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1. 发明授权

US09079830B2 Method for producing biaryl compound 有权
标题翻译：生产联芳基化合物的方法
公开(公告)号：US09079830B2
公开(公告)日：2015-07-14
申请号：US13386935
申请日：2010-07-26
申请人： Noriyuki Hida , Hiroaki Hibino
发明人： Noriyuki Hida , Hiroaki Hibino
IPC分类号： C07C309/00 , C07C303/32 , C07B37/04 , C07C201/12
CPC分类号： C07C303/32 , C07B37/04 , C07C201/12 , C07C309/39 , C07C205/06
摘要： A method for producing a biaryl compound represented by the formula (2) Ar—Ar (2) wherein Ar represents an aromatic group which can have a substituent, comprising conducting a coupling reaction of a compound represented by the formula (1) Ar—Cl (1) wherein Ar represents the same meaning as defined above, in the presence of copper metal and a copper salt.
摘要翻译：制备由式（2）表示的联芳基化合物的方法Ar-Ar（2）其中Ar表示可以具有取代基的芳香族基团，包括进行由式（1）表示的化合物的Ar-Cl （1）其中Ar表示与上述相同的含义，在铜金属和铜盐存在下。

2. 发明授权

US08236920B2 Polyarylene and process for producing the same 失效
标题翻译：聚亚芳基及其制备方法
公开(公告)号：US08236920B2
公开(公告)日：2012-08-07
申请号：US12224672
申请日：2006-09-06
申请人： Noriyuki Hida , Seiji Oda , Takashi Kamikawa , Katsuhiro Suenobu
发明人： Noriyuki Hida , Seiji Oda , Takashi Kamikawa , Katsuhiro Suenobu
IPC分类号： C08G75/20 , C08G75/23 , C08G8/02 , C07C317/16
CPC分类号： C08G61/02 , C07C309/73 , C07C311/16 , C08G61/10 , C08G65/4012 , C08G75/23 , C08G2261/122 , C08G2261/1452 , C08G2261/312 , C08G2261/516
摘要： A dihalobiphenyl compound represented by the formula (1): wherein A represents an amino group substituted with one or two C1-C20 hydrocarbon groups or a C1-C20 alkoxy group, R1 represents a fluorine atom, a C1-C20 alkyl group, etc., X1 represents a chlorine atom, a bromine atom or an iodine atom, an k represents an integer of 0 to 3, and a polyarylene comprising a repeating unit represented by the formula (2): wherein A, R1 and k represent the same meanings as defined above.
摘要翻译：由式（1）表示的二卤代联苯化合物：其中A表示被一个或两个C 1 -C 20烃基或C 1 -C 20烷氧基取代的氨基，R 1表示氟原子，C 1 -C 20烷基等。 X1表示氯原子，溴原子或碘原子，k表示0〜3的整数，以及含有由式（2）表示的重复单元的聚亚芳基：其中，A，R1和k表示相同的含义如上所述。

3. 发明授权

US07652159B2 Process for producing metallocene compound 失效
标题翻译：金属茂化合物的制备方法
公开(公告)号：US07652159B2
公开(公告)日：2010-01-26
申请号：US11660933
申请日：2005-07-11
申请人： Taichi Senda , Noriyuki Hida , Hidenori Hanaoka
发明人： Taichi Senda , Noriyuki Hida , Hidenori Hanaoka
IPC分类号： C07F7/00
CPC分类号： C07F17/00 , C08F10/00 , C08F2420/02 , C08F4/6592
摘要： The invention provides a process for producing a metallocene compound of formula (3) wherein R1 to R9 independently denote a hydrogen atom, a halogen atom, an alkyl, or the like; R10 denotes a halogen atom, an alkyl, an alkoxy, or the like; X5 and X6 independently denote a hydrogen atom, a halogen atom, or the like; and M denotes a transition metal atom of Group 4 of the Periodic Table, which process is characterized by reacting a silicon-substituted cyclopentadiene compound of formula (1) wherein R1 to R10 independently denote the same as described above; R11 denotes a hydrocarbon group or a tri-substituted silyl; and R12 to R14 independently denote a halogen atom or a hydrocarbon group, with a transition metal compound of the following formula (2) wherein M denotes the same as described above; X1, X2, X3, and X4 independently denotes a hydrogen atom, a halogen atom, an alkyl, or the like, in a solvent containing an aromatic hydrocarbon.
摘要翻译：本发明提供一种制备式（3）的茂金属化合物的方法，其中R 1至R 9独立地表示氢原子，卤素原子，烷基等; R 10表示卤素原子，烷基，烷氧基等; X 5和X 6独立地表示氢原子，卤素原子等; 并且M表示周期表第4族的过渡金属原子，该方法的特征在于使式（1）的硅取代的环戊二烯化合物（其中R 1至R 10独立地表示与上述相同的基团） R 11表示烃基或三取代甲硅烷基; 和R 12至R 14独立地表示卤素原子或烃基，与下式（2）的过渡金属化合物，其中M表示与上述相同的基团; X 1，X 2，X 3和X 4独立地表示在含有芳香族烃的溶剂中的氢原子，卤素原子，烷基等。

4. 发明申请

US20090036632A1 Polyarylene and Process for Producing the Same 失效
标题翻译：聚亚芳基及其制备方法
公开(公告)号：US20090036632A1
公开(公告)日：2009-02-05
申请号：US12224672
申请日：2006-09-06
申请人： Noriyuki Hida , Seiji Oda , Takashi Kamikawa , Katsuhiro Suenobu
发明人： Noriyuki Hida , Seiji Oda , Takashi Kamikawa , Katsuhiro Suenobu
IPC分类号： C08G75/23 , C07C317/16 , C08G75/30 , C08G8/02
CPC分类号： C08G61/02 , C07C309/73 , C07C311/16 , C08G61/10 , C08G65/4012 , C08G75/23 , C08G2261/122 , C08G2261/1452 , C08G2261/312 , C08G2261/516
摘要： A dihalobiphenyl compound represented by the formula (1): wherein A represents an amino group substituted with one or two C1-C20 hydrocarbon groups or a C1-C20 alkoxy group, R1 represents a fluorine atom, a C1-C20 alkyl group, etc., X1 represents a chlorine atom, a bromine atom or an iodine atom, an k represents an integer of 0 to 3, and a polyarylene comprising a repeating unit represented by the formula (2): wherein A, R1 and k represent the same meanings as defined above.
摘要翻译：由式（1）表示的二卤代联苯化合物：其中A表示被一个或两个C 1 -C 20烃基或C 1 -C 20烷氧基取代的氨基，R 1表示氟原子，C 1 -C 20烷基等。 X1表示氯原子，溴原子或碘原子，k表示0〜3的整数，以及含有由式（2）表示的重复单元的聚亚芳基：其中，A，R1和k表示相同的含义如上所述。

5. 发明申请

US20120164558A1 BIPHENYLTETRASULFONIC ACID COMPOUND, METHOD FOR PRODUCING SAME, POLYMER AND POLYMER ELECTROLYTE 审中-公开
标题翻译：联苯二酸酯化合物，其制备方法，聚合物和聚合物电解质
公开(公告)号：US20120164558A1
公开(公告)日：2012-06-28
申请号：US13394232
申请日：2010-09-09
申请人： Noriyuki Hida , Hiroaki Hibino , Toru Onodera
发明人： Noriyuki Hida , Hiroaki Hibino , Toru Onodera
IPC分类号： H01M8/10 , B01J31/10 , C08G75/24 , C07C309/39 , C07C303/22
CPC分类号： C07C309/73 , C08G61/10 , C08G2261/1452 , C08G2261/312 , C08G2261/516 , C08L65/00 , H01M8/1025 , H01M8/1027 , H01M2300/0082
摘要： Provided are a biphenyltetrasulfonic acid compound represented by the formula (1): wherein R1 represents a hydrogen atom, a cation, a hydrocarbon group, or the like; R2 represents a hydrogen atom, an alkyl group, an aryl group, an aryloxy group, an aralkyl group, an aralkyoxy group, or the like; and X1 represents a chlorine atom, a bromine atom, an iodine atom, a hydroxyl group, an amino group, or the like, and a polymer containing a structural unit originating from the biphenyltetrasulfonic acid compound.
摘要翻译：提供由式（1）表示的联苯基四磺酸化合物：其中R 1表示氢原子，阳离子，烃基等; R2表示氢原子，烷基，芳基，芳氧基，芳烷基，芳烷氧基等; X 1表示氯原子，溴原子，碘原子，羟基，氨基等，以及含有源自联苯基四磺酸化合物的结构单元的聚合物。

6. 发明申请

US20120123154A1 METHOD FOR PRODUCING BIARYL COMPOUND 有权
标题翻译：生产二元化合物的方法
公开(公告)号：US20120123154A1
公开(公告)日：2012-05-17
申请号：US13386935
申请日：2010-07-26
申请人： Noriyuki Hida , Hiroaki Hibino
发明人： Noriyuki Hida , Hiroaki Hibino
IPC分类号： C07C309/73 , C07C205/06
CPC分类号： C07C303/32 , C07B37/04 , C07C201/12 , C07C309/39 , C07C205/06
摘要： A method for producing a biaryl compound represented by the formula (2) Ar—Ar (2) wherein Ar represents an aromatic group which can have a substituent, comprising conducting a coupling reaction of a compound represented by the formula (1) Ar—Cl (1) wherein Ar represents the same meaning as defined above, in the presence of copper metal and a copper salt.
摘要翻译：制备由式（2）表示的联芳基化合物的方法Ar-Ar（2）其中Ar表示可以具有取代基的芳香族基团，包括进行由式（1）表示的化合物的Ar-Cl （1）其中Ar表示与上述相同的含义，在铜金属和铜盐存在下。

7. 发明申请

US20080319213A1 Process For Producing Metallocene Compound 失效
标题翻译：茂金属化合物生产工艺
公开(公告)号：US20080319213A1
公开(公告)日：2008-12-25
申请号：US11660933
申请日：2005-07-11
申请人： Taichi Senda , Noriyuki Hida , Hidenori Hanaoka
发明人： Taichi Senda , Noriyuki Hida , Hidenori Hanaoka
IPC分类号： C07F7/00 , C07F7/28
CPC分类号： C07F17/00 , C08F10/00 , C08F2420/02 , C08F4/6592
摘要： The invention provides a process for producing a metallocene compound of formula (3) wherein R1 to R9 independently denote a hydrogen atom, a halogen atom, an alkyl, or the like; R10 denotes a halogen atom, an alkyl, an alkoxy, or the like; X5 and X6 independently denote a hydrogen atom, a halogen atom, or the like; and M denotes a transition metal atom of Group 4 of the Periodic Table, which process is characterized by reacting a silicon-substituted cyclopentadiene compound of formula (1) wherein R1 to R10 independently denote the same as described above; R11 denotes a hydrocarbon group or a tri-substituted silyl; and R12 to R14 independently denote a halogen atom or a hydrocarbon group, with a transition metal compound of the following formula (2) wherein M denotes the same as described above; X1, X2, X3, and X4 independently denotes a hydrogen atom, a halogen atom, an alkyl, or the like, in a solvent containing an aromatic hydrocarbon.
摘要翻译：本发明提供了制备式（3）的茂金属化合物的方法，其中R 1至R 9独立地表示氢原子，卤素原子，烷基等; R 10表示卤素原子，烷基，烷氧基等; X 5和X 6独立地表示氢原子，卤素原子等; 并且M表示周期表第4族的过渡金属原子，该方法的特征在于使式（1）的硅取代的环戊二烯化合物（其中R 1至R 10独立地表示与上述相同的基团） R 11表示烃基或三取代甲硅烷基; 和R 12至R 14独立地表示卤素原子或烃基，与下式（2）的过渡金属化合物，其中M表示与上述相同的基团; X 1，X 2，X 3和X 4独立地表示在含有芳香族烃的溶剂中的氢原子，卤素原子，烷基等。

8. 发明申请

US20090253015A1 POLYARYLENE BLOCK COPOLYMER AND USE THEREOF 审中-公开
标题翻译：聚烯烃嵌段共聚物及其用途
公开(公告)号：US20090253015A1
公开(公告)日：2009-10-08
申请号：US11817835
申请日：2006-03-09
申请人： Toru Onodera , Takashi Yamada , Shigeru Sasaki , Katsuhiro Suenobu , Takashi Kamikawa , Noriyuki Hida
发明人： Toru Onodera , Takashi Yamada , Shigeru Sasaki , Katsuhiro Suenobu , Takashi Kamikawa , Noriyuki Hida
IPC分类号： H01M8/10 , B01J41/12 , C08J5/22
CPC分类号： H01M8/1058 , C08G61/12 , H01B1/122 , H01M8/1004 , H01M8/1023 , H01M8/1039 , H01M2300/0082 , Y02P70/56
摘要： Provided is a block copolymer comprising one or more segments having an acid group and one or more segments having substantially no acid group, wherein the segment having an acid group is represented by the following formula (1): wherein m represents an integer of 10 or more, Ar1, Ar2 and Ar3 each independently represent a divalent aromatic group, these divalent aromatic groups may be substituted by an alkyl group having 1-10 carbon atoms, an alkoxy group having 1-10 carbon atoms, an aryl group having 6-10 carbon atoms or an aryloxy group having 6-10 carbon atoms; at least one of Ar1 and Ar2 has an acid group, Ar3 may or may not have an acid group; Y represents —CO— or —SO2—, a plurality of Ys may be different from each other, and the segment having substantially no acid group has a repeating unit represented by the following formula (2): wherein n represents an integer of 10 or more, Ar4 and Ar5 each independently represent a divalent aromatic group, these divalent aromatic groups may be substituted by an alkyl group having 1-10 carbon atoms, an alkoxy group having 1-10 carbon atoms, an aryl group having 6-10 carbon atoms, an aryloxy group having 6-10 carbon atoms or a fluoro group; Z represents —CO—, or —SO2—, a plurality of Zs may be different from each other. It shows more excellent performance as a polymer electrolyte in fuel cells and the like.
摘要翻译：本发明提供含有一个或多个具有酸基和一个或多个基本上不含酸基的链段的嵌段共聚物，其中具有酸基的链段由下式（1）表示：其中m表示整数10或更优选Ar 1，Ar 2和Ar 3各自独立地表示二价芳族基团，这些二价芳族基团可以被具有1-10个碳原子的烷基，具有1-10个碳原子的烷氧基，6-10 碳原子或具有6-10个碳原子的芳氧基; Ar 1和Ar 2中的至少一个具有酸基，Ar 3可以具有或不具有酸基; Y表示-CO-或-SO2-，多个Y可以彼此不同，并且基本上没有酸基的链段具有由下式（2）表示的重复单元：其中n表示整数10或此外，Ar 4和Ar 5各自独立地表示二价芳族基团，这些二价芳基可以被具有1-10个碳原子的烷基，具有1-10个碳原子的烷氧基，具有6-10个碳原子的芳基取代，具有6-10个碳原子的芳氧基或氟基; Z表示-CO-或-SO 2 - ，多个Z可以彼此不同。作为燃料电池等中的高分子电解质，表现出更优异的性能。

9. 发明申请

US20080287646A1 Polyarylene and Method for Producing the Same 审中-公开
标题翻译：聚亚芳基及其制备方法
公开(公告)号：US20080287646A1
公开(公告)日：2008-11-20
申请号：US12083336
申请日：2006-09-06
申请人： Noriyuki Hida , Seiji Oda , Takashi Kamikawa , Toru Onodera
发明人： Noriyuki Hida , Seiji Oda , Takashi Kamikawa , Toru Onodera
IPC分类号： C08G75/24 , C08G75/30 , C07C309/39
CPC分类号： C08G61/10 , C07C309/73 , C07C311/16 , C07C2601/14 , H01M8/1025 , H01M8/1027 , H01M8/103 , H01M8/1032 , H01M8/1039 , H01M8/1072 , H01M2300/0082 , Y02P70/56
摘要： A dihalobenzene compound represented by the formula (1): wherein A represents a C3-C20 alkoxy group etc., R1 represents a hydrogen atom, a fluorine atom, a C1-C20 alkyl group, etc., X1 represents a chlorine atom, etc., m represents 1 or 2, and k represents 4-m, and a polyarylene comprising a repeating unit represented by the formula (2): wherein A, R1, m and k represent the same meanings as defined above.
摘要翻译：由式（1）表示的二卤苯化合物：其中A表示C 3 -C 20烷氧基等，R 1表示氢原子，氟原子，C 1 -C 20烷基等，X 1表示氯原子等，m表示1或2，k表示4-m，并且包含由式（2）表示的重复单元的聚亚芳基：其中A，R m和k表示与上述相同的含义。

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