride in the presence of a phase transfer catalyst and a base.
摘要翻译：本发明的目的是提供一种用作农业和园艺农药和杀真菌剂的4-羰基氧喹啉衍生物的方法。该目的可以通过制备由通式（1）表示的4-羰基氧喹啉衍生物的方法来实现，该方法包括在相转移催化剂和碱的存在下使喹诺酮衍生物与卤代化合物或酸酐反应。

8. 发明授权

US08853414B2 Process for producing pyripyropene derivatives 有权
标题翻译：生产拟南芥衍生物的方法
公开(公告)号：US08853414B2
公开(公告)日：2014-10-07
申请号：US13581857
申请日：2010-11-10
申请人： Yoshimasa Fukuda , Takashi Ando , Kimihiko Goto , Nozomu Nakanishi , Takashi Watanabe , Kenichi Kurihara , Nobuto Minowa , Masaaki Mitomi
发明人： Yoshimasa Fukuda , Takashi Ando , Kimihiko Goto , Nozomu Nakanishi , Takashi Watanabe , Kenichi Kurihara , Nobuto Minowa , Masaaki Mitomi
IPC分类号： C07D401/04 , C07D493/04
CPC分类号： C07D493/04
摘要： Disclosed is a process for efficiently producing pyripyropene derivatives having acyloxy at the 1-position and 11-position and hydroxyl at the 7-position. The process comprises selectively acylating hydroxyl at the 1-position and 11-position of a compound represented by formula B1 through one to three steps with an acylating agent in the presence or absence of a base.
摘要翻译：公开了一种有效生产在1-位和11位上具有酰氧基并在7-位具有羟基的吡啶并苯衍生物的方法。该方法包括在存在或不存在碱的情况下用酰化剂选择性地将式B1化合物的1位和11位羟基选择性酰化1至3个步骤。

9. 发明授权

US08329935B2 Process for producing phosphorus-containing dehydroamino acid 有权
标题翻译：生产含磷脱氢氨基酸的方法
公开(公告)号：US08329935B2
公开(公告)日：2012-12-11
申请号：US12529953
申请日：2008-03-19
申请人： Kenichi Kurihara , Nobuto Minowa , Nozomu Nakanishi , Masaaki Mitomi
发明人： Kenichi Kurihara , Nobuto Minowa , Nozomu Nakanishi , Masaaki Mitomi
IPC分类号： C07F9/28
CPC分类号： C07F9/4006 , C07F9/3217
摘要： A process for efficiently producing through a small number of steps an N-substituted 2-amino-4-(substituted-oxymethylphosphinyl)-2-butenoic ester which is an intermediate for herbicide L-AMPB. The process comprises reacting a compound represented by the following formula (1): (where R1 represents C1-4 alkyl group) with a compound represented by the following formula (2): (wherein R2, R2′, and R3 each represents C1-4 alkyl and R4 represents benzyloxycarbonyl) in the presence of a base.
摘要翻译：通过少量步骤有效地制备作为除草剂L-AMPB的中间体的N-取代的2-氨基-4-（取代的 - 氧甲基氧膦基）-2-丁烯酸酯的方法。该方法包括使由下式（1）表示的化合物（其中R 1表示C 1-4烷基）与下式（2）表示的化合物反应：（其中R2，R2'和R3各自表示C1- 4烷基，R 4表示苄氧基羰基）。

10. 发明授权

US07795464B2 Method for producing α-amino acid including phosphorus and production intermediates thereof 有权
标题翻译：包括磷的α-氨基酸的生产方法和生产中间体
公开(公告)号：US07795464B2
公开(公告)日：2010-09-14
申请号：US12442011
申请日：2007-09-19
申请人： Nobuto Minowa , Nozomu Nakanishi , Masaaki Mitomi
发明人： Nobuto Minowa , Nozomu Nakanishi , Masaaki Mitomi
IPC分类号： C07F9/32
CPC分类号： C07B53/00 , B01J31/0207 , B01J31/0209 , B01J31/0235 , B01J31/0237 , B01J31/0261 , B01J31/0271 , B01J2231/341 , C07F9/3211 , Y02P20/55
摘要： A method for efficiently producing L-2-amino-4-(hydroxymethylphosphinyl)-butanoic acid, useful as a herbicide, by a catalytic asymmetric synthesis reaction with a high asymmetric yield. The method includes a step in which a compound represented by the below formula (1) and a benzylamine are reacted in the presence of dehydrating agent, then the resulting mass is reacted with hydrogen cyanide in the presence of an asymmetric catalyst, followed by acid hydrolysis, further followed by elimination of a protective group. [chemical formula 1] (1) (where, R1 represents a C1-4 alkyl group).
摘要翻译：通过具有高不对称产率的催化不对称合成反应有效生产可用作除草剂的L-2-氨基-4-（羟甲基氧膦基） - 丁酸的方法。该方法包括在脱水剂的存在下使由下式（1）表示的化合物和苄胺反应的步骤，然后将所得物质与氰化氢在不对称催化剂的存在下反应，随后进行酸水解，然后除去保护基。 [化学式1]（1）（其中，R1表示C1-4烷基）。

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