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1. 发明申请

US20100056361A1 PROCESS FOR PRODUCING DISPERSION OF FINE CORE/SHELL TYPE METAL OXIDE PARTICLES AND DISPERSION 审中-公开
标题翻译：生产细核/壳型金属氧化物颗粒和分散体的分散方法
公开(公告)号：US20100056361A1
公开(公告)日：2010-03-04
申请号：US12444508
申请日：2007-10-04
申请人： Noriya Izu , Ichiro Matsubara , Toshio Itoh , Woosuck Shin
发明人： Noriya Izu , Ichiro Matsubara , Toshio Itoh , Woosuck Shin
IPC分类号： B01J31/06 , C08K3/22
CPC分类号： B01J13/14 , B82Y30/00 , C01B13/32 , C01F17/0043 , C01G9/02 , C01G99/006 , C01P2002/72 , C01P2002/82 , C01P2002/88 , C01P2004/03 , C01P2004/04 , C01P2004/10 , C01P2004/32 , C01P2004/52 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C01P2004/84 , C01P2006/22 , C09C3/10
摘要： The present invention is to provide a process for producing a dispersion of fine core/shell type metal oxide particles and the dispersion thereby produced, the present invention are a process for producing a dispersion of fine core/shell type metal oxide particles comprising the steps of mixing a metal salt and a polymer in an organic solvent to obtain a mixture and heating this mixture under reflux at a prescribed temperature to precipitate metal oxide, wherein the metal salt is a nitrate salt or acetate salt and the particle diameter of the fine core/shell type metal oxide particles is adjusted using the molecular weight of the polymer, and a dispersion of fine core/shell type metal oxide particles obtained by the process, which does not undergo sedimentation even after standing for at least one day, and exhibits long-term stability, and a powder thereof.
摘要翻译：本发明提供一种核/壳型金属氧化物微粒分散体的制造方法及其制造的分散体，本发明是一种核/壳型金属氧化物微粒分散体的制造方法，其特征在于，将金属盐和聚合物在有机溶剂中混合以获得混合物，并在规定温度下将该混合物加热回流以沉淀金属氧化物，其中金属盐为硝酸盐或乙酸盐，细芯/ 使用聚合物的分子量调节壳型金属氧化物粒子，通过该方法获得的细芯/壳型金属氧化物粒子的分散体，即使在静置至少一天后也不会沉降，长期稳定性及其粉末。

2. 发明授权

US07282384B2 Thermoelectric transducing material thin film, sensor device, and its manufacturing method 有权
标题翻译：热电转换材料薄膜，传感器装置及其制造方法
公开(公告)号：US07282384B2
公开(公告)日：2007-10-16
申请号：US10532825
申请日：2003-11-11
申请人： Woosuck Shin , Fabin Qiu , Noriya Izu , Ichiro Matsubara , Norimitsu Murayama
发明人： Woosuck Shin , Fabin Qiu , Noriya Izu , Ichiro Matsubara , Norimitsu Murayama
IPC分类号： H01L21/203 , H01L35/34
CPC分类号： H01L35/22 , G01N27/16
摘要： The present invention provides an SiGe-based thin film, a method for manufacturing this thin film, and applications of this thin film. The present invention relates to a method for producing, by sputtering, an SiGe-based semiconductor thin film to serve as a member of a thermoelectric transducing material component that is a constituent element of a sensor device whose signal source is a temperature differential and that transduces a local temperature differential into an electric signal, wherein the SiGe-based thin film is produced by heat treating a SiGe-based semiconductor thin film material after sputtering vaporization; to the above-mentioned method for forming a thin film wherein the substrate temperature and/or the plasma output is raised in the formation of the SiGe-based semiconductor thin film by sputtering vaporization, to form a thin film with a more highly crystallized structure; to an SiGe-based thin film produced by the above-mentioned method, which serves as a member of a thermoelectric transducing material component that is a constituent element of a sensor device whose signal source is a temperature differential and that transduces a local temperature differential into an electric signal, and which has been endowed with good thermoelectric characteristics by heat treatment; and to a gas sensor device containing as a constituent element the above-mentioned SiGe-based thin film.
摘要翻译：本发明提供一种SiGe系薄膜，该薄膜的制造方法以及该薄膜的应用。本发明涉及通过溅射制造SiGe系半导体薄膜，作为其信号源为温度差的传感器装置的构成元件的热电转换材料部件的部件的制造方法，局部温差成为电信号，其中通过在溅射蒸发之后热处理SiGe基半导体薄膜材料来制造SiGe基薄膜; 涉及上述形成薄膜的方法，其中在通过溅射蒸发形成SiGe基半导体薄膜时衬底温度和/或等离子体输出升高以形成具有更高结晶结构的薄膜; 涉及通过上述方法制造的基于SiGe的薄膜，其作为热电转换材料成分的一部分，该热电转换材料成分是其信号源是温差的传感器装置的组成元件，并将局部温差转换成电信号，通过热处理赋予了良好的热电特性; 以及包含作为构成元素的上述SiGe系薄膜的气体传感器装置。

3. 发明申请

US20060063291A1 Thermoelectric transducing material thin film, sensor device, and its manufacturing method 有权
标题翻译：热电转换材料薄膜，传感器装置及其制造方法
公开(公告)号：US20060063291A1
公开(公告)日：2006-03-23
申请号：US10532825
申请日：2003-11-11
申请人： Woosuck Shin , Fabin Qiu , Noriya Izu , Ichiro Matsubara , Norimitsu Murayama
发明人： Woosuck Shin , Fabin Qiu , Noriya Izu , Ichiro Matsubara , Norimitsu Murayama
IPC分类号： H01L21/363 , H01L29/12
CPC分类号： H01L35/22 , G01N27/16
摘要： The present invention provides an SiGe-based thin film, a method for manufacturing this thin film, and applications of this thin film. The present invention relates to a method for producing, by sputtering, an SiGe-based semiconductor thin film to serve as a member of a thermoelectric transducing material component that is a constituent element of a sensor device whose signal source is a temperature differential and that transduces a local temperature differential into an electric signal, wherein the SiGe-based thin film is produced by heat treating a SiGe-based semiconductor thin film material after sputtering vaporization; to the above-mentioned method for forming a thin film wherein the substrate temperature and/or the plasma output is raised in the formation of the SiGe-based semiconductor thin film by sputtering vaporization, to form a thin film with a more highly crystallized structure; to an SiGe-based thin film produced by the above-mentioned method, which serves as a member of a thermoelectric transducing material component that is a constituent element of a sensor device whose signal source is a temperature differential and that transduces a local temperature differential into an electric signal, and which has been endowed with good thermoelectric characteristics by heat treatment; and to a gas sensor device containing as a constituent element the above-mentioned SiGe-based thin film.
摘要翻译：本发明提供一种SiGe系薄膜，该薄膜的制造方法以及该薄膜的应用。本发明涉及通过溅射制造SiGe系半导体薄膜，作为其信号源为温度差的传感器装置的构成元件的热电转换材料部件的部件的制造方法，局部温差成为电信号，其中通过在溅射蒸发之后热处理SiGe基半导体薄膜材料来制造SiGe基薄膜; 涉及上述形成薄膜的方法，其中在通过溅射蒸发形成SiGe基半导体薄膜时衬底温度和/或等离子体输出升高以形成具有更高结晶结构的薄膜; 涉及通过上述方法制造的基于SiGe的薄膜，其作为热电转换材料成分的一部分，该热电转换材料成分是其信号源是温差的传感器装置的组成元件，并将局部温度差转换成电信号，通过热处理赋予了良好的热电特性; 以及包含作为构成元素的上述SiGe系薄膜的气体传感器装置。

4. 发明申请

US20060057292A1 Process for producing oxygen partial pressure detecting part of resistance oxygen sensor 审中-公开
标题翻译：电阻氧传感器氧分压检测部分生产工艺
公开(公告)号：US20060057292A1
公开(公告)日：2006-03-16
申请号：US10540873
申请日：2003-12-22
申请人： Noriya Izu , Woosuck Shin , Ichiro Matsubara , Norimitsu Murayama , Yukihiko Yamauchi , Shuzo Kanzaki
发明人： Noriya Izu , Woosuck Shin , Ichiro Matsubara , Norimitsu Murayama , Yukihiko Yamauchi , Shuzo Kanzaki
IPC分类号： B05D3/02 , C08J7/04
CPC分类号： G01N27/125
摘要： The present invention provides a method of manufacturing a porous thick film of an oxide that has extremely few cracks and can be satisfactorily used as an oxygen partial pressure detecting part of an oxygen sensor. The present invention relates to a method of manufacturing such a porous thick film as an oxygen partial pressure detecting part of a resistive oxygen sensor comprising taking a fine particle powder of an oxide containing cerium oxide as a raw material powder, preparing a paste containing the oxide, printing the paste onto a substrate by screen printing, calcining and sintering, the method comprising a step of carrying out heat treatment to effect particle growth from the average particle diameter of the raw material powder to a particle diameter less than the average particle diameter of the ultimately obtained thick film, a step of mixing the particle growth-effected powder with a solvent, a step of dispersing agglomerated particles in the solvent, a step of removing a precipitate, a step of evaporating off the solvent, and a step of mixing the resulting oxide with an organic binder to obtain the paste.
摘要翻译：本发明提供一种制造氧化物的多孔厚膜的方法，其具有极少的裂纹，可以令人满意地用作氧传感器的氧分压检测部。本发明涉及一种电阻式氧传感器的氧分压检测部分的多孔厚膜的制造方法，其特征在于，将含有氧化铈的氧化物的微粒粉末作为原料粉末，制备含有氧化物通过丝网印刷，煅烧和烧结将糊料印刷在基材上，该方法包括进行热处理以使颗粒生长从原料粉末的平均粒径到小于平均粒径的粒径的步骤最终获得的厚膜，将颗粒生长粉末与溶剂混合的步骤，将附聚颗粒分散在溶剂中的步骤，除去沉淀物的步骤，蒸发溶剂的步骤和混合步骤得到的氧化物与有机粘合剂得到糊状物。

5. 发明授权

US09216305B2 Core-shell-type cerium oxide microparticle, dispersion solution comprising the microparticle, and process for production of the microparticle or dispersion solution 有权
标题翻译：核壳型氧化铈微粒，包含微粒的分散液，以及微粒或分散液的制造方法
公开(公告)号：US09216305B2
公开(公告)日：2015-12-22
申请号：US12444799
申请日：2007-10-09
申请人： Noriya Izu , Ichiro Matsubara , Woosuck Shin , Toshio Itoh
发明人： Noriya Izu , Ichiro Matsubara , Woosuck Shin , Toshio Itoh
IPC分类号： C01F1/00 , A61Q17/04 , A61K8/02 , A61K8/11 , A61K8/19 , A61K8/73 , A61K8/81 , B01J13/14 , B82Y30/00 , C01F17/00
CPC分类号： A61Q17/04 , A61K8/0275 , A61K8/11 , A61K8/19 , A61K8/731 , A61K8/8176 , A61K2800/413 , A61K2800/437 , A61K2800/624 , B01J13/14 , B82Y30/00 , C01F17/0043 , C01P2002/82 , C01P2002/84 , C01P2002/88 , C01P2004/02 , C01P2004/03 , C01P2004/04 , C01P2004/32 , C01P2004/52 , C01P2004/64 , C01P2004/84 , Y10T428/2998
摘要： An object of the present invention is to provide a core-shell-type cerium oxide microparticle, a dispersion solution comprising the microparticle, and a process for production of the microparticle or dispersion solution, and to achieve the object, the present invention provides a core-shell-type cerium oxide microparticle which has an average particle diameter of 30 to 200 nm and a coefficient of variation therein no greater than 0.25, and in which the secondary particle forming the core portion is spherical in shape and a polymer is attached to its surface, a dispersion solution of this cerium oxide microparticle and a dry powder from the cerium oxide microparticle dispersion solution, and a process of producing a core-shell-type cerium oxide microparticle or a dispersion solution thereof, which comprises the steps of: mixing a cerium salt and a polymer in an organic solvent to obtain a mixture; and heating this mixture under reflux at a prescribed temperature to precipitate core-shell-type cerium oxide microparticles, wherein the cerium salt is cerium nitrate and the particle diameter of the microparticles is adjusted using the molecular weight of the polymer.
摘要翻译：本发明的目的是提供一种核 - 壳型氧化铈微粒，包含该微粒的分散溶液以及该微粒或分散液的制造方法，其目的在于提供一种核壳型氧化铈微粒，其平均粒径为30〜200nm，变异系数不大于0.25，其中形成芯部的二次粒子为球状，聚合物附着于其上表面，该氧化铈微粒的分散溶液和来自氧化铈微粒分散液的干粉，以及制备核 - 壳型氧化铈微粒或其分散液的方法，其包括以下步骤：将铈盐和聚合物在有机溶剂中得到混合物; 并在规定的温度下将该混合物加热回流以析出核 - 壳型氧化铈微粒，其中铈盐为硝酸铈，并使用聚合物的分子量调节微粒的粒径。

6. 发明授权

US08647679B2 Core-shell type zinc oxide microparticle or dispersion containing the microparticle, and production process and use of the microparticle or the dispersion 有权
标题翻译：含有微粒的核壳型氧化锌微粒或分散体，以及微粒或分散体的制造方法和用途
公开(公告)号：US08647679B2
公开(公告)日：2014-02-11
申请号：US12865464
申请日：2009-02-06
申请人： Noriya Izu , Ichiro Matsubara , Toshio Itoh , Woosuck Shin , Maiko Nishibori
发明人： Noriya Izu , Ichiro Matsubara , Toshio Itoh , Woosuck Shin , Maiko Nishibori
IPC分类号： A61K33/32 , A61K8/00 , A61K9/00 , A01N25/26 , A01N55/02
CPC分类号： A61K8/27 , A61K8/0275 , A61K8/731 , A61K8/8176 , A61K2800/412 , A61K2800/624 , A61Q17/04 , B82Y30/00 , C01G9/02 , C01P2002/72 , C01P2002/82 , C01P2002/88 , C01P2004/03 , C01P2004/04 , C01P2004/62 , C01P2004/64 , C01P2004/84 , C09C1/043
摘要： Disclosed herein are core-shell type zinc oxide microparticles, a dispersion containing such microparticles, and a production process and uses of the microparticles and the dispersion. As disclosed herein, the core-shell type zinc oxide microparticles have an average particle diameter of from 50 to 1,000 nm. The core is a secondary particle of spherical shape to the surface of which a polymer is attached as a shell. Methods for making the microparticles include the steps of: mixing together a zinc salt and a polymer in an organic solvent so as to obtain a mixture; and heating/refluxing the mixture at a predetermined temperature so as to cause core-shell type zinc oxide microparticles to precipitate, wherein the zinc salt is zinc acetate; and uses such as cosmetics, resins and fibers which contain the core-shell type zinc oxide microparticles and have an ultraviolet light blocking action.
摘要翻译：本文公开了核 - 壳型氧化锌微粒，含有这种微粒的分散体，以及微粒和分散体的制造方法和用途。如本文所公开的，核 - 壳型氧化锌微粒的平均粒径为50〜1000nm。核心是其表面上的球形二次颗粒，其中聚合物作为壳连接。制造微粒的方法包括以下步骤：在有机溶剂中将锌盐和聚合物混合在一起以获得混合物; 并在预定温度下加热/回流混合物以使核壳型氧化锌微粒沉淀，其中锌盐为乙酸锌; 并且使用含有核 - 壳型氧化锌微粒的化妆品，树脂和纤维，并且具有紫外线阻挡作用。

7. 发明申请

US20100209710A1 MANUFACTURING METHOD OF CORE-SHELL-TYPE CERIA-POLYMER HYBRID NANOPARTICLES AND DISPERSION SOLS OF THEM 有权
标题翻译：核心类型聚合物混合纳米粒子及其分散体的制备方法
公开(公告)号：US20100209710A1
公开(公告)日：2010-08-19
申请号：US12646295
申请日：2009-12-23
申请人： Noriya IZU , Ichiro Matsubara , Toshio Itoh , Woosuck Shin , Maiko Nishibori , Toshio Uchida
发明人： Noriya IZU , Ichiro Matsubara , Toshio Itoh , Woosuck Shin , Maiko Nishibori , Toshio Uchida
IPC分类号： C08K3/22 , B32B1/00
CPC分类号： C09C1/00 , B82Y30/00 , C01F17/0043 , C01P2004/52 , C01P2004/62 , C01P2004/64 , C01P2004/84 , C01P2006/10 , C01P2006/12 , Y10T428/2998
摘要： The invention provides a method for manufacturing spherical, monodispersed core-shell type ceria-polymer hybrid nanoparticles including, a mixing step in which a cerium salt and a polymer are mixed together in a high-boiling-point organic solvent to obtain a mixture, and a heating and reflux step in which this mixture is heated and refluxed at a temperature of 110° C. or more to thereby generate a boiling phenomenon in the heating and reflux step, and rapidly cooling the mixture after the heating and reflux step to precipitate cerium oxide, and a liquid dispersion thereof.
摘要翻译：本发明提供一种制造球形单分散核 - 壳型二氧化铈 - 聚合物杂化纳米颗粒的方法，包括将铈盐和聚合物在高沸点有机溶剂中混合以获得混合物的混合步骤，以及加热回流步骤，其中将该混合物在110℃或更高的温度下加热回流，从而在加热和回流步骤中产生沸腾现象，并在加热和回流步骤后迅速冷却混合物以沉淀铈氧化物及其液体分散体。

8. 发明授权

US07578974B2 Resistive type oxygen sensor and air/fuel ratio control system using it 有权
标题翻译：电阻式氧传感器和空/燃比控制系统使用它
公开(公告)号：US07578974B2
公开(公告)日：2009-08-25
申请号：US11252721
申请日：2005-10-19
申请人： Noriya Izu , Norimitsu Murayama , Woosuck Shin , Ichiro Matsubara
发明人： Noriya Izu , Norimitsu Murayama , Woosuck Shin , Ichiro Matsubara
IPC分类号： G01N30/96
CPC分类号： G01N27/125
摘要： A resistance-type oxygen sensor which is provided to be used mainly for measuring the oxygen gas partial pressure of automobile exhaust gas, and which has a short output response time in response to changes in oxygen partial pressure, low resistivity of the oxide semiconductor, and low temperature dependence of the resistivity.In a resistance-type oxygen sensor, in which the oxygen gas detection part comprises an oxide semiconductor, the oxide semiconductor is an oxide comprising cerium ions and hafnium ions, the amount of substance of cerium ions as a percentage of the amount of substance of positive ions is 60 mol % or more, the amount of substance of hafnium ions as a percentage of the amount of substance of positive ions is 3 to 30 mol %, and the hafnium ions are an oxide in solid solution in the parent phase.
摘要翻译：一种电阻型氧传感器，其主要用于测量汽车废气的氧气分压，并且响应于氧分压的变化，氧化物半导体的低电阻率而具有短的输出响应时间，以及电阻率的低温依赖性。在其中氧气检测部分包含氧化物半导体的电阻型氧传感器中，氧化物半导体是包含铈离子和铪离子的氧化物，铈离子的物质的量作为阳性物质的量的百分比离子为60摩尔％以上，作为正离子的物质的量的百分比，铪离子的含量为3〜30摩尔％，铪离子为母相的固溶体中的氧化物。

9. 发明授权

US08846785B2 Manufacturing method of core-shell-type ceria-polymer hybrid nanoparticles and dispersion sols of them 有权
标题翻译：核壳型二氧化铈 - 聚合物杂化纳米粒子及其分散溶胶的制备方法
公开(公告)号：US08846785B2
公开(公告)日：2014-09-30
申请号：US12646295
申请日：2009-12-23
申请人： Noriya Izu , Ichiro Matsubara , Toshio Itoh , Woosuck Shin , Maiko Nishibori , Toshio Uchida
发明人： Noriya Izu , Ichiro Matsubara , Toshio Itoh , Woosuck Shin , Maiko Nishibori , Toshio Uchida
IPC分类号： C08K9/10 , B82Y30/00 , C09C1/00 , C01F17/00
CPC分类号： C09C1/00 , B82Y30/00 , C01F17/0043 , C01P2004/52 , C01P2004/62 , C01P2004/64 , C01P2004/84 , C01P2006/10 , C01P2006/12 , Y10T428/2998
摘要： The invention provides a method for manufacturing spherical, monodispersed core-shell type ceria-polymer hybrid nanoparticles including, a mixing step in which a cerium salt and a polymer are mixed together in a high-boiling-point organic solvent to obtain a mixture, and a heating and reflux step in which this mixture is heated and refluxed at a temperature of 110° C. or more to thereby generate a boiling phenomenon in the heating and reflux step, and rapidly cooling the mixture after the heating and reflux step to precipitate cerium oxide, and a liquid dispersion thereof.
摘要翻译：本发明提供一种制造球形单分散核 - 壳型二氧化铈 - 聚合物杂化纳米颗粒的方法，其包括将铈盐和聚合物在高沸点有机溶剂中混合以获得混合物的混合步骤，以及加热回流步骤，其中将该混合物在110℃或更高的温度下加热回流，从而在加热和回流步骤中产生沸腾现象，并在加热和回流步骤后迅速冷却混合物以沉淀铈氧化物及其液体分散体。

10. 发明申请

US20120142808A1 Aggregate of Spherical Core-Shell Cerium Oxide/Polymer Hybrid Nanoparticles and Method for Producing the Same 有权
标题翻译：球形核 - 壳氧化铈/聚合物杂化纳米粒子的聚集体及其制备方法
公开(公告)号：US20120142808A1
公开(公告)日：2012-06-07
申请号：US13389140
申请日：2010-07-23
申请人： Noriya Izu , Toshio Uchida , Ichiro Matsubara , Toshio Itoh , Woosuck Shin , Maiko Nishibori
发明人： Noriya Izu , Toshio Uchida , Ichiro Matsubara , Toshio Itoh , Woosuck Shin , Maiko Nishibori
IPC分类号： C08K3/22 , C08J3/28 , B82Y30/00 , B82Y40/00
CPC分类号： C09D11/10 , B82Y30/00 , C01F17/0043 , C01P2004/03 , C01P2004/32 , C01P2004/64 , C01P2004/84 , C09D11/037
摘要： The present invention provides an aggregate of spherical core-shell cerium oxide/polymer hybrid nanoparticles, a process for producing the same, and a product such as an anti-reflection film having a high refractive index layer. The present invention relates to an aggregate of spherical core-shell cerium oxide/polymer hybrid nanoparticles in which the core and shell are cerium oxide and a polymer, respectively, and the aggregate is highly concentrated, with a volume fraction of the spherical core-shell cerium oxide/polymer hybrid nanoparticles being at least 32% or higher, the aggregate contains a fixing agent, the aggregate is configured such that the fixing agent fills in voids between the spherical core-shell cerium oxide/polymer hybrid nanoparticles, the aggregate has a uniform distribution of the core-shell cerium oxide/polymer hybrid nanoparticles, which are spherical secondary particles synthesized by the polyol method, and the aggregate has excellent mechanical strength, light transmittance, and UV light-blocking properties; and the present invention further relates a process for producing the same; and an antireflection film and ink having the same.
摘要翻译：本发明提供球形核 - 壳氧化铈/聚合物杂化纳米粒子的集合体，其制造方法以及具有高折射率层的抗反射膜等制品。本发明涉及一种球形核 - 壳氧化铈/聚合物杂化纳米颗粒的集合体，其中核和壳分别为氧化铈和聚合物，聚集体高度浓缩，体积分数为球形核 - 壳氧化铈/聚合物杂化纳米粒子为至少32％以上，聚集体含有固色剂，所述骨料被构造为使得固定剂填充在球形核 - 壳氧化铈/聚合物杂化纳米颗粒之间的空隙中，聚集体具有通过多元醇法合成的球形二次粒子的核 - 壳氧化铈/聚合物杂化纳米粒子的均匀分布，骨料具有优异的机械强度，透光率和UV遮光性; 本发明还涉及其制造方法; 以及具有该防反射膜和防反射膜的墨。

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