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1. 发明授权

US5776237A Process for preparing pigment composition, pigment composition and its use 失效
标题翻译：制备颜料组合物，颜料组合物及其用途的方法
公开(公告)号：US5776237A
公开(公告)日：1998-07-07
申请号：US840930
申请日：1997-04-25
申请人： Nobuyuki Tomiya , Mikio Hayashi
发明人： Nobuyuki Tomiya , Mikio Hayashi
IPC分类号： C09B67/08 , C08K5/56 , C08L101/00 , C09B67/04 , C09B67/20 , C09B67/50 , C09D11/00 , C09D11/033 , C09D11/037 , C09D11/10 , C09D11/103
CPC分类号： C09B67/0097 , C09B67/0002 , C09B67/0026 , C09D11/037
摘要： According to the present invention, a resin is added to crude copper phthalocyanine comprising an .alpha.-form and a .beta.-form crystals in combination and dry-milling is performed in a deoxygenated atmosphere, to provide copper phthalocyanine pigment composition of superior quality which reduces considerable expenditure of time and labor associated with the pigmentation process of crude copper phthalocyanine and the printing ink production process of a pigment, and printing ink comprising .beta.-form copper phthalocyanine pigment superior quality.
摘要翻译：根据本发明，将一种树脂加入到包含α型和β型晶体的粗铜酞菁中，并在脱氧气氛中进行干磨，以提供优异品质的铜酞菁颜料组合物，其降低可观与粗铜酞菁的着色过程和颜料的印刷油墨生产过程相关的时间和劳动的支出，以及包含β-型铜酞菁颜料优质的印刷油墨。

2. 发明申请

US20080022902A1 Process for producing dichlorodiketopyrrolopyrrole pigment of the alpha modificaton, dichlorodiketopyrrolopyrrole pigment of the alpha modification produced by the process, and coloring composition using the same 有权
标题翻译：用于制备由该方法生产的α改性的α修饰二氯二吡咯并吡咯颜料的二氯二吡咯并吡咯颜料和使用其的着色组合物的方法
公开(公告)号：US20080022902A1
公开(公告)日：2008-01-31
申请号：US11826864
申请日：2007-07-19
申请人： Hidenori Minashima , Nobuyuki Tomiya , Taro Murohoshi
发明人： Hidenori Minashima , Nobuyuki Tomiya , Taro Murohoshi
IPC分类号： C08K5/00 , C07D487/04
CPC分类号： C09B67/003 , C09B67/0002 , C09B67/0014 , C09B67/0022 , C09B67/0033 , C09B67/0039 , C09B67/0041 , C09D11/02 , C09D11/037
摘要： A process for producing dichlorodiketopyrrolopyrrole pigment of the α modification, which comprises wet milling crude dichlorodiketopyrrolopyrrole pigment wherein an α modification and a β modification coexist in the presence of a milling agent and a wetting agent, dichlorodiketopyrrolopyrrole pigment of the α modification obtained the process and a color composition which contains the pigment and a pigment carrier.
摘要翻译：一种制备α改性的二氯代二吡咯并吡咯颜料的方法，其包括湿法研磨粗二氯二吡咯并吡咯并吡咯颜料，其中α修饰和β修饰在研磨剂和润湿剂的存在下共存，得到该方法的α修饰的二氯双吡咯并吡咯颜料和含有颜料和颜料载体的颜色组合物。

3. 发明授权

US5772750A Process for producing .beta.-form copper phthalocyanine pigment 失效
标题翻译：生产β型铜酞菁颜料的方法
公开(公告)号：US5772750A
公开(公告)日：1998-06-30
申请号：US840928
申请日：1997-04-25
申请人： Nobuyuki Tomiya , Mikio Hayashi
发明人： Nobuyuki Tomiya , Mikio Hayashi
IPC分类号： C09B67/12 , C09B67/20 , C09B67/50 , C09B47/04
CPC分类号： C09B67/0026 , C09B67/0016
摘要： The present invention is a method for preparing a .beta.-form copper phthalocyanine pigment comprising the steps of; dry milling crude copper phthalocyanine at a temperature between 110.degree. and 200.degree. C., and transforming an .alpha.-form crystal to a .beta.-form crystal by treating the resulting .alpha.-.beta. mixture of copper phthalocyanine in an organic solvent or a liquid mixture of water and an organic solvent. The preparation method of the present invention offers a .beta.-form copper phthalocyanine pigment at lower cost having equivalent or superior quality in color strength, clearness, fluidity and hue compared to the pigment produced by the conventional salt milling method.
摘要翻译：本发明是一种制备β型铜酞菁颜料的方法，包括以下步骤：在110℃至200℃的温度下干燥粗铜酞菁，并将α-型晶体转化为β-型晶体，通过将所得的酞菁铜的α-β混合物在有机溶剂或液体混合物水和有机溶剂。本发明的制备方法与常规的盐磨法制备的颜料相比，以较低的成本提供了具有相同或更优异的色强度，清晰度，流动性和色调的β型铜酞菁颜料。

4. 发明授权

US07431762B2 Process for producing dichlorodiketopyrrolopyrrole pigment of the α modification, dichlorodiketopyrrolopyrrole pigment of the α modification produced by the process, and coloring composition using the same 有权
标题翻译：通过该方法制备的α改性的二氯二吡咯并吡咯颜料的方法，由该方法生产的α改性的二氯二吡咯并吡咯颜料和使用其的着色组合物
公开(公告)号：US07431762B2
公开(公告)日：2008-10-07
申请号：US11826864
申请日：2007-07-19
申请人： Hidenori Minashima , Nobuyuki Tomiya , Taro Murohoshi
发明人： Hidenori Minashima , Nobuyuki Tomiya , Taro Murohoshi
IPC分类号： C09B67/04 , C09B67/10 , C09B67/20 , C09B67/22 , C09B67/48 , C07D487/04 , C08K5/00
CPC分类号： C09B67/003 , C09B67/0002 , C09B67/0014 , C09B67/0022 , C09B67/0033 , C09B67/0039 , C09B67/0041 , C09D11/02 , C09D11/037
摘要： A process for producing dichlorodiketopyrrolopyrrole pigment of the α modification, which comprises wet milling crude dichlorodiketopyrrolopyrrole pigment wherein an α modification and a β modification coexist in the presence of a milling agent and a wetting agent, dichlorodiketopyrrolopyrrole pigment of the α modification obtained the process and a color composition which contains the pigment and a pigment carrier.
摘要翻译：一种制备α改性的二氯代二吡咯并吡咯颜料的方法，其包括湿法研磨粗二氯二吡咯并吡咯并吡咯颜料，其中α修饰和β修饰在研磨剂和润湿剂的存在下共存，得到该方法的α修饰的二氯双吡咯并吡咯颜料和含有颜料和颜料载体的颜色组合物。

5. 发明授权

US5942028A Process for producing printing ink 失效
标题翻译：印刷油墨的制造方法
公开(公告)号：US5942028A
公开(公告)日：1999-08-24
申请号：US930428
申请日：1997-10-06
申请人： Nobuyuki Tomiya , Mikio Hayashi , Hideto Noguchi
发明人： Nobuyuki Tomiya , Mikio Hayashi , Hideto Noguchi
IPC分类号： C09B67/20 , C09B67/04 , C09B67/12 , C09B67/50 , C09D11/02 , C09D11/033 , C09D11/037 , C09D11/10 , C09D11/103 , C09D11/104 , C09D11/106 , C09D11/107 , C09D11/108
CPC分类号： C09D11/037 , C09B67/0002 , C09B67/0016
摘要： High quality .beta.-form copper phthalocyanine pigment printing ink is produced by the present method, this method reducing the large amount of time and labor required in the process of pigmentation of crude copper phthalocyanine and production of the pigment printing ink.To this end, the production method of printing ink according to the present invention is characterized by adding to crude copper phthalocyanine, 20-80 weight % of printing ink resin based on the amount of the crude copper phthalocyanine, dry-milling the mixture at 80-170.degree. C., and heating the ground material in printing ink solvent. The printing ink obtained contains copper phthalocyanine particles of .beta.-form crystals with an aspect ratio of 1-2.
摘要翻译： PCT No.PCT / JP97 / 00275 Sec。 371日期：1997年10月6日 102（e）日期1997年10月6日PCT 1997年2月5日提交PCT公布。 WO97 / 28224 PCT公开号日期1997年7月8日通过本方法生产高品质的β型铜酞菁颜料印刷油墨，该方法减少了粗铜酞菁色素沉淀和色素印刷油墨生产所需的大量时间和劳动。为此，根据本发明的印刷油墨的制造方法的特征在于，将粗铜酞菁添加至基于粗铜酞菁的量的20-80重量％的印刷油墨树脂，将混合物在80℃下干磨 -170℃，并在印刷油墨溶剂中加热研磨材料。获得的印刷油墨含有长宽比为1-2的β型晶体的铜酞菁颗粒。

6. 发明授权

US5243031A Process for the production of monoazo lake pigment coated with water-insoluble rosin and improved in lipophilic nature and water resistance 失效
标题翻译：生产涂有水不溶性松香的单偶氮色淀颜料和改善亲油性和耐水性的方法
公开(公告)号：US5243031A
公开(公告)日：1993-09-07
申请号：US817461
申请日：1992-01-06
申请人： Hitoshi Sugamo , Nobuyuki Tomiya , Yusuke Watabe
发明人： Hitoshi Sugamo , Nobuyuki Tomiya , Yusuke Watabe
IPC分类号： C09B63/00 , C09B67/08
CPC分类号： C09B63/005 , C09B67/001 , Y10S534/04
摘要： A process for the production of a monoazo lake coated with a water-insoluble metal salt of rosin, which comprises the steps of:(a) adjusting a mixed solution containing a monoazo dye having a water-soluble group and an alkali metal or ammonium salt of rosin to pH of 8 to 12, and adding an stoichiometeric amount of a metal salt of at least one metal for insolubilizing rosin selected from the group consisting of zinc, aluminum, copper and manganese to form a water-insoluble rosin metal salt, and(b) adjusting the resultant mixture containing the water-insoluble rosin metal salt to pH of 9 to 12 and adding a metal salt of at least one metal for forming a lake of a monoazo dye selected from the group consisting of calcium, barium and strontium to form a monoazo lake.
摘要翻译：一种用非水溶性松香金属盐涂覆的单偶氮湖的方法，其包括以下步骤：（a）调节含有水溶性基团的单偶氮染料和碱金属或铵盐的混合溶液的松香，pH为8〜12，加入化学计量量的至少一种金属的金属盐，用于不溶解选自锌，铝，铜和锰的松香，以形成水不溶性松香金属盐，以及（b）将含有水不溶性松香金属盐的所得混合物调节至pH为9至12，并加入至少一种用于形成选自钙，钡和锶的单偶氮染料的湖的金属的金属盐形成一个单体湖。

7. 发明授权

US5144014A Process for production of monoazo lake coated with water-insoluble metal salt of rosin 失效
标题翻译：生产涂有松香不溶性水溶性金属盐的单偶氮湖的方法
公开(公告)号：US5144014A
公开(公告)日：1992-09-01
申请号：US564312
申请日：1990-08-08
申请人： Hitoshi Sugamo , Nobuyuki Tomiya , Yusuke Watabe
发明人： Hitoshi Sugamo , Nobuyuki Tomiya , Yusuke Watabe
IPC分类号： C09B63/00 , C09B67/08
CPC分类号： C09B67/001 , C09B63/005 , Y10S534/04
摘要： A monoazo lake which comprises a monoazo dye, a lake-forming metal and a water-insoluble metal salt of a rosin, and which is coated with the water-insoluble water salt of the rosin, the lake-forming metal being at least one metal selected from calcium, barium and strontium, the metal of the water-insoluble metal salt being at least one metal selected from zinc, aluminum, copper and manganese, and a process for the production of a monoazo lake coated with a water-insoluble metal salt of a rosin, which comprises carrying out the following steps (1) and (2) in the order of (1) to (2) or (2) to (1):(1) a step of forming a monoazo lake by forming a lake of a monoazo dye with a metal salt of at least one metal for formation of a lake of the monoazo dye selected from calcium, barium and strontium, and(2) a step of forming the water-insoluble metal salt of the rosin by insolubilizing the rosin with a metal salt of at least one metal for insolubilization of the rosin selected from zinc, aluminum, copper and manganese.
摘要翻译：一种单偶氮湖，其包含单偶氮染料，成盐金属和松香的水不溶性金属盐，并且涂覆有松香的水不溶性水盐，成湖金属是至少一种金属选自钙，钡和锶，不溶于水的金属盐的金属为选自锌，铝，铜和锰中的至少一种金属，以及制备涂覆有不溶于水的金属盐的单偶氮湖的方法包括按照（1）至（2）或（2）至（1）的顺序进行以下步骤（1）和（2）：（1）通过成型形成单偶氮湖的步骤用于形成选自钙，钡和锶的单偶氮染料的湖的至少一种金属的单偶氮染料的湖，以及（2）通过以下步骤形成松香的水不溶性金属盐的步骤：用至少一种金属的金属盐使松香不溶化，用于使选自锌，铝的松香不溶化数字，铜和锰。

8. 再颁专利

USRE37191E1 Process for preparing pigment composition, pigment composition and its use 有权
标题翻译：制备颜料组合物，颜料组合物及其用途的方法
公开(公告)号：USRE37191E1
公开(公告)日：2001-05-29
申请号：US09340582
申请日：1999-06-25
申请人： Nobuyuki Tomiya , Mikio Hayashi
发明人： Nobuyuki Tomiya , Mikio Hayashi
IPC分类号： C09B6750
CPC分类号： C09B67/0097 , C09B67/0002 , C09B67/0026 , C09D11/037
摘要： According to the present invention, a resin is added to crude copper phthalocyanine comprising an &agr;-form and a &bgr;-form crystals in combination and dry-milling is performed in a deoxygenated atmosphere, to provide copper phthalocyanine pigment composition of superior quality which reduces considerable expenditure of time and labor associated with the pigmentation process of crude copper phthalocyanine and the printing ink production process of a pigment, and printing ink comprising &bgr;-form copper phthalocyanine pigment superior quality.
摘要翻译：根据本发明，将组合物中含有α型和β型晶体的粗铜酞菁加入树脂中，在脱氧气氛中进行干磨，得到优异品质的铜酞菁颜料组合物，其降低可观与粗铜酞菁的色素沉淀过程相关的时间和劳动费用以及颜料的印刷油墨生产过程，以及包含β型铜酞菁颜料的印刷油墨具有优良的品质。

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